KR101930024B1 - 형광체 입자, 그 제조방법, 및 발광 다이오드 - Google Patents

형광체 입자, 그 제조방법, 및 발광 다이오드 Download PDF

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KR101930024B1
KR101930024B1 KR1020110144889A KR20110144889A KR101930024B1 KR 101930024 B1 KR101930024 B1 KR 101930024B1 KR 1020110144889 A KR1020110144889 A KR 1020110144889A KR 20110144889 A KR20110144889 A KR 20110144889A KR 101930024 B1 KR101930024 B1 KR 101930024B1
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particles
phosphor
particle size
average particle
plasma
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KR20120080130A (ko
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토시히코 츠카타니
카즈히로 와타야
야스시 타카이
타케히사 미노와
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신에쓰 가가꾸 고교 가부시끼가이샤
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/77Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
    • C09K11/7766Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals
    • C09K11/7774Aluminates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00Compounds of rare earth metals
    • C01F17/30Compounds containing rare earth metals and at least one element other than a rare earth metal, oxygen or hydrogen, e.g. La4S3Br6
    • C01F17/32Compounds containing rare earth metals and at least one element other than a rare earth metal, oxygen or hydrogen, e.g. La4S3Br6 oxide or hydroxide being the only anion, e.g. NaCeO2 or MgxCayEuO
    • C01F17/34Aluminates, e.g. YAlO3 or Y3-xGdxAl5O12
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10HINORGANIC LIGHT-EMITTING SEMICONDUCTOR DEVICES HAVING POTENTIAL BARRIERS
    • H10H20/00Individual inorganic light-emitting semiconductor devices having potential barriers, e.g. light-emitting diodes [LED]
    • H10H20/80Constructional details
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/50Solid solutions
    • C01P2002/52Solid solutions containing elements as dopants
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/80Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/84Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by UV- or VIS- data
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • C01P2004/32Spheres
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/50Agglomerated particles
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Luminescent Compositions (AREA)
  • Electroluminescent Light Sources (AREA)
  • Led Device Packages (AREA)
KR1020110144889A 2011-01-06 2011-12-28 형광체 입자, 그 제조방법, 및 발광 다이오드 Expired - Fee Related KR101930024B1 (ko)

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JP2011001132 2011-01-06
JPJP-P-2011-001132 2011-01-06

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KR20120080130A KR20120080130A (ko) 2012-07-16
KR101930024B1 true KR101930024B1 (ko) 2018-12-17

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US (1) US9617469B2 (enExample)
EP (1) EP2474589B1 (enExample)
JP (2) JP5041190B2 (enExample)
KR (1) KR101930024B1 (enExample)
CN (1) CN102627971B (enExample)
TW (1) TWI515284B (enExample)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9617469B2 (en) 2011-01-06 2017-04-11 Shin-Etsu Chemical Co., Ltd. Phosphor particles, making method, and light-emitting diode
US8865022B2 (en) * 2011-01-06 2014-10-21 Shin-Etsu Chemical Co., Ltd. Phosphor particles and making method
EP2607449B1 (en) * 2011-12-22 2014-04-02 Shin-Etsu Chemical Co., Ltd. Preparation of yttrium-cerium-aluminum garnet phosphor
JP2014019860A (ja) * 2012-07-24 2014-02-03 Shin Etsu Chem Co Ltd 蛍光体前駆体の製造方法、蛍光体の製造方法及び波長変換部品
CN103811637B (zh) * 2012-11-05 2018-01-30 晶元光电股份有限公司 波长转换材料及其应用
US20140175968A1 (en) * 2012-12-21 2014-06-26 Shin-Etsu Chemical Co., Ltd. Yttrium-cerium-aluminum garnet phosphor and light-emitting device
TW201428087A (zh) 2013-01-11 2014-07-16 kai-xiong Cai 發光裝置及其耐溫碳化物螢光材料
CN103937500B (zh) * 2013-01-22 2016-02-10 蔡凯雄 发光装置及其耐温碳化物荧光材料
JP2014177601A (ja) * 2013-03-15 2014-09-25 Toshiba Corp 黄色発光蛍光体およびそれを用いた発光装置
JP6261196B2 (ja) 2013-06-12 2018-01-17 信越化学工業株式会社 発光装置
CZ307024B6 (cs) * 2014-05-05 2017-11-22 Crytur, Spol.S R.O. Světelný zdroj
CN104253198B (zh) * 2014-09-18 2017-01-25 华中科技大学 一种荧光粉复合颗粒、其制备方法及应用
EP3444858A4 (en) * 2016-04-12 2019-03-20 Panasonic Intellectual Property Management Co., Ltd. Wavelength conversion element
CN106270523B (zh) * 2016-09-30 2018-02-13 中国人民大学 一种大面积超薄单晶及其快速生长方法和应用
JP6471727B2 (ja) * 2016-05-30 2019-02-20 日亜化学工業株式会社 希土類アルミニウム酸塩の組成を有する蛍光体及び発光装置
JP6428813B2 (ja) * 2017-03-13 2018-11-28 信越化学工業株式会社 発光装置
CN113416544B (zh) * 2021-06-29 2022-05-10 有研稀土新材料股份有限公司 一种石榴石结构荧光粉及包含该荧光粉的发光装置
CN117682856B (zh) * 2022-09-02 2025-07-04 松山湖材料实验室 闪烁陶瓷及其制备方法和应用

