JPS6327389B2 - - Google Patents
Info
- Publication number
- JPS6327389B2 JPS6327389B2 JP59093111A JP9311184A JPS6327389B2 JP S6327389 B2 JPS6327389 B2 JP S6327389B2 JP 59093111 A JP59093111 A JP 59093111A JP 9311184 A JP9311184 A JP 9311184A JP S6327389 B2 JPS6327389 B2 JP S6327389B2
- Authority
- JP
- Japan
- Prior art keywords
- rare earth
- manufacturing
- route
- temperature
- oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000203 mixture Substances 0.000 claims abstract description 114
- 238000005498 polishing Methods 0.000 claims abstract description 63
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 63
- 239000011521 glass Substances 0.000 claims abstract description 32
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229940044927 ceric oxide Drugs 0.000 claims abstract description 20
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 claims abstract description 20
- 229910052727 yttrium Inorganic materials 0.000 claims abstract description 14
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229910052747 lanthanoid Inorganic materials 0.000 claims abstract description 12
- 150000002602 lanthanoids Chemical class 0.000 claims abstract description 12
- 229910052692 Dysprosium Inorganic materials 0.000 claims abstract description 5
- 229910052688 Gadolinium Inorganic materials 0.000 claims abstract description 5
- 229910052772 Samarium Inorganic materials 0.000 claims abstract description 5
- 229910052775 Thulium Inorganic materials 0.000 claims abstract description 5
- 229910052769 Ytterbium Inorganic materials 0.000 claims abstract description 5
- KBQHZAAAGSGFKK-UHFFFAOYSA-N dysprosium atom Chemical compound [Dy] KBQHZAAAGSGFKK-UHFFFAOYSA-N 0.000 claims abstract description 5
- UIWYJDYFSGRHKR-UHFFFAOYSA-N gadolinium atom Chemical compound [Gd] UIWYJDYFSGRHKR-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052746 lanthanum Inorganic materials 0.000 claims abstract description 5
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims abstract description 5
- OHSVLFRHMCKCQY-UHFFFAOYSA-N lutetium atom Chemical compound [Lu] OHSVLFRHMCKCQY-UHFFFAOYSA-N 0.000 claims abstract description 5
- KZUNJOHGWZRPMI-UHFFFAOYSA-N samarium atom Chemical compound [Sm] KZUNJOHGWZRPMI-UHFFFAOYSA-N 0.000 claims abstract description 5
- NAWDYIZEMPQZHO-UHFFFAOYSA-N ytterbium Chemical compound [Yb] NAWDYIZEMPQZHO-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052693 Europium Inorganic materials 0.000 claims abstract 3
- OGPBJKLSAFTDLK-UHFFFAOYSA-N europium atom Chemical compound [Eu] OGPBJKLSAFTDLK-UHFFFAOYSA-N 0.000 claims abstract 3
- 239000002244 precipitate Substances 0.000 claims description 53
- 238000004519 manufacturing process Methods 0.000 claims description 42
- 238000000034 method Methods 0.000 claims description 41
- 239000000243 solution Substances 0.000 claims description 40
- 238000006243 chemical reaction Methods 0.000 claims description 27
- 239000007864 aqueous solution Substances 0.000 claims description 25
- 239000012429 reaction media Substances 0.000 claims description 24
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical class OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 22
- 239000002245 particle Substances 0.000 claims description 21
- 239000012266 salt solution Substances 0.000 claims description 21
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum(3+);oxygen(2-) Chemical group [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 claims description 20
- 238000002156 mixing Methods 0.000 claims description 19
- 230000008569 process Effects 0.000 claims description 19
- 150000003839 salts Chemical class 0.000 claims description 19
- 229910052684 Cerium Inorganic materials 0.000 claims description 18
- 150000000703 Cerium Chemical class 0.000 claims description 17
- 238000001354 calcination Methods 0.000 claims description 16
- 238000001035 drying Methods 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 230000032683 aging Effects 0.000 claims description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 239000007900 aqueous suspension Substances 0.000 claims description 11
