KR101724697B1 - 그래핀 산화물의 탈산소공정 - Google Patents
그래핀 산화물의 탈산소공정 Download PDFInfo
- Publication number
- KR101724697B1 KR101724697B1 KR1020100030054A KR20100030054A KR101724697B1 KR 101724697 B1 KR101724697 B1 KR 101724697B1 KR 1020100030054 A KR1020100030054 A KR 1020100030054A KR 20100030054 A KR20100030054 A KR 20100030054A KR 101724697 B1 KR101724697 B1 KR 101724697B1
- Authority
- KR
- South Korea
- Prior art keywords
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- graphene oxide
- thin film
- deoxygenation
- light
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 86
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 74
- 238000006392 deoxygenation reaction Methods 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 claims abstract description 34
- 239000010409 thin film Substances 0.000 claims description 19
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 18
- 229910052760 oxygen Inorganic materials 0.000 claims description 18
- 239000001301 oxygen Substances 0.000 claims description 18
- 238000006243 chemical reaction Methods 0.000 claims description 17
- 239000010408 film Substances 0.000 claims description 14
- 239000002270 dispersing agent Substances 0.000 claims description 12
- 239000003054 catalyst Substances 0.000 claims description 7
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 6
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 229910052749 magnesium Inorganic materials 0.000 claims description 5
- 239000011777 magnesium Substances 0.000 claims description 5
- 230000003197 catalytic effect Effects 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- 238000000354 decomposition reaction Methods 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
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- 238000010521 absorption reaction Methods 0.000 description 7
- 229910052799 carbon Inorganic materials 0.000 description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
- 238000001878 scanning electron micrograph Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
- 239000003638 chemical reducing agent Substances 0.000 description 4
- 239000002109 single walled nanotube Substances 0.000 description 4
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- 229910003481 amorphous carbon Inorganic materials 0.000 description 3
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
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- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- 229910052724 xenon Inorganic materials 0.000 description 2
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 235000015842 Hesperis Nutrition 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 235000012633 Iberis amara Nutrition 0.000 description 1
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- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 229910001507 metal halide Inorganic materials 0.000 description 1
- 150000005309 metal halides Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
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- 229910052754 neon Inorganic materials 0.000 description 1
- GKAOGPIIYCISHV-UHFFFAOYSA-N neon atom Chemical compound [Ne] GKAOGPIIYCISHV-UHFFFAOYSA-N 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
