CN104854031B - 沸石材料的后处理 - Google Patents

沸石材料的后处理 Download PDF

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Publication number
CN104854031B
CN104854031B CN201380062829.8A CN201380062829A CN104854031B CN 104854031 B CN104854031 B CN 104854031B CN 201380062829 A CN201380062829 A CN 201380062829A CN 104854031 B CN104854031 B CN 104854031B
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zeolitic material
acid
aqueous solution
zeolitic
range
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Chinese (zh)
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CN104854031A (zh
Inventor
S·毛雷尔
F·奥伊泽克瑞姆
安德烈-尼古拉·帕乌莱斯库
J·杨
U·穆勒
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/38—Base treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
CN201380062829.8A 2012-10-18 2013-10-09 沸石材料的后处理 Active CN104854031B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12189040 2012-10-18
EP12189040.4 2012-10-18
PCT/EP2013/071041 WO2014060260A1 (en) 2012-10-18 2013-10-09 Post-treatment of a zeolitic material

Publications (2)

Publication Number Publication Date
CN104854031A CN104854031A (zh) 2015-08-19
CN104854031B true CN104854031B (zh) 2018-04-06

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ID=47115431

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CN201380062829.8A Active CN104854031B (zh) 2012-10-18 2013-10-09 沸石材料的后处理

Country Status (13)

Country Link
US (1) US10000387B2 (https=)
EP (1) EP2909144B1 (https=)
JP (1) JP6367812B2 (https=)
KR (1) KR102179936B1 (https=)
CN (1) CN104854031B (https=)
BR (1) BR112015008391B1 (https=)
ES (1) ES2697129T3 (https=)
MX (1) MX357216B (https=)
MY (1) MY181782A (https=)
RU (1) RU2637021C2 (https=)
SG (2) SG11201503017XA (https=)
WO (1) WO2014060260A1 (https=)
ZA (1) ZA201503392B (https=)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016058541A1 (en) 2014-10-15 2016-04-21 Basf Se Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom
KR102558113B1 (ko) * 2015-02-12 2023-07-24 바스프 에스이 Bea 골격 구조를 갖는 탈알루미늄화된 제올라이트 물질의 제조 방법
JP6879680B2 (ja) * 2015-06-29 2021-06-02 日揮触媒化成株式会社 高シリカチャバザイト型ゼオライトの製造方法および高シリカチャバザイト型ゼオライト
JP6949842B2 (ja) * 2015-12-09 2021-10-13 ビーエーエスエフ コーポレーション Ｃｈａ型ゼオライト材料、並びにシクロアルキル−、及びエチルトリメチルアンモニウム化合物の組み合わせを用いるそれらの製造方法
RU2018131407A (ru) * 2016-02-03 2020-03-03 Басф Корпорейшн Шабазитный катализатор, совместно обмененный на медь и железо
US10995008B2 (en) * 2016-03-30 2021-05-04 Basf Se Process for the flash calcination of a zeolitic material
CN109195911B (zh) * 2016-05-23 2023-04-07 东曹株式会社 Cha型沸石和其制造方法
CN109153578A (zh) * 2016-06-07 2019-01-04 雪佛龙美国公司 高硅afx骨架型分子筛
BR112019006347A2 (pt) * 2016-09-30 2019-06-18 Johnson Matthey Plc métodos para produzir um zeólito de aluminossilicato, para armazenar nox, para reduzir seletivamente nox e para oxidar um componente de um gás de escape, catalisador, artigo catalisador, e, zeólito de aluminossilicato.
CN110402246A (zh) 2017-03-15 2019-11-01 巴斯夫欧洲公司 通过使羟基羧酸或酰胺与酸性BEA(H-β多晶型A)型沸石反应而制备环状二酯或环状二酰胺的方法
CN108946755B (zh) * 2017-05-22 2020-08-07 中国石油化工股份有限公司 无锗iwr沸石分子筛的合成方法
MY190284A (en) * 2017-10-11 2022-04-12 Tosoh Corp Metal-containing cha-type zeolite and method for producing the same
KR20200118129A (ko) * 2018-02-06 2020-10-14 바스프 에스이 Rth 골격 구조 유형을 갖는 제올라이트 물질의 제조 방법
FR3081347B1 (fr) * 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
WO2021052466A1 (en) * 2019-09-20 2021-03-25 Basf Se Synthesis and use of zeolitic material having the ith framework structure type
CN111252781B (zh) * 2020-02-05 2022-01-07 浙江大学 无有机模板剂晶种法合成高硅kfi沸石分子筛的方法
JP7514467B2 (ja) * 2020-05-12 2024-07-11 国立大学法人 東京大学 ゼオライトの製造方法、ゼオライト、触媒、及び吸着剤
US20240158245A1 (en) 2021-03-19 2024-05-16 Basf Se Process for the dealumination of zeolitic materials
JPWO2024204696A1 (https=) 2023-03-31 2024-10-03