- 238000010304 firing Methods 0.000 claims description 10
- 239000007800 oxidant agent Substances 0.000 claims description 9
- 230000005070 ripening Effects 0.000 claims description 8
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- 229910052765 Lutetium Inorganic materials 0.000 claims description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- HSJPMRKMPBAUAU-UHFFFAOYSA-N cerium(3+);trinitrate Chemical compound [Ce+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O HSJPMRKMPBAUAU-UHFFFAOYSA-N 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical class [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical class [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 150000001805 chlorine compounds Chemical class 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 150000002823 nitrates Chemical class 0.000 claims description 2
- 239000001301 oxygen Chemical class 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 claims 4
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical class OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 claims 2
- 229910004664 Cerium(III) chloride Inorganic materials 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- VYLVYHXQOHJDJL-UHFFFAOYSA-K cerium trichloride Chemical compound Cl[Ce](Cl)Cl VYLVYHXQOHJDJL-UHFFFAOYSA-K 0.000 claims 1
- XTEGARKTQYYJKE-UHFFFAOYSA-N chloric acid Chemical class OCl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-N 0.000 claims 1
- 229940005991 chloric acid Drugs 0.000 claims 1
- 238000006056 electrooxidation reaction Methods 0.000 claims 1
- 238000000605 extraction Methods 0.000 claims 1
- 239000012065 filter cake Substances 0.000 claims 1
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical class ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 claims 1
- 150000004968 peroxymonosulfuric acids Chemical class 0.000 claims 1
- 238000010298 pulverizing process Methods 0.000 claims 1
- 239000000725 suspension Substances 0.000 abstract description 26
- -1 yttrium rare earth Chemical class 0.000 abstract description 8
- 238000009472 formulation Methods 0.000 abstract 1
- 238000005816 glass manufacturing process Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 description 30
- 230000000694 effects Effects 0.000 description 24
- 238000012360 testing method Methods 0.000 description 23
- 238000003756 stirring Methods 0.000 description 17
- 239000002585 base Substances 0.000 description 15
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 14
- 238000002360 preparation method Methods 0.000 description 9
- 230000001105 regulatory effect Effects 0.000 description 9
- 239000003153 chemical reaction reagent Substances 0.000 description 8
- 238000009826 distribution Methods 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 238000001914 filtration Methods 0.000 description 7
- 230000005484 gravity Effects 0.000 description 7
- 229910000420 cerium oxide Inorganic materials 0.000 description 6
- 239000011737 fluorine Substances 0.000 description 6
- 229910052731 fluorine Inorganic materials 0.000 description 6
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 description 6
- 238000000926 separation method Methods 0.000 description 6
- 229920005830 Polyurethane Foam Polymers 0.000 description 5
- 238000000227 grinding Methods 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 239000011496 polyurethane foam Substances 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- 150000002910 rare earth metals Chemical class 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 238000010908 decantation Methods 0.000 description 4
- 238000010979 pH adjustment Methods 0.000 description 4
- 230000002688 persistence Effects 0.000 description 4
- 238000004062 sedimentation Methods 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- DRVWBEJJZZTIGJ-UHFFFAOYSA-N cerium(3+);oxygen(2-) Chemical class [O-2].[O-2].[O-2].[Ce+3].[Ce+3] DRVWBEJJZZTIGJ-UHFFFAOYSA-N 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- CMIHHWBVHJVIGI-UHFFFAOYSA-N gadolinium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[Gd+3].[Gd+3] CMIHHWBVHJVIGI-UHFFFAOYSA-N 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- FYDKNKUEBJQCCN-UHFFFAOYSA-N lanthanum(3+);trinitrate Chemical compound [La+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O FYDKNKUEBJQCCN-UHFFFAOYSA-N 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 2