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- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical compound C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 238000010895 photoacoustic effect Methods 0.000 description 1
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- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
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Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
- C01B32/19—Preparation by exfoliation
- C01B32/192—Preparation by exfoliation starting from graphitic oxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/04—Specific amount of layers or specific thickness
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/20—Graphene characterized by its properties
- C01B2204/22—Electronic properties
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/20—Graphene characterized by its properties
- C01B2204/30—Purity
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/20—Graphene characterized by its properties
- C01B2204/32—Size or surface area
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Physics & Mathematics (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Composite Materials (AREA)
- Carbon And Carbon Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/386,303 | 2009-04-16 | ||
| US12/386,303 US8317984B2 (en) | 2009-04-16 | 2009-04-16 | Graphene oxide deoxygenation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20100114827A KR20100114827A (ko) | 2010-10-26 |
| KR101724697B1 true KR101724697B1 (ko) | 2017-04-07 |
Family
ID=42751173
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020100030054A Active KR101724697B1 (ko) | 2009-04-16 | 2010-04-01 | 그래핀 산화물의 탈산소공정 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US8317984B2 (enExample) |
| JP (1) | JP5555035B2 (enExample) |
| KR (1) | KR101724697B1 (enExample) |
| DE (1) | DE102010002124B4 (enExample) |
| TW (1) | TWI511922B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20190083550A (ko) | 2018-01-04 | 2019-07-12 | 한국전기연구원 | 광소결을 통해 질소가 도핑된 산화그래핀 환원물 및 그 제조방법 |
Families Citing this family (79)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8968525B2 (en) * | 2009-02-27 | 2015-03-03 | Northwestern University | Methods of flash reduction and patterning of graphite oxide and its polymer composites |
| US9162896B2 (en) * | 2009-05-31 | 2015-10-20 | College Of William And Mary | Method for making polymer composites containing graphene sheets |
| JP2013500922A (ja) | 2009-07-31 | 2013-01-10 | マサチューセッツ インスティテュート オブ テクノロジー | 炭素系ナノ構造の形成に関するシステムおよび方法 |
| EP2504278A2 (en) * | 2009-11-25 | 2012-10-03 | Massachusetts Institute of Technology | Systems and methods for enhancing growth of carbon-based nanostructures |
| US9768355B2 (en) * | 2009-12-10 | 2017-09-19 | Virginia Commonwealth University | Production of graphene and nanoparticle catalysts supported on graphene using laser radiation |
| KR101180176B1 (ko) | 2010-10-26 | 2012-09-05 | 주식회사 엘지실트론 | 화합물 반도체 장치 및 그 제조 방법 |
| US9663368B2 (en) | 2010-10-28 | 2017-05-30 | Massachusetts Institute Of Technology | Carbon-based nanostructure formation using large scale active growth structures |
