KR100809167B1 - 유기 모노 또는 폴리이소시아네이트의 연속 제조 방법 및장치 - Google Patents

유기 모노 또는 폴리이소시아네이트의 연속 제조 방법 및장치 Download PDF

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Publication number
KR100809167B1
KR100809167B1 KR1020027015867A KR20027015867A KR100809167B1 KR 100809167 B1 KR100809167 B1 KR 100809167B1 KR 1020027015867 A KR1020027015867 A KR 1020027015867A KR 20027015867 A KR20027015867 A KR 20027015867A KR 100809167 B1 KR100809167 B1 KR 100809167B1
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South Korea
Prior art keywords
starting material
annular gap
phosgene
stream
mixing
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Expired - Fee Related
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KR1020027015867A
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English (en)
Korean (ko)
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KR20030022132A (ko
Inventor
안드레아스 뵐페르트
울리히 펜젤
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바스프 악티엔게젤샤프트
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2405—Stationary reactors without moving elements inside provoking a turbulent flow of the reactants, such as in cyclones, or having a high Reynolds-number
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20—Jet mixers, i.e. mixers using high-speed fluid streams
    • B01F25/23—Mixing by intersecting jets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/244—Concentric tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91—Direction of flow or arrangement of feed and discharge openings
    • B01F2025/915—Reverse flow, i.e. flow changing substantially 180° in direction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Accessories For Mixers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
KR1020027015867A 2000-05-26 2001-05-21 유기 모노 또는 폴리이소시아네이트의 연속 제조 방법 및장치 Expired - Fee Related KR100809167B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10026142A DE10026142A1 (de) 2000-05-26 2000-05-26 Verfahren und Vorrichtung zur kontinuierlichen Herstellung von organischen Mono- oder Polyisocyanaten
DE10026142.6 2000-05-26

Publications (2)

Publication Number Publication Date
KR20030022132A KR20030022132A (ko) 2003-03-15
KR100809167B1 true KR100809167B1 (ko) 2008-02-29

Family

ID=7643675

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020027015867A Expired - Fee Related KR100809167B1 (ko) 2000-05-26 2001-05-21 유기 모노 또는 폴리이소시아네이트의 연속 제조 방법 및장치

Country Status (12)

Country Link
US (1) US6867324B2 (https=)
EP (1) EP1289649B1 (https=)
JP (1) JP4959092B2 (https=)
KR (1) KR100809167B1 (https=)
CN (1) CN1216681C (https=)
AT (1) ATE358532T1 (https=)
AU (1) AU2001267470A1 (https=)
DE (2) DE10026142A1 (https=)
ES (1) ES2282264T3 (https=)
HU (1) HU229267B1 (https=)
PT (1) PT1289649E (https=)
WO (1) WO2001091898A1 (https=)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004053662A1 (de) 2004-11-03 2006-05-04 Basf Ag Verfahren zur Herstellung von Polyisocyanaten
JP2008002453A (ja) * 2006-05-22 2008-01-10 Nidec Sankyo Corp ミキシングポンプ装置および燃料電池
US8436204B2 (en) 2006-07-13 2013-05-07 Basf Aktiengesellschaft Method for producing isocyanates
JP2010507614A (ja) * 2006-10-26 2010-03-11 ビーエーエスエフ ソシエタス・ヨーロピア イソシアネートの製造方法
US9708185B2 (en) 2007-09-07 2017-07-18 Turbulent Energy, Llc Device for producing a gaseous fuel composite and system of production thereof
US8715378B2 (en) 2008-09-05 2014-05-06 Turbulent Energy, Llc Fluid composite, device for producing thereof and system of use
US8746965B2 (en) * 2007-09-07 2014-06-10 Turbulent Energy, Llc Method of dynamic mixing of fluids
US9310076B2 (en) 2007-09-07 2016-04-12 Turbulent Energy Llc Emulsion, apparatus, system and method for dynamic preparation
DE102008063728A1 (de) * 2008-12-18 2010-06-24 Bayer Materialscience Ag Verfahren zur Herstellung von Isocyanaten in der Gasphase
CN101708438B (zh) * 2009-12-04 2011-12-28 天津大学 一种混合器及制备有机异氰酸酯的方法
BR112012031995B1 (pt) 2010-06-14 2020-02-27 Dow Global Technologies Llc Misturador a jato reativo estático
WO2012050858A1 (en) * 2010-09-28 2012-04-19 Dow Global Technologies Llc Reactive flow static mixer with cross-flow obstructions
IN2014CN04741A (https=) * 2011-11-29 2015-09-18 Basf Se
CN108325492B (zh) * 2018-03-14 2023-12-19 湖北丽康源化工有限公司 一种制备h酸的硝化工艺及装置
US20230219044A1 (en) * 2020-06-10 2023-07-13 The Johns Hopkins University Axisymmetric confined impinging jet mixer