Citations (4)

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Publication number Priority date Publication date Assignee Title
EP0394948A2 (en) * 1989-04-24 1990-10-31 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
EP0690024A2 (en) * 1994-06-30 1996-01-03 ARCO Chemical Technology, L.P. Dealumination of aluminosilicates
WO2004050548A2 (en) * 2002-11-27 2004-06-17 Pq Holding, Inc. High surface area zeolites and methods for preparation and use thereof
CN102421740A (zh) * 2009-05-14 2012-04-18 英国石油化学品有限公司 羰基化方法

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FR2445747A1 (fr) 1979-01-05 1980-08-01 Armines Procede de fabrication de pieces en silicium nitrure
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US5443812A (en) * 1989-04-24 1995-08-22 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
JP2826868B2 (ja) * 1989-04-24 1998-11-18 鐘紡株式会社 安定化された合成ゼオライト及びその製造法
JPH0596175A (ja) 1991-10-03 1993-04-20 Catalysts & Chem Ind Co Ltd 変性結晶性アルミノシリケートゼオライトの製造方法
CN1081086C (zh) 1993-09-30 2002-03-20 山阳石油化学株式会社 沸石系催化剂的部分脱铝方法
DE10061715A1 (de) * 2000-12-12 2002-06-13 Basf Ag Verfahren zur Herstellung von Homo- und Copolymeren des Isobutens
AU2002248274A1 (en) 2000-12-22 2002-07-30 California Institute Of Technology Synthesis of molecular sieves by hydrothermal treatment with acid
EP2025402A1 (en) 2007-07-31 2009-02-18 Total Petrochemicals Research Feluy Phosphorus modified molecular sieves, their use in conversion of organics to olefins
EP2174713A1 (en) 2008-10-13 2010-04-14 BP Chemicals Limited Dealumination process
JP5508744B2 (ja) * 2009-03-13 2014-06-04 出光興産株式会社 ベータゼオライトの製造方法及び水素化分解触媒の製造方法
EP2694437B1 (en) 2011-04-08 2020-10-21 Basf Se Process for producing acylation catalyst
WO2014060259A1 (en) 2012-10-18 2014-04-24 Basf Se Post-treatment of deboronated zeolite beta
RU2638851C2 (ru) 2012-10-18 2017-12-18 Басф Се Последующая обработка деборированного цеолита mww

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0394948A2 (en) * 1989-04-24 1990-10-31 Kanebo Ltd. Stabilized synthetic zeolite and a process for the preparation thereof
EP0690024A2 (en) * 1994-06-30 1996-01-03 ARCO Chemical Technology, L.P. Dealumination of aluminosilicates
WO2004050548A2 (en) * 2002-11-27 2004-06-17 Pq Holding, Inc. High surface area zeolites and methods for preparation and use thereof
CN102421740A (zh) * 2009-05-14 2012-04-18 英国石油化学品有限公司 羰基化方法

Also Published As

Publication number Publication date
MX357216B (es) 2018-06-29
ZA201503392B (en) 2019-12-18
KR20150074085A (ko) 2015-07-01
US10000387B2 (en) 2018-06-19
MX2015004946A (es) 2016-02-22
BR112015008391B1 (pt) 2022-03-29
SG10201703183UA (en) 2017-06-29
RU2015118227A (ru) 2016-12-10
BR112015008391A2 (pt) 2017-08-08
RU2637021C2 (ru) 2017-11-29
US20150284255A1 (en) 2015-10-08
JP2015536291A (ja) 2015-12-21
EP2909144A1 (en) 2015-08-26
MY181782A (en) 2021-01-06
CN104854031A (zh) 2015-08-19
EP2909144B1 (en) 2018-08-15
JP6367812B2 (ja) 2018-08-01
SG11201503017XA (en) 2015-05-28
WO2014060260A1 (en) 2014-04-24
KR102179936B1 (ko) 2020-11-17
ES2697129T3 (es) 2019-01-22

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