| WO2012057702A1 (en) * | 2010-10-28 | 2012-05-03 | Nanyang Technological University | Method of preparing a porous graphene film |
| KR102650871B1 (ko) | 2011-06-03 | 2024-03-26 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 전극을 제조하기 위한 방법 |
| US9218916B2 (en) | 2011-06-24 | 2015-12-22 | Semiconductor Energy Laboratory Co., Ltd. | Graphene, power storage device, and electric device |
| US9249524B2 (en) | 2011-08-31 | 2016-02-02 | Semiconductor Energy Laboratory Co., Ltd. | Manufacturing method of composite oxide and manufacturing method of power storage device |
| US8828193B2 (en) | 2011-09-06 | 2014-09-09 | Indian Institute Of Technology Madras | Production of graphene using electromagnetic radiation |
| KR102514830B1 (ko) | 2011-09-30 | 2023-03-30 | 가부시키가이샤 한도오따이 에네루기 켄큐쇼 | 양극, 리튬 이차 전지, 전기 자동차, 하이브리드 자동차, 이동체, 시스템, 및 전기 기기 |
| CN103035922B (zh) | 2011-10-07 | 2019-02-19 | 株式会社半导体能源研究所 | 蓄电装置 |
| US9487880B2 (en) | 2011-11-25 | 2016-11-08 | Semiconductor Energy Laboratory Co., Ltd. | Flexible substrate processing apparatus |
| CN102615290B (zh) * | 2011-12-12 | 2016-04-06 | 湖南理工学院 | 一种Ag/石墨烯纳米复合材料的制备方法 |
| JP6016597B2 (ja) | 2011-12-16 | 2016-10-26 | 株式会社半導体エネルギー研究所 | リチウムイオン二次電池用正極の製造方法 |
| US20160077074A1 (en) * | 2011-12-21 | 2016-03-17 | The Regents Of The University Of California | Interconnected corrugated carbon-based network |
| US20140239236A1 (en) * | 2012-01-18 | 2014-08-28 | Deepak Shukla | Method for reducing graphite oxide |
| US20130180842A1 (en) * | 2012-01-18 | 2013-07-18 | Thomas Nelson Blanton | Method for reducing graphite oxide |
| JP5806618B2 (ja) * | 2012-01-26 | 2015-11-10 | Dowaエレクトロニクス株式会社 | 酸化グラフェンの還元方法およびその方法を利用した電極材料の製造方法 |
| JP5719859B2 (ja) | 2012-02-29 | 2015-05-20 | 株式会社半導体エネルギー研究所 | 蓄電装置 |
| CN109524246B (zh) | 2012-03-05 | 2021-07-27 | 加州大学评议会 | 具有由互连波纹状碳基网络制成的电极的电容器 |
| US9059466B2 (en) | 2012-03-22 | 2015-06-16 | Chun-Chieh Chang | Direct synthesis of lithium ion battery electrode materials using graphene treated raw materials as the reactant |
| US9090476B2 (en) | 2012-03-22 | 2015-07-28 | Chun-Chieh Chang | Direct deposition of graphene on substrate material |
| US9422165B2 (en) * | 2012-04-27 | 2016-08-23 | Empire Technology Development Llc | Graphene compositions and methods of making the same |
| US9527043B2 (en) | 2012-05-17 | 2016-12-27 | Samsung Electronics Co., Ltd. | Gas separation membrane and method of preparing the same |
| KR101920716B1 (ko) | 2012-05-17 | 2019-02-13 | 삼성전자주식회사 | 기체 분리막 및 그 제조방법 |
| US9236633B2 (en) | 2012-06-12 | 2016-01-12 | Uwm Research Foundation, Inc. | Synthesis and applications of graphene based nanomaterials |
| US9225003B2 (en) | 2012-06-15 | 2015-12-29 | Semiconductor Energy Laboratory Co., Ltd. | Method for manufacturing storage battery electrode, storage battery electrode, storage battery, and electronic device |
| US20140050910A1 (en) * | 2012-08-15 | 2014-02-20 | Rensselaer Polytechnic Institute | Rapid macro-scale synthesis of free-standing graphene, high performance, binder-free graphene anode material, and methods of synthesizing the anode material |
