JPS6335449A - 磁器組成物の製造方法 - Google Patents
磁器組成物の製造方法Info
- Publication number
- JPS6335449A JPS6335449A JP61179639A JP17963986A JPS6335449A JP S6335449 A JPS6335449 A JP S6335449A JP 61179639 A JP61179639 A JP 61179639A JP 17963986 A JP17963986 A JP 17963986A JP S6335449 A JPS6335449 A JP S6335449A
- Authority
- JP
- Japan
- Prior art keywords
- composition
- alkoxide
- plzt
- lanthanum
- lead
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000203 mixture Substances 0.000 title claims description 60
- 239000000919 ceramic Substances 0.000 title claims description 24
- 238000004519 manufacturing process Methods 0.000 title claims description 15
- 150000004703 alkoxides Chemical class 0.000 claims description 19
- -1 zirconium alkoxide Chemical class 0.000 claims description 16
- 229910052573 porcelain Inorganic materials 0.000 claims description 13
- 239000010936 titanium Substances 0.000 claims description 11
- 239000007864 aqueous solution Substances 0.000 claims description 10
- 229910052726 zirconium Inorganic materials 0.000 claims description 10
- 229910052746 lanthanum Inorganic materials 0.000 claims description 9
- 229910052719 titanium Inorganic materials 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 239000002244 precipitate Substances 0.000 claims description 8
- FYDKNKUEBJQCCN-UHFFFAOYSA-N lanthanum(3+);trinitrate Chemical compound [La+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O FYDKNKUEBJQCCN-UHFFFAOYSA-N 0.000 claims description 7
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 6
- JLRJWBUSTKIQQH-UHFFFAOYSA-K lanthanum(3+);triacetate Chemical compound [La+3].CC([O-])=O.CC([O-])=O.CC([O-])=O JLRJWBUSTKIQQH-UHFFFAOYSA-K 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 239000003960 organic solvent Substances 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 238000000354 decomposition reaction Methods 0.000 claims description 2
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 239000000843 powder Substances 0.000 description 22
- 238000005259 measurement Methods 0.000 description 17
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 12
- 229910052751 metal Inorganic materials 0.000 description 9
- 239000002184 metal Substances 0.000 description 9
- 239000002994 raw material Substances 0.000 description 9
- 239000003990 capacitor Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 238000010304 firing Methods 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- AGZCHLPJCXXPDM-UHFFFAOYSA-N dibutoxylead Chemical compound [Pb+2].CCCC[O-].CCCC[O-] AGZCHLPJCXXPDM-UHFFFAOYSA-N 0.000 description 4
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 229910052709 silver Inorganic materials 0.000 description 3
- 239000004332 silver Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- BSDOQSMQCZQLDV-UHFFFAOYSA-N butan-1-olate;zirconium(4+) Chemical compound [Zr+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] BSDOQSMQCZQLDV-UHFFFAOYSA-N 0.000 description 2
- 238000000975 co-precipitation Methods 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000008096 xylene Substances 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000003985 ceramic capacitor Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- VSFQMZYFJAOOOG-UHFFFAOYSA-N di(propan-2-yloxy)lead Chemical group CC(C)O[Pb]OC(C)C VSFQMZYFJAOOOG-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum oxide Inorganic materials [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000009766 low-temperature sintering Methods 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000007777 multifunctional material Substances 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- ZGSOBQAJAUGRBK-UHFFFAOYSA-N propan-2-olate;zirconium(4+) Chemical group [Zr+4].CC(C)[O-].CC(C)[O-].CC(C)[O-].CC(C)[O-] ZGSOBQAJAUGRBK-UHFFFAOYSA-N 0.000 description 1
- 230000035936 sexual power Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
- C04B35/49—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates containing also titanium oxides or titanates
- C04B35/491—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates containing also titanium oxides or titanates based on lead zirconates and lead titanates, e.g. PZT
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G25/00—Compounds of zirconium
- C01G25/006—Compounds containing, besides zirconium, two or more other elements, with the exception of oxygen or hydrogen
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Nanotechnology (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Composite Materials (AREA)
