KR100472911B1 - 난황 레시틴의 추출 방법 - Google Patents
난황 레시틴의 추출 방법 Download PDFInfo
- Publication number
- KR100472911B1 KR100472911B1 KR10-2002-0065268A KR20020065268A KR100472911B1 KR 100472911 B1 KR100472911 B1 KR 100472911B1 KR 20020065268 A KR20020065268 A KR 20020065268A KR 100472911 B1 KR100472911 B1 KR 100472911B1
- Authority
- KR
- South Korea
- Prior art keywords
- extraction
- lecithin
- yolk
- yolk powder
- extracting
- Prior art date
Links
- 238000000605 extraction Methods 0.000 title claims abstract description 71
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 title claims abstract description 43
- 239000000787 lecithin Substances 0.000 title claims abstract description 43
- 229940067606 lecithin Drugs 0.000 title claims abstract description 43
- 235000010445 lecithin Nutrition 0.000 title claims abstract description 43
- 238000000034 method Methods 0.000 claims abstract description 58
- 210000002969 egg yolk Anatomy 0.000 claims abstract description 57
- 239000007788 liquid Substances 0.000 claims abstract description 38
- 239000000843 powder Substances 0.000 claims abstract description 38
- 239000000284 extract Substances 0.000 claims abstract description 37
- 239000002904 solvent Substances 0.000 claims abstract description 28
- 238000004062 sedimentation Methods 0.000 claims abstract description 18
- 238000001704 evaporation Methods 0.000 claims abstract description 12
- 239000011877 solvent mixture Substances 0.000 claims abstract description 11
- 238000007738 vacuum evaporation Methods 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 230000008020 evaporation Effects 0.000 claims abstract description 7
- 150000002632 lipids Chemical class 0.000 claims abstract description 6
- 230000007935 neutral effect Effects 0.000 claims abstract description 6
- 239000006227 byproduct Substances 0.000 claims abstract description 5
- 239000012467 final product Substances 0.000 claims abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 36
- 239000000203 mixture Substances 0.000 claims description 6
- JQWAHKMIYCERGA-UHFFFAOYSA-N (2-nonanoyloxy-3-octadeca-9,12-dienoyloxypropoxy)-[2-(trimethylazaniumyl)ethyl]phosphinate Chemical compound CCCCCCCCC(=O)OC(COP([O-])(=O)CC[N+](C)(C)C)COC(=O)CCCCCCCC=CCC=CCCCCC JQWAHKMIYCERGA-UHFFFAOYSA-N 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 102000002322 Egg Proteins Human genes 0.000 abstract description 8
- 108010000912 Egg Proteins Proteins 0.000 abstract description 8
- 235000013345 egg yolk Nutrition 0.000 abstract description 8
- 238000000926 separation method Methods 0.000 description 6
- 239000000725 suspension Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 150000003904 phospholipids Chemical class 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000000306 component Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000013601 eggs Nutrition 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 206010003210 Arteriosclerosis Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 208000007536 Thrombosis Diseases 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000008358 core component Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 208000010125 myocardial infarction Diseases 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- WTJKGGKOPKCXLL-RRHRGVEJSA-N phosphatidylcholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCCC=CCCCCCCCC WTJKGGKOPKCXLL-RRHRGVEJSA-N 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J7/00—Phosphatide compositions for foodstuffs, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/14—Extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2300/00—Processes
- A23V2300/50—Concentrating, enriching or enhancing in functional factors
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Fats And Perfumes (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
Description
Claims (5)
- 레시틴의 추출 방법에 있어서,중성 지질이 제거된 정제 난황분 혹은 난황분 가공부산물에 3 내지 10배 내외의 추출 용매를 첨가하고 미리 설정된 시간동안 교반하는 추출 과정과;상기 추출 과정을 거친 난황분/추출 용매 혼합물을 침지시켜 액상의 추출액만을 이송시키는 침강 과정과;상기 침강 과정을 거친 난황분/추출 용매 혼합물의 침강된 정제 난황분을 재침지시켜 액상의 추출액만을 이송시키는 재추출 과정과;상기 침강 과정 및 재추출 과정의 액상 추출액을 연속식 진공증발 농축하여 추출 용매를 1차 증발시키는 1차 농축 과정과;상기 1차 농축 과정을 거친 액상 추출액을 회분식 진공증발 농축하여 잔존 추출 용매를 2차 증발시켜 최종 생산물인 레시틴을 얻는 2차 농축 과정을 포함함을 특징으로 하는 난황 레시틴의 추출 방법.