| JP6159228B2 (ja) | 2012-11-07 | 2017-07-05 | 株式会社半導体エネルギー研究所 | 非水系二次電池用正極の製造方法 |
| CN102963886A (zh) * | 2012-11-28 | 2013-03-13 | 同济大学 | 一种多孔状氧化石墨烯的制备方法 |
| JP6074270B2 (ja) * | 2013-01-15 | 2017-02-01 | 東京エレクトロン株式会社 | グラフェンのパターニング方法、及びパターンニング用部材 |
| US9284195B2 (en) * | 2013-01-30 | 2016-03-15 | Research & Business Foundation Sungkyunkwan University | Aggregated graphene oxide and preparing method thereof, aggregated graphene and preparing method thereof, and aggregated and nitrogen-doped graphene and preparing method thereof |
| KR20140100619A (ko) * | 2013-02-05 | 2014-08-18 | 도시바삼성스토리지테크놀러지코리아 주식회사 | 복수의 광원을 사용한 그래핀 제조장치 |
| KR20140100146A (ko) * | 2013-02-05 | 2014-08-14 | 도시바삼성스토리지테크놀러지코리아 주식회사 | 복수의 광원을 사용한 그래핀 제조방법 |
| US9673454B2 (en) | 2013-02-18 | 2017-06-06 | Semiconductor Energy Laboratory Co., Ltd. | Sodium-ion secondary battery |
| JP6373284B2 (ja) | 2013-02-28 | 2018-08-15 | エヌ12 テクノロジーズ, インク.N12 Technologies, Inc. | ナノ構造フィルムのカートリッジベース払い出し |
| KR101447680B1 (ko) * | 2013-03-08 | 2014-10-08 | 한국과학기술연구원 | 전극의 제조 방법, 상기 제조 방법에 따라 제조된 전극, 상기 전극을 포함하는 슈퍼 커패시터 및 리튬 이차 전지 |
| KR20140115198A (ko) * | 2013-03-20 | 2014-09-30 | 한국과학기술연구원 | 산화그래핀의 환원 방법, 상기 방법으로 얻어진 환원 산화그래핀 및 상기 환원 산화그래핀을 포함하는 박막 트랜지스터 |
| US9490472B2 (en) * | 2013-03-28 | 2016-11-08 | Semiconductor Energy Laboratory Co., Ltd. | Method for manufacturing electrode for storage battery |
| JP6214028B2 (ja) * | 2013-04-05 | 2017-10-18 | 国立大学法人北海道大学 | 酸化グラフェン含有液の製造方法及びその利用 |
| CN104211047B (zh) * | 2013-05-30 | 2017-02-08 | 纳米新能源(唐山)有限责任公司 | 石墨烯、石墨烯电极、石墨烯超级电容器及其制备方法 |
| US9908780B2 (en) | 2013-10-31 | 2018-03-06 | East China University Of Science And Technology | Methods and systems for preparing graphene |
| JP2016013958A (ja) | 2013-12-02 | 2016-01-28 | 株式会社半導体エネルギー研究所 | 素子、膜の作製方法 |
| WO2015089272A2 (en) * | 2013-12-12 | 2015-06-18 | Rensselaer Polytechnic Institute | Porous graphene network electrodes and an all-carbon lithium ion battery containing the same |
| JP6200094B2 (ja) * | 2013-12-17 | 2017-09-20 | ノキア テクノロジーズ オサケユイチア | 酸化グラフェンをパターニングする方法及び装置 |
| JP6688225B2 (ja) * | 2014-04-04 | 2020-04-28 | シグニファイ ホールディング ビー ヴィSignify Holding B.V. | グラフェン層の製造方法 |
| CN103964424A (zh) * | 2014-05-13 | 2014-08-06 | 桂林理工大学 | 一种光照还原氧化石墨烯薄膜的制备方法 |
| JP6745587B2 (ja) | 2014-05-29 | 2020-08-26 | 株式会社半導体エネルギー研究所 | 電極の製造方法 |
| US9099376B1 (en) | 2014-06-06 | 2015-08-04 | Nano And Advanced Materials Institute Limited | Laser direct patterning of reduced-graphene oxide transparent circuit |
| MX378624B (es) | 2014-06-16 | 2025-03-10 | Univ California | Celda electroquimica hibrida. |
| CN104810163B (zh) * | 2014-07-18 | 2017-08-08 | 纳米新能源(唐山)有限责任公司 | 石墨烯超级电容器的制备方法、石墨烯超级电容器及储能系统 |
| US20160099116A1 (en) * | 2014-10-05 | 2016-04-07 | Yongzhi Yang | Methods and apparatus for the production of capacitor with electrodes made of interconnected corrugated carbon-based network |
| CN104370282A (zh) * | 2014-10-21 | 2015-02-25 | 桂林理工大学 | 一种简易制备n型石墨烯场效应管的方法 |
| US9593663B2 (en) * | 2014-10-31 | 2017-03-14 | The United States Of America As Represented By The Secretary Of The Air Force | Photo-ignition torch for combustion initiation and gas generation |
