KR100893688B1 - 에틸렌디아민 염 재순환에 의한 n-[2-아미노 에틸]아미노알킬알콕시실란 제조방법 - Google Patents

에틸렌디아민 염 재순환에 의한 n-[2-아미노 에틸]아미노알킬알콕시실란 제조방법 Download PDF

Info

Publication number
KR100893688B1
KR100893688B1 KR1020047012330A KR20047012330A KR100893688B1 KR 100893688 B1 KR100893688 B1 KR 100893688B1 KR 1020047012330 A KR1020047012330 A KR 1020047012330A KR 20047012330 A KR20047012330 A KR 20047012330A KR 100893688 B1 KR100893688 B1 KR 100893688B1
Authority
KR
South Korea
Prior art keywords
ethylenediamine
phase
reactor
salt
aminoalkylalkoxysilane
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1020047012330A
Other languages
English (en)
Korean (ko)
Other versions
KR20040097125A (ko
Inventor
웰리엄 씨. 마키
호워드 뱅크
스티븐 에이치. 와이어
브라이언 씨. 맥도날드
Original Assignee
다우 코닝 코포레이션
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 다우 코닝 코포레이션 filed Critical 다우 코닝 코포레이션
Publication of KR20040097125A publication Critical patent/KR20040097125A/ko
Application granted granted Critical
Publication of KR100893688B1 publication Critical patent/KR100893688B1/ko
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/18Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/18Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
    • C07F7/1804Compounds having Si-O-C linkages
    • C07F7/1872Preparation; Treatments not provided for in C07F7/20
    • C07F7/1892Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020047012330A 2002-02-11 2003-01-16 에틸렌디아민 염 재순환에 의한 n-[2-아미노 에틸]아미노알킬알콕시실란 제조방법 Expired - Fee Related KR100893688B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/073,444 2002-02-11
US10/073,444 US6452033B1 (en) 2002-02-11 2002-02-11 Method of making N-[2-aminoethyl] aminoalkylalkoxysilanes with ethyenediamine salt recycle
PCT/US2003/001296 WO2003068780A1 (en) 2002-02-11 2003-01-16 Method of making n- [2-aminoethyl] aminoalkylalkoxysilanes with ethylene diamine salt recycle

Publications (2)

Publication Number Publication Date
KR20040097125A KR20040097125A (ko) 2004-11-17
KR100893688B1 true KR100893688B1 (ko) 2009-04-17

Family

ID=22113713

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020047012330A Expired - Fee Related KR100893688B1 (ko) 2002-02-11 2003-01-16 에틸렌디아민 염 재순환에 의한 n-[2-아미노 에틸]아미노알킬알콕시실란 제조방법

Country Status (9)

Country Link
US (1) US6452033B1 (enExample)
EP (1) EP1476450B1 (enExample)
JP (1) JP4309287B2 (enExample)
KR (1) KR100893688B1 (enExample)
CN (1) CN1267440C (enExample)
AT (1) ATE459629T1 (enExample)
AU (1) AU2003207577A1 (enExample)
DE (1) DE60331526D1 (enExample)
WO (1) WO2003068780A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100413555C (zh) * 2003-02-10 2008-08-27 严晓东 含β-氨乙基-γ-氨丙基基团的有机硅烷偶联剂的生产废料的回收处理方法
DE102007037193A1 (de) * 2007-08-07 2009-02-12 Wacker Chemie Ag Verfahren zur Herstellung von Aminoorganosilanen
DE102009000500A1 (de) * 2009-01-30 2010-08-05 Wacker Chemie Ag Verfahren zur Herstellung von Bis- und Tris(silylorgano)aminen
DE102009026755A1 (de) 2009-06-04 2010-12-09 Wacker Chemie Ag Verfahren zur Herstellung von Aminoorganosilanen
DE102015225879A1 (de) 2015-12-18 2017-06-22 Evonik Degussa Gmbh Tris-(alkylalkoxysilyl)amin-reiche Zusammensetzungen, deren Herstellung und deren Verwendung
DE102015225883A1 (de) 2015-12-18 2017-06-22 Evonik Degussa Gmbh Bis(alkylalkoxysilyl)amin-reiche Zusammensetzungen, ein Verfahren zur deren Herstellung und deren Verwendung
DE102016215260A1 (de) 2016-08-16 2018-02-22 Evonik Degussa Gmbh Verwendung einer (Alkylalkoxysily)amin-, Bis-(alkylalkoxysilyl)amin und/oder Tris-(alkylalkoxysilyl)amin-enthaltenden Zusammensetzung
WO2018033199A1 (de) 2016-08-16 2018-02-22 Wacker Chemie Ag Verfahren zur herstellung von sekundären aminoorganosiliciumverbindungen
JP7077966B2 (ja) * 2019-01-07 2022-05-31 信越化学工業株式会社 アミノ基含有有機ケイ素化合物の製造方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4546996A (en) 1984-06-18 1985-10-15 J. I. Case Company Multi-surface stabilizer pad assembly
US5446181A (en) 1992-10-26 1995-08-29 Shin-Etsu Chemical Co., Ltd. Method and apparatus for preparing 3-[N-(2-aminoethyl)]aminopropylalkoxysilane

