KR20210118408A - 세라믹 성형체로부터의 유기물 성분의 제거 방법 - Google Patents
세라믹 성형체로부터의 유기물 성분의 제거 방법 Download PDFInfo
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- KR20210118408A KR20210118408A KR1020217024775A KR20217024775A KR20210118408A KR 20210118408 A KR20210118408 A KR 20210118408A KR 1020217024775 A KR1020217024775 A KR 1020217024775A KR 20217024775 A KR20217024775 A KR 20217024775A KR 20210118408 A KR20210118408 A KR 20210118408A
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- 239000000919 ceramic Substances 0.000 title claims abstract description 238
- 238000000034 method Methods 0.000 title claims abstract description 75
- 239000011230 binding agent Substances 0.000 claims abstract description 122
- 150000001875 compounds Chemical class 0.000 claims abstract description 107
- 239000000654 additive Substances 0.000 claims abstract description 64
- 230000000996 additive effect Effects 0.000 claims abstract description 61
- 229920005989 resin Polymers 0.000 claims abstract description 61
- 239000011347 resin Substances 0.000 claims abstract description 61
- -1 nitroxy Chemical group 0.000 claims abstract description 51
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 30
- 150000001412 amines Chemical class 0.000 claims abstract description 21
- 150000007522 mineralic acids Chemical class 0.000 claims abstract description 18
- 150000003839 salts Chemical class 0.000 claims abstract description 18
- 229910001428 transition metal ion Inorganic materials 0.000 claims abstract description 18
- 239000002002 slurry Substances 0.000 claims description 95
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- 238000004519 manufacturing process Methods 0.000 claims description 51
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- 239000002904 solvent Substances 0.000 claims description 20
- 239000003985 ceramic capacitor Substances 0.000 claims description 19
- 239000007983 Tris buffer Substances 0.000 claims description 16
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 14
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- AQBLLJNPHDIAPN-MUCWUPSWSA-K iron(3+);(e)-4-oxopent-2-en-2-olate Chemical compound [Fe+3].C\C([O-])=C/C(C)=O.C\C([O-])=C/C(C)=O.C\C([O-])=C/C(C)=O AQBLLJNPHDIAPN-MUCWUPSWSA-K 0.000 claims description 12
- 229910052723 transition metal Inorganic materials 0.000 claims description 12
- 150000003624 transition metals Chemical class 0.000 claims description 12
- REDXJYDRNCIFBQ-UHFFFAOYSA-N aluminium(3+) Chemical compound [Al+3] REDXJYDRNCIFBQ-UHFFFAOYSA-N 0.000 claims description 9
- ZQZQURFYFJBOCE-SYWGCQIGSA-L manganese(2+);(e)-4-oxopent-2-en-2-olate Chemical compound [Mn+2].C\C([O-])=C/C(C)=O.C\C([O-])=C/C(C)=O ZQZQURFYFJBOCE-SYWGCQIGSA-L 0.000 claims description 9
- JWORPXLMBPOPPU-LNTINUHCSA-K chromium(3+);(z)-4-oxopent-2-en-2-olate Chemical compound [Cr+3].C\C([O-])=C\C(C)=O.C\C([O-])=C\C(C)=O.C\C([O-])=C\C(C)=O JWORPXLMBPOPPU-LNTINUHCSA-K 0.000 claims description 8
- LFTLOKWAGJYHHR-UHFFFAOYSA-N N-methylmorpholine N-oxide Chemical compound CN1(=O)CCOCC1 LFTLOKWAGJYHHR-UHFFFAOYSA-N 0.000 claims description 7
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- JFJXUVXSIUJJNC-LWTKGLMZSA-N (Z)-5-hydroxy-2,2,6,6-tetramethylhept-4-en-3-one manganese Chemical compound [Mn].CC(C)(C)C(\O)=C\C(=O)C(C)(C)C.CC(C)(C)C(\O)=C\C(=O)C(C)(C)C.CC(C)(C)C(\O)=C\C(=O)C(C)(C)C JFJXUVXSIUJJNC-LWTKGLMZSA-N 0.000 claims description 5
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 claims description 5
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 claims description 4
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 claims description 4
- GYCHYNMREWYSKH-UHFFFAOYSA-L iron(ii) bromide Chemical compound [Fe+2].[Br-].[Br-] GYCHYNMREWYSKH-UHFFFAOYSA-L 0.000 claims description 4
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- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims 2
- 238000005259 measurement Methods 0.000 description 43
- 239000000126 substance Substances 0.000 description 43
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- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 description 13
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- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 4
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- HYZQBNDRDQEWAN-MUCWUPSWSA-K manganese(3+);(e)-4-oxopent-2-en-2-olate Chemical compound [Mn+3].C\C([O-])=C/C(C)=O.C\C([O-])=C/C(C)=O.C\C([O-])=C/C(C)=O HYZQBNDRDQEWAN-MUCWUPSWSA-K 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
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- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
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- 230000015572 biosynthetic process Effects 0.000 description 1
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- AOWKSNWVBZGMTJ-UHFFFAOYSA-N calcium titanate Chemical compound [Ca+2].[O-][Ti]([O-])=O AOWKSNWVBZGMTJ-UHFFFAOYSA-N 0.000 description 1