| JP6378059B2 (ja) * | 2014-11-18 | 2018-08-22 | 国立研究開発法人物質・材料研究機構 | グラフェン酸化物発泡体、グラフェン酸化物/カーボンナノチューブ複合体発泡体、グラフェン・エアロゲル又はグラフェン/カーボンナノチューブ複合体エアロゲルの製造方法 |
| BR112017010257B8 (pt) | 2014-11-18 | 2023-10-31 | Univ California | Compósito de rede à base de carbono corrugado interligado poroso (iccn), e, método para produzir o compósito |
| CN104910536A (zh) * | 2015-05-07 | 2015-09-16 | 深圳市华星光电技术有限公司 | 石墨烯基树脂球的制备方法与导电框胶的制备方法 |
| JP2016222526A (ja) | 2015-05-29 | 2016-12-28 | 株式会社半導体エネルギー研究所 | 膜の作製方法および素子 |
| KR101797145B1 (ko) | 2015-11-03 | 2017-11-13 | 성균관대학교산학협력단 | 환원된 산화그래핀의 제조방법 |
| PL229151B1 (pl) * | 2015-11-16 | 2018-06-29 | Inst Niskich Temperatur I Badan Strukturalnych Im Wlodzimierza Trzebiatowskiego Polskiej Akademii Na | Źródło światła białego i sposób generowania światła białego |
| US10655020B2 (en) | 2015-12-22 | 2020-05-19 | The Regents Of The University Of California | Cellular graphene films |
| AU2017209117B2 (en) | 2016-01-22 | 2021-10-21 | The Regents Of The University Of California | High-voltage devices |
| CN109074966A (zh) | 2016-03-23 | 2018-12-21 | 加利福尼亚大学董事会 | 用于高电压和太阳能应用的装置和方法 |
| KR102378286B1 (ko) | 2016-04-01 | 2022-03-23 | 더 리전트 오브 더 유니버시티 오브 캘리포니아 | 가요성이고 고성능인 슈퍼커패시터를 위한 탄소 클로쓰 상에서의 폴리아닐린 나노튜브의 직접 성장 |
| US10876210B1 (en) * | 2016-05-05 | 2020-12-29 | Iowa State University Research Foundation, Inc. | Tunable nano-structured inkjet printed graphene via UV pulsed-laser irradiation for electrochemical sensing |
| CN105776200B (zh) * | 2016-05-20 | 2017-09-05 | 西北有色金属研究院 | 一种光催化还原连续制备石墨烯的装置及方法 |
| US11097951B2 (en) | 2016-06-24 | 2021-08-24 | The Regents Of The University Of California | Production of carbon-based oxide and reduced carbon-based oxide on a large scale |
| US20190224628A1 (en) * | 2016-08-30 | 2019-07-25 | Swinburne University Of Technology | Porous Graphene-Based Films And Processes For Preparing The Films |
| WO2018044786A1 (en) | 2016-08-31 | 2018-03-08 | The Regents Of The University Of California | Devices comprising carbon-based material and fabrication thereof |
| AU2018301683B2 (en) | 2017-07-14 | 2024-04-04 | The Regents Of The University Of California | Simple route to highly conductive porous graphene from carbon nanodots for supercapacitor applications |
| KR102080501B1 (ko) | 2018-06-04 | 2020-02-24 | 세종대학교 산학협력단 | 강자성 그래핀 및 이의 제조방법 |
| US10941041B2 (en) * | 2018-07-06 | 2021-03-09 | Savannah River Nuclear Solutions, Llc | Method of manufacturing graphene using photoreduction |
| TWI676793B (zh) * | 2018-09-05 | 2019-11-11 | 國立清華大學 | 具有雙功能性電極對與紫外激活三元奈米複合材料之可攜式氣體感測裝置 |
| US10938032B1 (en) | 2019-09-27 | 2021-03-02 | The Regents Of The University Of California | Composite graphene energy storage methods, devices, and systems |
| KR102338321B1 (ko) * | 2020-07-10 | 2021-12-10 | 연세대학교 산학협력단 | 그래핀 박막의 연속 제조방법 |
| CZ309452B6 (cs) * | 2021-05-05 | 2023-01-25 | Masarykova Univerzita | Způsob spuštění samovolně se šířícího procesu redukce-exfoliace oxidu grafenu v porézním materiálu |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010001703A1 (en) | 1996-03-07 | 2001-05-24 | Makoto Takahashi | Method for the formation of resist patterns |
| JP2002356317A (ja) | 2001-03-27 | 2002-12-13 | Osaka Gas Co Ltd | グラファイトリボンおよびその製造方法 |
