KR102179936B1 - 제올라이트 물질의 후처리 - Google Patents

제올라이트 물질의 후처리 Download PDF

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KR102179936B1
KR102179936B1 KR1020157012944A KR20157012944A KR102179936B1 KR 102179936 B1 KR102179936 B1 KR 102179936B1 KR 1020157012944 A KR1020157012944 A KR 1020157012944A KR 20157012944 A KR20157012944 A KR 20157012944A KR 102179936 B1 KR102179936 B1 KR 102179936B1
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zeolite material
zeolite
range
acid
treatment
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KR20150074085A (ko
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슈테판 마우러
파루크 외즈키림
안드레이-니콜라 파르불레스쿠
제프 양
울리히 뮐러
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바스프 에스이
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B01J35/1014—
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
KR1020157012944A 2012-10-18 2013-10-09 제올라이트 물질의 후처리 Active KR102179936B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12189040 2012-10-18
EP12189040.4 2012-10-18
PCT/EP2013/071041 WO2014060260A1 (en) 2012-10-18 2013-10-09 Post-treatment of a zeolitic material

Publications (2)

Publication Number Publication Date
KR20150074085A KR20150074085A (ko) 2015-07-01
KR102179936B1 true KR102179936B1 (ko) 2020-11-17

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ID=47115431

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KR1020157012944A Active KR102179936B1 (ko) 2012-10-18 2013-10-09 제올라이트 물질의 후처리

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Country Link
US (1) US10000387B2 (https=)
EP (1) EP2909144B1 (https=)
JP (1) JP6367812B2 (https=)
KR (1) KR102179936B1 (https=)
CN (1) CN104854031B (https=)
BR (1) BR112015008391B1 (https=)
ES (1) ES2697129T3 (https=)
MX (1) MX357216B (https=)
MY (1) MY181782A (https=)
RU (1) RU2637021C2 (https=)
SG (2) SG10201703183UA (https=)
WO (1) WO2014060260A1 (https=)
ZA (1) ZA201503392B (https=)

Families Citing this family (19)

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Publication number Priority date Publication date Assignee Title
US10301185B2 (en) 2014-10-15 2019-05-28 Basf Se Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom
WO2016128917A1 (en) 2015-02-12 2016-08-18 Basf Se Process for the preparation of a dealuminated zeolitic material having the bea framework structure
JP6879680B2 (ja) * 2015-06-29 2021-06-02 日揮触媒化成株式会社 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト
JP6949842B2 (ja) * 2015-12-09 2021-10-13 ビーエーエスエフ コーポレーション Ｃｈａ型ゼオライト材料、並びにシクロアルキル−、及びエチルトリメチルアンモニウム化合物の組み合わせを用いるそれらの製造方法
KR102797067B1 (ko) * 2016-02-03 2025-04-18 바스프 모바일 에미션스 카탈리스츠 엘엘씨 구리 및 철 동시-교환된 캐버자이트 촉매
US10995008B2 (en) * 2016-03-30 2021-05-04 Basf Se Process for the flash calcination of a zeolitic material
CN109195911B (zh) 2016-05-23 2023-04-07 东曹株式会社 Cha型沸石和其制造方法
ES2901603T3 (es) * 2016-06-07 2022-03-23 Chevron Usa Inc Zeolitas de tipo marco AFX con alto contenido de sílice
EP3519354A1 (en) * 2016-09-30 2019-08-07 Johnson Matthey Public Limited Company A novel zeolite synthesis with a fluoride source
JP2020514329A (ja) 2017-03-15 2020-05-21 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 環状ジエステルまたは環状ジアミドを製造する、ゼオライト触媒による方法
CN108946755B (zh) * 2017-05-22 2020-08-07 中国石油化工股份有限公司 无锗iwr沸石分子筛的合成方法
MY190284A (en) * 2017-10-11 2022-04-12 Tosoh Corp Metal-containing cha-type zeolite and method for producing the same
EP3749611A4 (en) * 2018-02-06 2022-02-23 Basf Se PROCESS FOR PRODUCTION OF A ZEOLITE MATERIAL WITH RTH FRAME STRUCTURE
FR3081347B1 (fr) * 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
KR20220069039A (ko) * 2019-09-20 2022-05-26 바스프 에스이 Ith 프레임워크 구조 유형을 갖는 제올라이트 물질의 합성 및 용도
CN111252781B (zh) * 2020-02-05 2022-01-07 浙江大学 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法
JP7514467B2 (ja) * 2020-05-12 2024-07-11 国立大学法人 東京大学 ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤
JP2024510661A (ja) 2021-03-19 2024-03-08 ビーエーエスエフ ソシエタス・ヨーロピア ゼオライト材料の脱アルミニウム化方法
JPWO2024204696A1 (https=) 2023-03-31 2024-10-03

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Also Published As

Publication number Publication date
EP2909144A1 (en) 2015-08-26
KR20150074085A (ko) 2015-07-01
BR112015008391A2 (pt) 2017-08-08
SG11201503017XA (en) 2015-05-28
MX357216B (es) 2018-06-29
ZA201503392B (en) 2019-12-18
JP2015536291A (ja) 2015-12-21
BR112015008391B1 (pt) 2022-03-29
US20150284255A1 (en) 2015-10-08
MY181782A (en) 2021-01-06
WO2014060260A1 (en) 2014-04-24
ES2697129T3 (es) 2019-01-22
US10000387B2 (en) 2018-06-19
EP2909144B1 (en) 2018-08-15
JP6367812B2 (ja) 2018-08-01
CN104854031B (zh) 2018-04-06
RU2015118227A (ru) 2016-12-10
CN104854031A (zh) 2015-08-19
RU2637021C2 (ru) 2017-11-29
MX2015004946A (es) 2016-02-22
SG10201703183UA (en) 2017-06-29

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