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005527692A (ja) * 2002-05-29 2005-09-15 オスラム オプト セミコンダクターズ ゲゼルシャフト ミット ベシュレンクテル ハフツング 蛍光体粉末、蛍光体粉末の製造方法及び蛍光体粉末を有する蛍光体ボディ
JP2012017454A (ja) 2010-06-09 2012-01-26 Shin-Etsu Chemical Co Ltd 蛍光粒子及び発光ダイオード並びにこれらを用いた照明装置及び液晶パネル用バックライト装置

Family Cites Families (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4479886A (en) 1983-08-08 1984-10-30 Gte Products Corporation Method of making cerium activated yttrium aluminate phosphor
JPH0745655B2 (ja) 1985-11-07 1995-05-17 化成オプトニクス株式会社 蛍光体の製造方法
EP0292616B1 (en) 1987-05-26 1992-05-20 Agfa-Gevaert N.V. X-ray conversion into light
JPH0662938B2 (ja) 1987-10-19 1994-08-17 日亜化学工業株式会社 螢光体の製造方法
JPH069956A (ja) 1991-12-27 1994-01-18 Fuji Photo Film Co Ltd 球形焼結蛍光体およびその製造法
JP3141634B2 (ja) 1993-08-03 2001-03-05 セイコーエプソン株式会社 半導体装置の製造方法及び樹脂封止用金型
US5644193A (en) 1993-12-17 1997-07-01 Kabushiki Kaisha Toshiba Phosphor, cathode-ray tube, fluorescent lamp and radiation intensifying screen
JPH09235547A (ja) 1995-12-28 1997-09-09 Kasei Optonix Co Ltd 希土類酸化物蛍光体及び希土類酸硫化物蛍光体の製造方法
US5851428A (en) 1996-03-15 1998-12-22 Kabushiki Kaisha Toshiba Phosphor and manufacturing method thereof
TW383508B (en) 1996-07-29 2000-03-01 Nichia Kagaku Kogyo Kk Light emitting device and display
JPH1036835A (ja) 1996-07-29 1998-02-10 Nichia Chem Ind Ltd フォトルミネセンス蛍光体
US6197218B1 (en) 1997-02-24 2001-03-06 Superior Micropowders Llc Photoluminescent phosphor powders, methods for making phosphor powders and devices incorporating same
JP3445473B2 (ja) 1997-07-25 2003-09-08 株式会社東芝 蛍光体及び蛍光膜
JP2002267800A (ja) 2001-03-14 2002-09-18 Fuji Photo Film Co Ltd 放射線像変換パネルの蛍光体層塗布液の調製方法、および放射線像変換パネルの製造方法
US7001537B2 (en) * 2001-04-27 2006-02-21 Kasei Optonix, Ltd. Phosphor and its production process
JP4663927B2 (ja) 2001-08-29 2011-04-06 信越化学工業株式会社 希土類含有酸化物部材
US7015640B2 (en) 2002-09-11 2006-03-21 General Electric Company Diffusion barrier coatings having graded compositions and devices incorporating the same
JP2004162057A (ja) 2002-10-25 2004-06-10 Mitsubishi Chemicals Corp 蛍光体
EP2497758B1 (en) 2003-01-20 2019-05-29 Ube Industries, Ltd. Ceramic composite material for optical conversion
FR2855169B1 (fr) 2003-05-23 2006-06-16 Rhodia Elect & Catalysis Composes precurseurs d'aluminates d'alcalino-terreux ou de terre rare, leur procede de preparation et leur utilisation comme precurseur de luminophore notamment
KR100526343B1 (ko) 2003-07-21 2005-11-08 엘지전자 주식회사 형광체 잉크 제조 방법
JP4128564B2 (ja) 2004-04-27 2008-07-30 松下電器産業株式会社 発光装置
EP2113549B1 (en) 2004-04-27 2011-12-28 Panasonic Corporation Phosphor composition and light-emitting device using the same