- 229910010293 ceramic material Inorganic materials 0.000 description 2
- 230000001186 cumulative effect Effects 0.000 description 2
- 239000005357 flat glass Substances 0.000 description 2
- 238000005189 flocculation Methods 0.000 description 2
- 230000016615 flocculation Effects 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- PLDDOISOJJCEMH-UHFFFAOYSA-N neodymium(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Nd+3].[Nd+3] PLDDOISOJJCEMH-UHFFFAOYSA-N 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000004438 BET method Methods 0.000 description 1
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical class [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- HHEFNVCDPLQQTP-UHFFFAOYSA-N ammonium perchlorate Chemical class [NH4+].[O-]Cl(=O)(=O)=O HHEFNVCDPLQQTP-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000003637 basic solution Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- XMPZTFVPEKAKFH-UHFFFAOYSA-P ceric ammonium nitrate Chemical compound [NH4+].[NH4+].[Ce+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O XMPZTFVPEKAKFH-UHFFFAOYSA-P 0.000 description 1
- UNJPQTDTZAKTFK-UHFFFAOYSA-K cerium(iii) hydroxide Chemical compound [OH-].[OH-].[OH-].[Ce+3] UNJPQTDTZAKTFK-UHFFFAOYSA-K 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000007705 chemical test Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 229910001938 gadolinium oxide Inorganic materials 0.000 description 1
- 229940075613 gadolinium oxide Drugs 0.000 description 1
- MWFSXYMZCVAQCC-UHFFFAOYSA-N gadolinium(iii) nitrate Chemical compound [Gd+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O MWFSXYMZCVAQCC-UHFFFAOYSA-N 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 235000003642 hunger Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical class Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910000358 iron sulfate Inorganic materials 0.000 description 1
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
- 239000005355 lead glass Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 238000011022 operating instruction Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- MMKQUGHLEMYQSG-UHFFFAOYSA-N oxygen(2-);praseodymium(3+) Chemical compound [O-2].[O-2].[O-2].[Pr+3].[Pr+3] MMKQUGHLEMYQSG-UHFFFAOYSA-N 0.000 description 1
- 238000003921 particle size analysis Methods 0.000 description 1
- FHHJDRFHHWUPDG-UHFFFAOYSA-N peroxysulfuric acid Chemical compound OOS(O)(=O)=O FHHJDRFHHWUPDG-UHFFFAOYSA-N 0.000 description 1
- JRKICGRDRMAZLK-UHFFFAOYSA-L persulfate group Chemical group S(=O)(=O)([O-])OOS(=O)(=O)[O-] JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000007517 polishing process Methods 0.000 description 1
- 229910003447 praseodymium oxide Inorganic materials 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000001226 reprecipitation Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 1
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
- 239000008234 soft water Substances 0.000 description 1
- 230000037351 starvation Effects 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000010456 wollastonite Substances 0.000 description 1
- 229910052882 wollastonite Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/002—Use of waste materials, e.g. slags
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/14—Anti-slip materials; Abrasives
- C09K3/1454—Abrasive powders, suspensions and pastes for polishing
Landscapes
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Geochemistry & Mineralogy (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polishing Bodies And Polishing Tools (AREA)
- Catalysts (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Mechanical Treatment Of Semiconductor (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
- Glass Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR83.08003 | 1983-05-13 | ||