- 제 1항에 있어서,상기 추출 과정은 30 내지 65℃의 온도, 5 내지 100mmHg의 진공도 환경하에서 수행함을 특징으로 하는 난황 레시틴의 추출 방법.
- 제 1항 또는 제2항에 있어서,상기 추출 과정의 교반은 0.5 내지 3시간동안 수행함을 특징으로 하는 난황 레시틴의 추출 방법.
- 제 1항에 있어서,상기 1차 농축 과정 및 2차 농축 과정은 30 내지 60℃의 온도, 5 내지 100mmHg의 진공도 환경하에서 수행함을 특징으로 하는 난황 레시틴의 추출 방법.
- 제 1항에 있어서,상기 추출 과정의 추출 용매로는 에탄올, 물 혹은 에탄올/물 혼합액을 사용함을 특징으로 하는 난황 레시틴의 추출 방법.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR10-2002-0065268A KR100472911B1 (ko) | 2002-10-24 | 2002-10-24 | 난황 레시틴의 추출 방법 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR10-2002-0065268A KR100472911B1 (ko) | 2002-10-24 | 2002-10-24 | 난황 레시틴의 추출 방법 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR20040036303A KR20040036303A (ko) | 2004-04-30 |
KR100472911B1 true KR100472911B1 (ko) | 2005-03-10 |
Family
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Family Applications (1)
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KR10-2002-0065268A KR100472911B1 (ko) | 2002-10-24 | 2002-10-24 | 난황 레시틴의 추출 방법 |
Country Status (1)
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KR (1) | KR100472911B1 (ko) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20200022417A (ko) * | 2020-02-24 | 2020-03-03 | 정시호 | 난황레시틴 기반 홍삼 및 석류 함유 조성물의 제조방법 |
KR20210119600A (ko) * | 2020-03-24 | 2021-10-06 | 한양대학교 산학협력단 | 루테인 및 제아잔틴의 함량이 증대된 계란 생산방법, 이로부터 생산된 계란, 및 상기 계란으로부터 난황유 또는 난황 분말을 제조하는 방법 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101862570B1 (ko) * | 2018-01-19 | 2018-05-30 | 정시호 | 사포닌 흡수 증진을 위한 난황레시틴 기반 홍삼 함유 조성물의 제조방법 및 그 조성물 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01277457A (ja) * | 1988-04-27 | 1989-11-07 | Kao Corp | レシチンの精製方法 |
JPH0726287A (ja) * | 1993-07-14 | 1995-01-27 | Taiyo Kagaku Co Ltd | 卵黄脂質の製造方法 |
JPH1118688A (ja) * | 1997-07-02 | 1999-01-26 | Q P Corp | 卵黄レシチンの製造方法 |
KR20030066196A (ko) * | 2002-02-05 | 2003-08-09 | 강성식 | 난황 레시틴의 제조방법 |
-
2002
- 2002-10-24 KR KR10-2002-0065268A patent/KR100472911B1/ko active IP Right Grant
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01277457A (ja) * | 1988-04-27 | 1989-11-07 | Kao Corp | レシチンの精製方法 |
JPH0726287A (ja) * | 1993-07-14 | 1995-01-27 | Taiyo Kagaku Co Ltd | 卵黄脂質の製造方法 |
JPH1118688A (ja) * | 1997-07-02 | 1999-01-26 | Q P Corp | 卵黄レシチンの製造方法 |
KR20030066196A (ko) * | 2002-02-05 | 2003-08-09 | 강성식 | 난황 레시틴의 제조방법 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20200022417A (ko) * | 2020-02-24 | 2020-03-03 | 정시호 | 난황레시틴 기반 홍삼 및 석류 함유 조성물의 제조방법 |
KR102120165B1 (ko) | 2020-02-24 | 2020-06-08 | 정시호 | 난황레시틴 기반 홍삼 및 석류 함유 조성물의 제조방법 |
KR20210119600A (ko) * | 2020-03-24 | 2021-10-06 | 한양대학교 산학협력단 | 루테인 및 제아잔틴의 함량이 증대된 계란 생산방법, 이로부터 생산된 계란, 및 상기 계란으로부터 난황유 또는 난황 분말을 제조하는 방법 |
KR102508306B1 (ko) | 2020-03-24 | 2023-03-10 | 한양대학교 산학협력단 | 루테인 및 제아잔틴의 함량이 증대된 계란 생산방법, 이로부터 생산된 계란, 및 상기 계란으로부터 난황유 또는 난황 분말을 제조하는 방법 |
Also Published As
Publication number | Publication date |
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KR20040036303A (ko) | 2004-04-30 |
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