JP4645089B2 (ja) 2004-07-26 2011-03-09 日亜化学工業株式会社 発光装置および蛍光体
WO2006072849A2 (en) 2005-01-04 2006-07-13 Philips Intellectual Property & Standards Gmbh Wavelength conversion layers with embedded crystallites
US20060162497A1 (en) 2005-01-21 2006-07-27 Cabot Corporation Processes for forming nanoparticles in a flame spray system
WO2006093015A1 (ja) 2005-02-28 2006-09-08 Mitsubishi Chemical Corporation 蛍光体及びその製造方法並びにその応用
JP2007002086A (ja) 2005-06-23 2007-01-11 Ishihara Sangyo Kaisha Ltd 電子線励起赤色蛍光体の製造方法
EP1980606B1 (en) 2006-01-19 2017-09-06 Ube Industries, Ltd. Ceramic composite light converting member and light emitting device using the same
JP2008007390A (ja) 2006-05-29 2008-01-17 Tohoku Univ 複合金属化合物の製造方法
TWI357927B (en) 2006-11-20 2012-02-11 Denki Kagaku Kogyo Kk Fluorescent substance and manufacturing method the
KR20080075972A (ko) 2007-02-14 2008-08-20 신라대학교 산학협력단 와이에이지계 형광체 나노 분말의 제조 방법
US20100048378A1 (en) 2007-04-24 2010-02-25 Nanocerox, Inc. Sintered polycrystalline yttrium aluminum garnet and use thereof in optical devices
JP5347354B2 (ja) 2007-09-18 2013-11-20 日亜化学工業株式会社 蛍光物質成形体及びその製造方法、発光装置
US7959885B2 (en) 2008-02-15 2011-06-14 Nitto Denko Corporation Nanoparticle synthesis by solvothermal process
JP5675339B2 (ja) 2008-03-10 2015-02-25 株式会社東芝 固体シンチレータ、放射線検出器およびx線断層写真撮影装置
US8461535B2 (en) 2009-05-20 2013-06-11 Lawrence Livermore National Security, Llc Phase stable rare earth garnets
WO2011063028A1 (en) 2009-11-19 2011-05-26 Nitto Denko Corporation Method for producing nanoparticles
CN102782089B (zh) 2010-02-04 2015-07-22 日东电工株式会社 发光陶瓷层压制件及其制造方法
US9617469B2 (en) 2011-01-06 2017-04-11 Shin-Etsu Chemical Co., Ltd. Phosphor particles, making method, and light-emitting diode
US8865022B2 (en) 2011-01-06 2014-10-21 Shin-Etsu Chemical Co., Ltd. Phosphor particles and making method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005527692A (ja) * 2002-05-29 2005-09-15 オスラム オプト セミコンダクターズ ゲゼルシャフト ミット ベシュレンクテル ハフツング 蛍光体粉末、蛍光体粉末の製造方法及び蛍光体粉末を有する蛍光体ボディ
JP2012017454A (ja) 2010-06-09 2012-01-26 Shin-Etsu Chemical Co Ltd 蛍光粒子及び発光ダイオード並びにこれらを用いた照明装置及び液晶パネル用バックライト装置

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JP5041190B2 (ja) 2012-10-03
EP2474589B1 (en) 2016-10-12
JP2012153879A (ja) 2012-08-16
TW201243025A (en) 2012-11-01
CN102627971A (zh) 2012-08-08
CN102627971B (zh) 2016-04-13
US9617469B2 (en) 2017-04-11
TWI515284B (zh) 2016-01-01
EP2474589A3 (en) 2014-03-19
EP2474589A2 (en) 2012-07-11
JP2012153905A (ja) 2012-08-16
US20120175658A1 (en) 2012-07-12
JP5862447B2 (ja) 2016-02-16
KR20120080130A (ko) 2012-07-16

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