| FR8308003A FR2545830B1 (fr) | 1983-05-13 | 1983-05-13 | Nouvelle composition de polissage a base de cerium et son procede de fabrication |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6035075A JPS6035075A (ja) | 1985-02-22 |
| JPS6327389B2 true JPS6327389B2 (cg-RX-API-DMAC10.html) | 1988-06-02 |
Family
ID=9288843
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59093111A Granted JPS6035075A (ja) | 1983-05-13 | 1984-05-11 | 新規なセリウム系研磨組成物及びその製造法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4786325A (cg-RX-API-DMAC10.html) |
| EP (1) | EP0126675B1 (cg-RX-API-DMAC10.html) |
| JP (1) | JPS6035075A (cg-RX-API-DMAC10.html) |
| AT (1) | ATE37896T1 (cg-RX-API-DMAC10.html) |
| AU (1) | AU571518B2 (cg-RX-API-DMAC10.html) |
| BR (1) | BR8402229A (cg-RX-API-DMAC10.html) |
| DE (1) | DE3474563D1 (cg-RX-API-DMAC10.html) |
| FR (1) | FR2545830B1 (cg-RX-API-DMAC10.html) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0359894U (cg-RX-API-DMAC10.html) * | 1989-08-21 | 1991-06-12 | ||
| US6887289B2 (en) | 2000-12-25 | 2005-05-03 | Nissan Chemical Industries, Ltd. | Cerium oxide sol and abrasive |
| WO2012101871A1 (ja) * | 2011-01-25 | 2012-08-02 | コニカミノルタホールディングス株式会社 | 研磨材微粒子及びその製造方法 |
| JP2015120844A (ja) * | 2013-12-24 | 2015-07-02 | 旭硝子株式会社 | 研磨剤の製造方法、研磨方法および半導体集積回路装置の製造方法 |
| WO2017183290A1 (ja) * | 2016-04-20 | 2017-10-26 | 信越化学工業株式会社 | 合成石英ガラス基板用研磨剤及び合成石英ガラス基板の研磨方法 |
| WO2018190077A1 (ja) * | 2017-04-10 | 2018-10-18 | 信越化学工業株式会社 | 合成石英ガラス基板用研磨剤及びその製造方法並びに合成石英ガラス基板の研磨方法 |
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| FR2584388B1 (fr) * | 1985-07-03 | 1991-02-15 | Rhone Poulenc Spec Chim | Composition a base d'oxyde cerique, sa preparation et ses utilisations |
| FR2604443A1 (fr) * | 1986-09-26 | 1988-04-01 | Rhone Poulenc Chimie | Composition de polissage a base de cerium destinee au polissage des verres organiques |
| FR2617153B1 (fr) * | 1987-06-26 | 1991-04-05 | Rhone Poulenc Chimie | Procede d'obtention d'un oxyde cerique et oxyde cerique a nouvelles caracteristiques morphologiques |
| FR2617154B1 (fr) * | 1987-06-29 | 1990-11-30 | Rhone Poulenc Chimie | Procede d'obtention d'oxyde cerique et oxyde cerique a nouvelles caracteristiques morphologiques |
| ATE67469T1 (de) * | 1987-06-29 | 1991-10-15 | Rhone Poulenc Chimie | Verfahren zur gewinnung eines ceriumoxids. |
| FR2624519A1 (fr) * | 1987-12-09 | 1989-06-16 | Rhone Poulenc Chimie | Composition de polissage perfectionnee a base de cerium et son procede de preparation |
| FR2631630B1 (fr) * | 1988-05-18 | 1990-08-31 | Rhone Poulenc Chimie | Abrasifs a base de terres rares |
| US5106394A (en) * | 1990-10-01 | 1992-04-21 | The United States Of America As Represented By The Secretary Of The Navy | Fiber optic polishing system |
| US5376222A (en) * | 1991-09-04 | 1994-12-27 | Fujitsu Limited | Polishing method for polycrystalline silicon |
| US5264010A (en) * | 1992-04-27 | 1993-11-23 | Rodel, Inc. | Compositions and methods for polishing and planarizing surfaces |
| US5654057A (en) * | 1994-12-28 | 1997-08-05 | Hoya Corporation | Sheet glass flattening method, method of manufacturing glass substrate for an information recording disk using flattened glass, method of manufacturing a magnetic recording disk using glass substrate, and magnetic recording medium |
| JP2746861B2 (ja) * | 1995-11-20 | 1998-05-06 | 三井金属鉱業株式会社 | 酸化セリウム超微粒子の製造方法 |
| WO1997029510A1 (fr) * | 1996-02-07 | 1997-08-14 | Hitachi Chemical Company, Ltd. | Abrasif d'oxyde de cerium, microplaquette semi-conductrice, dispositif semi-conducteur, procede pour les produire et procede pour polir les substrats |
| US5897675A (en) * | 1996-04-26 | 1999-04-27 | Degussa Aktiengesellschaft | Cerium oxide-metal/metalloid oxide mixture |
| US5962343A (en) * | 1996-07-30 | 1999-10-05 | Nissan Chemical Industries, Ltd. | Process for producing crystalline ceric oxide particles and abrasive |
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| US6447375B2 (en) | 2000-04-19 | 2002-09-10 | Rodel Holdings Inc. | Polishing method using a reconstituted dry particulate polishing composition |
| US6454821B1 (en) | 2000-06-21 | 2002-09-24 | Praxair S. T. Technology, Inc. | Polishing composition and method |