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0271684A2 (en) 1986-11-04 1988-06-22 Ube Cycon, Ltd. Process for agglomerating a polymer latex
EP0372483A1 (en) * 1988-12-05 1990-06-13 Albemarle Corporation Process to make alumunoxane
US5763697A (en) 1995-10-22 1998-06-09 Josef Meissner Gmbh & Co. Process for the nitration of aromatic compounds

Family Cites Families (21)

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Publication number Priority date Publication date Assignee Title
GB448489A (en) * 1935-10-10 1936-06-09 Concordia Elektrizitaets Ag A device for producing foam for fire extinguishing purposes
DE1146872B (de) * 1959-01-29 1963-04-11 Bayer Ag Verfahren zur Herstellung von organischen Isocyanaten
US3507626A (en) * 1965-10-15 1970-04-21 Mobay Chemical Corp Venturi mixer
GB1238669A (https=) * 1968-03-12 1971-07-07
FR2127146A5 (https=) 1971-02-25 1972-10-13 Brev Etudes Sibe
US3947484A (en) * 1971-10-26 1976-03-30 Bayer Aktiengesellschaft Continuous prephosgenation process for the production of organic isocyanates
CA1137076A (en) 1978-12-13 1982-12-07 John R. Bauer Fluid spray mixer - reactor system
US4289732A (en) * 1978-12-13 1981-09-15 The Upjohn Company Apparatus for intimately admixing two chemically reactive liquid components
JPS5748954A (en) * 1980-09-10 1982-03-20 Mitsui Toatsu Chem Inc Preparation of organic isocyanates
DE3630097A1 (de) * 1986-09-04 1988-03-17 Gerhard Ing Grad Moskau Verfahren und vorrichtung zur verbrennung, vergasung oder entgasung von abwaessern oder waessrigen schlaemmen
JPH0822375B2 (ja) * 1987-04-30 1996-03-06 ノードソン株式会社 液体の衝突式混合吐出又は噴出方法とその装置
JPS63286585A (ja) 1987-05-16 1988-11-24 Nippon Parkerizing Co Ltd チタンまたはその合金の化成処理液ならびに該化成処理液でのチタンまたはその合金の表面処理方法
DE3717057A1 (de) * 1987-05-21 1988-12-01 Bayer Ag Verfahren zur herstellung von isocyanaten
DE3744001C1 (de) 1987-12-24 1989-06-08 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Mono- oder Polyisocyanaten
JPH02152532A (ja) * 1988-12-02 1990-06-12 Minoru Nakamura 液体混合装置
DD300168A7 (de) * 1988-12-21 1992-05-27 Schwarzheide Synthesewerk Veb Verfahren und Vorrichtung zur kontinuierlichen Umsetzung von Diaminodiphenylmethan/Polyamin-Gemischen mit Phosgen zu Polyisocyanaten
JPH0676538B2 (ja) * 1989-05-30 1994-09-28 旭化成工業株式会社 ポリオキシメチレン組成物
SE505546C2 (sv) * 1995-12-11 1997-09-15 Moelnlycke Ab Metod att åstadkomma en svets eller ett klipp medelst ultraljud
DE19638567A1 (de) * 1996-09-20 1998-03-26 Bayer Ag Mischer-Reaktor und Verfahren zur Durchführung von Reaktionen, insbesondere die Phosgenierung von primären Aminen
JP3681561B2 (ja) * 1997-12-26 2005-08-10 日本碍子株式会社 物質の均一混合方法及び混合装置
DE19817691A1 (de) * 1998-04-21 1999-10-28 Basf Ag Verfahren zur Herstellung von Mischungen aus Diphenylmehandiisocyanaten und Polyphenylen-polymethylen-polyisocyanaten mit vermindertem Gehalt an chlorierten Nebenprodukten und verminderter Jodfarbzahl

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0271684A2 (en) 1986-11-04 1988-06-22 Ube Cycon, Ltd. Process for agglomerating a polymer latex
EP0372483A1 (en) * 1988-12-05 1990-06-13 Albemarle Corporation Process to make alumunoxane
US5763697A (en) 1995-10-22 1998-06-09 Josef Meissner Gmbh & Co. Process for the nitration of aromatic compounds

Also Published As

Publication number Publication date
CN1216681C (zh) 2005-08-31
JP4959092B2 (ja) 2012-06-20
PT1289649E (pt) 2007-05-31
US6867324B2 (en) 2005-03-15
CN1434743A (zh) 2003-08-06
DE50112295D1 (de) 2007-05-16
KR20030022132A (ko) 2003-03-15
ATE358532T1 (de) 2007-04-15
AU2001267470A1 (en) 2001-12-11
EP1289649B1 (de) 2007-04-04
EP1289649A1 (de) 2003-03-12
ES2282264T3 (es) 2007-10-16
WO2001091898A1 (de) 2001-12-06
JP2003535064A (ja) 2003-11-25
HUP0301844A3 (en) 2007-10-29
HU229267B1 (en) 2013-10-28
DE10026142A1 (de) 2001-12-13
HUP0301844A2 (hu) 2003-09-29
US20030166965A1 (en) 2003-09-04

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