| US20060121613A1 (en) | 2004-12-03 | 2006-06-08 | Havens Marvin R | Process for detecting leaks in sealed packages |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2798878A (en) | 1954-07-19 | 1957-07-09 | Nat Lead Co | Preparation of graphitic acid |
| JP4109952B2 (ja) | 2001-10-04 | 2008-07-02 | キヤノン株式会社 | ナノカーボン材料の製造方法 |
| JP4483152B2 (ja) | 2001-11-27 | 2010-06-16 | 富士ゼロックス株式会社 | 中空グラフェンシート構造体及び電極構造体とそれら製造方法並びにデバイス |
| JP2003231097A (ja) * | 2002-02-08 | 2003-08-19 | Mitsubishi Gas Chem Co Inc | 炭素からなる骨格を持つ薄膜状粒子を基板に載せた構造物およびその作製方法 |
| AU2003215253A1 (en) | 2002-02-19 | 2003-09-09 | Rensselaer Polytechnic Institute | Method of transforming carbon nanotubes |
| US7105108B2 (en) | 2002-08-15 | 2006-09-12 | Advanced Energy Technology Inc. | Graphite intercalation and exfoliation process |
| US7071258B1 (en) | 2002-10-21 | 2006-07-04 | Nanotek Instruments, Inc. | Nano-scaled graphene plates |
| US7381352B2 (en) | 2003-07-23 | 2008-06-03 | Mitsubishi Gas Chemical Company, Inc. | Dispersion of thin particles having a skeleton consisting of carbons |
| US7517215B1 (en) | 2004-07-09 | 2009-04-14 | Erc Incorporated | Method for distributed ignition of fuels by light sources |
| US7842271B2 (en) | 2004-12-07 | 2010-11-30 | Petrik Viktor I | Mass production of carbon nanostructures |
| JP3720044B1 (ja) | 2005-03-22 | 2005-11-24 | 株式会社物産ナノテク研究所 | 複合材料 |
| US7892514B2 (en) | 2007-02-22 | 2011-02-22 | Nanotek Instruments, Inc. | Method of producing nano-scaled graphene and inorganic platelets and their nanocomposites |
| FR2919856B1 (fr) * | 2007-08-09 | 2010-03-12 | Centre Nat Rech Scient | Solutions de graphene |
| JP2009062241A (ja) * | 2007-09-07 | 2009-03-26 | Hokkaido Univ | グラフェンシートの製造方法 |
| CN101990518A (zh) * | 2008-02-05 | 2011-03-23 | 普林斯顿大学理事会 | 包含官能化的石墨烯片的涂料以及用其涂覆的物品 |
| US8173095B2 (en) * | 2008-03-18 | 2012-05-08 | Georgia Tech Research Corporation | Method and apparatus for producing graphene oxide layers on an insulating substrate |
| US8871821B2 (en) * | 2008-12-04 | 2014-10-28 | Tyco Electronics Corporation | Graphene and graphene oxide aerogels |
-
2009
- 2009-04-16 US US12/386,303 patent/US8317984B2/en active Active
-
2010
- 2010-01-22 TW TW099101811A patent/TWI511922B/zh active
- 2010-02-18 DE DE102010002124.5A patent/DE102010002124B4/de active Active
- 2010-04-01 KR KR1020100030054A patent/KR101724697B1/ko active Active
- 2010-04-13 JP JP2010091959A patent/JP5555035B2/ja active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010001703A1 (en) | 1996-03-07 | 2001-05-24 | Makoto Takahashi | Method for the formation of resist patterns |
| JP2002356317A (ja) | 2001-03-27 | 2002-12-13 | Osaka Gas Co Ltd | グラファイトリボンおよびその製造方法 |
| US20060121613A1 (en) | 2004-12-03 | 2006-06-08 | Havens Marvin R | Process for detecting leaks in sealed packages |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20190083550A (ko) | 2018-01-04 | 2019-07-12 | 한국전기연구원 | 광소결을 통해 질소가 도핑된 산화그래핀 환원물 및 그 제조방법 |
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| JP5555035B2 (ja) | 2014-07-23 |
| TW201038474A (en) | 2010-11-01 |
| US8317984B2 (en) | 2012-11-27 |
| JP2010248066A (ja) | 2010-11-04 |
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