- Structural Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Insulating Materials (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61179639A JPS6335449A (ja) | 1986-07-30 | 1986-07-30 | 磁器組成物の製造方法 |
| GB8705883A GB2193204B (en) | 1986-07-30 | 1987-03-12 | Method of producing ceramic composition |
| BE8700317A BE1000125A4 (fr) | 1986-07-30 | 1987-03-27 | Procede de production d'une composition ceramique et composition ainsi obtenue. |
| DE19873710975 DE3710975A1 (de) | 1986-07-30 | 1987-04-01 | Verfahren zur herstellung einer keramikzusammensetzung |
| NL8701520A NL8701520A (nl) | 1986-07-30 | 1987-06-29 | Werkwijze voor het vervaardigen van een keramische samenstelling. |
| FR8710686A FR2602225B1 (fr) | 1986-07-30 | 1987-07-28 | Procede de preparation d'une composition ceramique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61179639A JPS6335449A (ja) | 1986-07-30 | 1986-07-30 | 磁器組成物の製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6335449A true JPS6335449A (ja) | 1988-02-16 |
Family
ID=16069283
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61179639A Pending JPS6335449A (ja) | 1986-07-30 | 1986-07-30 | 磁器組成物の製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS6335449A (fr) |
| BE (1) | BE1000125A4 (fr) |
| DE (1) | DE3710975A1 (fr) |
| FR (1) | FR2602225B1 (fr) |
| GB (1) | GB2193204B (fr) |
| NL (1) | NL8701520A (fr) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02246838A (ja) * | 1989-03-17 | 1990-10-02 | Toyota Motor Corp | 車両用安全制御装置 |
| JPH04296040A (ja) * | 1991-03-25 | 1992-10-20 | Ngk Insulators Ltd | 静電チャック |
| JP2007099268A (ja) * | 2002-06-10 | 2007-04-19 | Nissan Motor Co Ltd | 車両用運転操作補助装置およびその装置を備えた車両 |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10323816A1 (de) | 2003-05-23 | 2004-12-09 | Basf Ag | Verfahren zur Herstellung von Mischoxiden mit mittleren Durchmessern kleiner als 10 Nanometer |
| CN111499384B (zh) * | 2020-04-09 | 2021-06-15 | 中国科学院上海硅酸盐研究所 | 一种高储能密度温度稳定性plzt反铁电陶瓷材料及其制备方法 |
| CN113716606B (zh) * | 2021-08-25 | 2022-09-06 | 中国科学院上海硅酸盐研究所 | 一种plzt微米晶种及其制备方法和在诱导陶瓷生长中的应用 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58199719A (ja) * | 1982-05-17 | 1983-11-21 | Mitsubishi Mining & Cement Co Ltd | 金属酸化物固溶体の製造方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3718723A (en) * | 1970-10-23 | 1973-02-27 | Bell Telephone Labor Inc | Use of water soluble lanthanum compounds in lead zirconate-lead titanate ceramics |
| US3702724A (en) * | 1971-10-13 | 1972-11-14 | Atomic Energy Commission | Ferroelectric ceramic plate electrooptical light scattering device and method |
| US3923675A (en) * | 1973-08-09 | 1975-12-02 | Us Air Force | Method for preparing lead lanthanum zirconate-titanate powders |
| US3917780A (en) * | 1973-08-09 | 1975-11-04 | Us Air Force | Preparation of lead lanthanum zirconate titanate bodies |
| JPS60103031A (ja) * | 1983-11-10 | 1985-06-07 | Agency Of Ind Science & Technol | Ｐｌζｔ又はｐζｔの製造方法 |
| JPS60141675A (ja) * | 1983-12-28 | 1985-07-26 | 日本曹達株式会社 | 透光性強誘電体磁器の製造方法 |
| JPH0652332A (ja) * | 1992-08-03 | 1994-02-25 | Nec Corp | シングルチップマイクロコンピュータ |
-
1986
- 1986-07-30 JP JP61179639A patent/JPS6335449A/ja active Pending
-
1987
- 1987-03-12 GB GB8705883A patent/GB2193204B/en not_active Expired - Fee Related
- 1987-03-27 BE BE8700317A patent/BE1000125A4/fr not_active IP Right Cessation
- 1987-04-01 DE DE19873710975 patent/DE3710975A1/de active Granted
- 1987-06-29 NL NL8701520A patent/NL8701520A/nl not_active Application Discontinuation
- 1987-07-28 FR FR8710686A patent/FR2602225B1/fr not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58199719A (ja) * | 1982-05-17 | 1983-11-21 | Mitsubishi Mining & Cement Co Ltd | 金属酸化物固溶体の製造方法 |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02246838A (ja) * | 1989-03-17 | 1990-10-02 | Toyota Motor Corp | 車両用安全制御装置 |
| JPH04296040A (ja) * | 1991-03-25 | 1992-10-20 | Ngk Insulators Ltd | 静電チャック |
| JP2007099268A (ja) * | 2002-06-10 | 2007-04-19 | Nissan Motor Co Ltd | 車両用運転操作補助装置およびその装置を備えた車両 |
| JP4661758B2 (ja) * | 2002-06-10 | 2011-03-30 | 日産自動車株式会社 | 車両用運転操作補助装置およびその装置を備えた車両 |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2602225B1 (fr) | 1990-08-03 |
| BE1000125A4 (fr) | 1988-04-12 |
| DE3710975C2 (fr) | 1993-09-09 |
| GB8705883D0 (en) | 1987-04-15 |
| FR2602225A1 (fr) | 1988-02-05 |
| GB2193204A (en) | 1988-02-03 |
| GB2193204B (en) | 1990-04-04 |
| DE3710975A1 (de) | 1988-02-11 |
| NL8701520A (nl) | 1988-02-16 |
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