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB889001A (en) 1959-07-17 1962-02-07 Midland Silicones Ltd Aminated organosilicon compounds
US3146250A (en) 1961-10-11 1964-08-25 Dow Corning Nitrogen-containing cyclic silanes, their preparation and hydrolysis
US4064155A (en) * 1975-12-22 1977-12-20 Dow Corning Corporation Preparation of silylamine hydrochlorides
JPS56104891A (en) 1980-01-28 1981-08-20 Toray Ind Inc Preparation of (n-aminoethyl)aminoalkylsilane
US4448694A (en) * 1981-09-04 1984-05-15 Dow Corning Corporation Metal extraction from solution and immobilized chelating agents used therefor
US4526996A (en) * 1984-06-19 1985-07-02 Union Carbide Corporation Process for the preparation of N-substituted aminoalkylsilanes
JPH053177A (ja) * 1991-06-25 1993-01-08 Sony Corp ドライエツチング方法
JP2687787B2 (ja) * 1991-10-02 1997-12-08 ソニー株式会社 ドライエッチング方法
JP3761918B2 (ja) * 1994-09-13 2006-03-29 株式会社東芝 半導体装置の製造方法
EP0702017B1 (de) * 1994-09-14 2001-11-14 Degussa AG Verfahren zur Herstellung von chloridarmen bzw. chloridfreien aminofunktionellen Organosilanen
JP2842284B2 (ja) * 1995-02-14 1998-12-24 日本電気株式会社 半導体装置の製造方法
US6165910A (en) * 1997-12-29 2000-12-26 Lam Research Corporation Self-aligned contacts for semiconductor device

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4546996A (en) 1984-06-18 1985-10-15 J. I. Case Company Multi-surface stabilizer pad assembly
US5446181A (en) 1992-10-26 1995-08-29 Shin-Etsu Chemical Co., Ltd. Method and apparatus for preparing 3-[N-(2-aminoethyl)]aminopropylalkoxysilane

Also Published As

Publication number Publication date
US6452033B1 (en) 2002-09-17
JP2005517707A (ja) 2005-06-16
WO2003068780A1 (en) 2003-08-21
CN1630660A (zh) 2005-06-22
AU2003207577A1 (en) 2003-09-04
ATE459629T1 (de) 2010-03-15
JP4309287B2 (ja) 2009-08-05
EP1476450B1 (en) 2010-03-03
CN1267440C (zh) 2006-08-02
EP1476450A1 (en) 2004-11-17
KR20040097125A (ko) 2004-11-17
DE60331526D1 (de) 2010-04-15
EP1476450A4 (en) 2008-02-13

Similar Documents

Publication Publication Date Title
KR100893688B1 (ko) 에틸렌디아민 염 재순환에 의한 n-[2-아미노 에틸]아미노알킬알콕시실란 제조방법
JP5049204B2 (ja) SiHを有するシランの製造方法
US4380660A (en) Producing alkoxysilanes and alkoxy-oximinosilanes
US7208617B2 (en) Hydrolysis of chlorosilanes
US3983148A (en) Process for producing cyclic siloxanes
JP4934096B2 (ja) 再循環された塩化水素を用いたクロロメタンの製造方法
US20120165564A1 (en) Method for preparing purified aminosilane
KR101208324B1 (ko) 클로로실란의 반응성 증류
US8314263B2 (en) Method for producing amino-organosilanes
JPS64956B2 (enExample)
CN100516075C (zh) 制造带有氨基的硅化合物的方法
WO2021138148A2 (en) Cationic surfactant and method of preparing same
US4401826A (en) Method for production of mercapto functional silanes
US5939575A (en) Process for the continuous preparation of acyloxysilanes
KR100573784B1 (ko) 고순도 알킬알콕시실란의 제조방법
US4855473A (en) Process for the preparation of organooxychlorosilanes
KR20070084166A (ko) 실릴알콕시메틸 할라이드의 제조방법
KR100521614B1 (ko) 3-[n-(2-아미노에틸)]아미노프로필알콕시실란의 제조방법
KR100634025B1 (ko) 아미노알콕시실란의 제조방법
JP2003226693A (ja) アルキルアミンの連続製法
JPS5931782A (ja) ハロシラン類を同時アルコキシル化し得られる生成物を分離する方法
CA3162997C (en) Cationic surfactant and method of preparing same
JPS6253516B2 (enExample)
CN118320750A (zh) 一种三甲基硅基二烷基胺的合成装置系统及制备方法
JPS63270693A (ja) 環状シロキサンの製造方法

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

T11-X000 Administrative time limit extension requested

St.27 status event code: U-3-3-T10-T11-oth-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

FPAY Annual fee payment

Payment date: 20130321

Year of fee payment: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

FPAY Annual fee payment

Payment date: 20140320

Year of fee payment: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

LAPS Lapse due to unpaid annual fee
PC1903 Unpaid annual fee

St.27 status event code: A-4-4-U10-U13-oth-PC1903

Not in force date: 20150410

Payment event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

PC1903 Unpaid annual fee

St.27 status event code: N-4-6-H10-H13-oth-PC1903

Ip right cessation event data comment text: Termination Category : DEFAULT_OF_REGISTRATION_FEE

Not in force date: 20150410

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

R18 Changes to party contact information recorded

Free format text: ST27 STATUS EVENT CODE: A-5-5-R10-R18-OTH-X000 (AS PROVIDED BY THE NATIONAL OFFICE)

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000