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- HVENHVMWDAPFTH-UHFFFAOYSA-N iron(3+) trinitrate hexahydrate Chemical compound O.O.O.O.O.O.[Fe+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O HVENHVMWDAPFTH-UHFFFAOYSA-N 0.000 description 1
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- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
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- 230000001590 oxidative effect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
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- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
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- 239000002994 raw material Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910052596 spinel Inorganic materials 0.000 description 1
- 239000011029 spinel Substances 0.000 description 1
- UHCGLDSRFKGERO-UHFFFAOYSA-N strontium peroxide Chemical compound [Sr+2].[O-][O-] UHCGLDSRFKGERO-UHFFFAOYSA-N 0.000 description 1
- VEALVRVVWBQVSL-UHFFFAOYSA-N strontium titanate Chemical compound [Sr+2].[O-][Ti]([O-])=O VEALVRVVWBQVSL-UHFFFAOYSA-N 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- FEONEKOZSGPOFN-UHFFFAOYSA-K tribromoiron Chemical compound Br[Fe](Br)Br FEONEKOZSGPOFN-UHFFFAOYSA-K 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- UYPYRKYUKCHHIB-UHFFFAOYSA-N trimethylamine N-oxide Chemical compound C[N+](C)(C)[O-] UYPYRKYUKCHHIB-UHFFFAOYSA-N 0.000 description 1
- 229910021642 ultra pure water Inorganic materials 0.000 description 1
- 239000012498 ultrapure water Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 229940105296 zinc peroxide Drugs 0.000 description 1
- 229910000859 α-Fe Inorganic materials 0.000 description 1
Classifications
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- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B11/00—Apparatus or processes for treating or working the shaped or preshaped articles
- B28B11/24—Apparatus or processes for treating or working the shaped or preshaped articles for curing, setting or hardening
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- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G4/00—Fixed capacitors; Processes of their manufacture
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Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JPJP-P-2019-013236 | 2019-01-29 | ||
| JP2019013236 | 2019-01-29 | ||
| PCT/JP2020/003006 WO2020158742A1 (ja) | 2019-01-29 | 2020-01-28 | セラミック成形体からの有機物成分の除去方法 |
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| CN (1) | CN113382977B (zh) |
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| JPH0684408A (ja) * | 1992-09-01 | 1994-03-25 | Matsushita Electric Ind Co Ltd | 耐還元性誘電体磁器組成物およびそれを用いた積層セラミックコンデンサ |
| JP3201011B2 (ja) * | 1992-10-23 | 2001-08-20 | 株式会社村田製作所 | 積層型電子部品用セラミックグリーンシート成形用バインダ |
| JP3201034B2 (ja) * | 1993-01-08 | 2001-08-20 | 株式会社村田製作所 | 積層型電子部品用セラミックグリーンシート形成用バインダ |
| US5726139A (en) * | 1996-03-14 | 1998-03-10 | The Procter & Gamble Company | Glass cleaner compositions having good filming/streaking characteristics containing amine oxide polymers functionality |
| JPH11157945A (ja) * | 1997-11-28 | 1999-06-15 | Matsushita Electric Ind Co Ltd | セラミック電子部品の製造方法及びそれに用いるダミー用グリーンシート |
| US6306948B1 (en) | 1999-10-26 | 2001-10-23 | 3M Innovative Properties Company | Molding composition containing a debinding catalyst for making ceramic microstructures |
| JP3473548B2 (ja) * | 2000-04-27 | 2003-12-08 | 株式会社村田製作所 | 金属粉末の製造方法，金属粉末，これを用いた導電性ペーストならびにこれを用いた積層セラミック電子部品 |
| US7867349B2 (en) * | 2004-08-04 | 2011-01-11 | Tdk Corporation | Thick film green sheet slurry, production method of thick film green sheet slurry, production method of thick film green sheet and production methods of thick film green sheet and electronic device |
| JPWO2007141883A1 (ja) * | 2006-06-06 | 2009-10-15 | 株式会社日本マイクロニクス | 電気配線の形成方法およびその補修方法 |
| WO2008050757A1 (fr) * | 2006-10-24 | 2008-05-02 | Murata Manufacturing Co., Ltd. | Composition de bouillie pour feuille de céramique crue et son procédé de fabrication, et composant électronique céramique multicouches et son procédé de fabrication |
| JPWO2010050590A1 (ja) * | 2008-10-30 | 2012-03-29 | 旭硝子株式会社 | ガラスペースト |
| KR101780839B1 (ko) * | 2010-01-26 | 2017-09-21 | 주식회사 쿠라레 | 세라믹 그린 시트용 슬러리 조성물, 세라믹 그린 시트 및 적층 세라믹 콘덴서 |
| WO2011102197A1 (ja) * | 2010-02-16 | 2011-08-25 | 株式会社クラレ | セラミックグリーンシート用ポリビニルアセタール樹脂、およびその製造方法、スラリー組成物、セラミックグリーンシート及び積層セラミックコンデンサ |
| US20130148263A1 (en) | 2010-08-19 | 2013-06-13 | Kuraray Co., Ltd | Polyvinyl acetal resin, slurry composition prepared therefrom, ceramic green sheet, and multilayer ceramic capacitor |
| JP5630333B2 (ja) | 2011-03-08 | 2014-11-26 | 信越化学工業株式会社 | 易焼結性炭化ケイ素粉末及び炭化ケイ素セラミックス焼結体 |
| CN103130511A (zh) * | 2013-03-05 | 2013-06-05 | 胡先念 | 含有乙酸仲丁酯的陶瓷浆料组合物及乙酸仲丁酯在制备陶瓷浆料组合物中的用途 |
| CN109768280A (zh) * | 2018-12-20 | 2019-05-17 | 中国科学院青岛生物能源与过程研究所 | 一种具有自由基捕获功能的锂电池正极 |
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| WO2020158742A1 (ja) | 2020-08-06 |
| CN113382977A (zh) | 2021-09-10 |
| JP7493946B2 (ja) | 2024-06-03 |
| CN113382977B (zh) | 2023-05-05 |
| JP2020121918A (ja) | 2020-08-13 |
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