| US20060032836A1 (en) * | 2001-11-16 | 2006-02-16 | Ferro Corporation | Methods of controlling the properties of abrasive particles for use in chemical-mechanical polishing slurries |
| US6596042B1 (en) | 2001-11-16 | 2003-07-22 | Ferro Corporation | Method of forming particles for use in chemical-mechanical polishing slurries and the particles formed by the process |
| US7666239B2 (en) * | 2001-11-16 | 2010-02-23 | Ferro Corporation | Hydrothermal synthesis of cerium-titanium oxide for use in CMP |
| WO2003044123A1 (en) * | 2001-11-16 | 2003-05-30 | Ferro Corporation | Particles for use in cmp slurries and method for producing them |
| JP4236857B2 (ja) * | 2002-03-22 | 2009-03-11 | 三井金属鉱業株式会社 | セリウム系研摩材およびその製造方法 |
| US7025943B2 (en) * | 2002-05-15 | 2006-04-11 | The Curators Of The University Of Missouri | Method for preparation of nanometer cerium-based oxide particles |
| JP2004222009A (ja) * | 2003-01-16 | 2004-08-05 | Nec Corp | 異種網接続ゲートウェイおよび異種網間通信課金システム |
| KR100647103B1 (ko) * | 2003-06-30 | 2006-11-23 | 미쓰이 긴조꾸 고교 가부시키가이샤 | 세륨계 연마재 및 그 원료 |
| US7279036B2 (en) * | 2004-12-23 | 2007-10-09 | Council Of Scientific And Industrial Research | Process for preparation of inorganic colorants from mixed rare earth compounds |
| AT502308B1 (de) * | 2005-07-20 | 2010-03-15 | Treibacher Ind Ag | Glasschleifmittel auf ceroxidbasis und verfahren zu dessen herstellung |
| US8883865B2 (en) | 2006-09-05 | 2014-11-11 | Cerion Technology, Inc. | Cerium-containing nanoparticles |
| US10435639B2 (en) | 2006-09-05 | 2019-10-08 | Cerion, Llc | Fuel additive containing lattice engineered cerium dioxide nanoparticles |
| JP2010502820A (ja) | 2006-09-05 | 2010-01-28 | セリオン テクノロジー， インコーポレーテッド | 二酸化セリウムナノ粒子含有燃料添加剤 |
| JP5237542B2 (ja) * | 2006-10-03 | 2013-07-17 | 三井金属鉱業株式会社 | 酸化セリウム系研摩材 |
| US8349764B2 (en) | 2007-10-31 | 2013-01-08 | Molycorp Minerals, Llc | Composition for treating a fluid |
| KR20100121636A (ko) * | 2008-02-08 | 2010-11-18 | 유미코르 | 조절된 형태를 갖는 도핑된 세리아 연마제 및 이의 제조 방법 |
| KR100873945B1 (ko) * | 2008-07-16 | 2008-12-12 | (주) 뉴웰 | 미세 산화세륨 분말 그 제조 방법 및 이를 포함하는 씨엠피슬러리 |
| CN102391833B (zh) * | 2011-09-08 | 2013-08-07 | 金华冠华水晶有限公司 | 一种再生应用于水晶玻璃的废弃稀土抛光粉的方法 |
| CN102643614B (zh) * | 2012-04-17 | 2014-02-12 | 江苏中晶科技有限公司 | 玻璃抛光粉及其制备方法 |
| CN103253694B (zh) * | 2013-05-19 | 2014-07-16 | 郭尧 | 一种制备氧化镧铈稀土抛光粉的煅烧工艺 |
| WO2015058037A1 (en) | 2013-10-17 | 2015-04-23 | Cerion, Llc | Malic acid stabilized nanoceria particles |
| KR102350893B1 (ko) * | 2014-06-24 | 2022-01-13 | 로디아 오퍼레이션스 | 금속 도핑된 세륨 산화물 조성물 |
| KR20250018539A (ko) * | 2022-07-12 | 2025-02-06 | 가부시끼가이샤 레조낙 | 세륨계 연마재, 연마액, 연마액의 제조방법, 및 유리 연마방법 |
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|---|---|---|---|---|
| US3097083A (en) * | 1959-07-02 | 1963-07-09 | American Potash & Chem Corp | Polishing composition and process of forming same |
| US3240580A (en) * | 1961-04-03 | 1966-03-15 | Libbey Owens Ford Glass Co | Glass polishing compositions of rare earth nitrates |
| DE1180723B (de) * | 1963-06-28 | 1964-11-05 | Degussa | Verfahren und Vorrichtung zur Herstellung von feinteiliger amorpher Kieselsaeure |
| US3317293A (en) * | 1964-04-20 | 1967-05-02 | Libbey Owens Ford Glass Co | Rare earth chlorides in a glass polishing composition |
| US3768989A (en) * | 1968-08-19 | 1973-10-30 | N Goetzinger | Process for the preparation of a rare earth oxide polishing composition |
| FI46249C (fi) * | 1970-09-15 | 1973-02-12 | Kemira Oy | Menetelmä ceriumoksidin valkoisuuden parantamiseksi |
| FR2472601A1 (fr) * | 1979-12-27 | 1981-07-03 | Rhone Poulenc Ind | Procede de fabrication de compositions de polissage a base de cerium |
-
1983
- 1983-05-13 FR FR8308003A patent/FR2545830B1/fr not_active Expired
-
1984
- 1984-05-04 EP EP84400920A patent/EP0126675B1/fr not_active Expired
- 1984-05-04 DE DE8484400920T patent/DE3474563D1/de not_active Expired
- 1984-05-04 AT AT84400920T patent/ATE37896T1/de not_active IP Right Cessation
- 1984-05-11 JP JP59093111A patent/JPS6035075A/ja active Granted
- 1984-05-11 BR BR8402229A patent/BR8402229A/pt not_active IP Right Cessation
- 1984-05-11 AU AU27955/84A patent/AU571518B2/en not_active Ceased
-
1986
- 1986-07-21 US US06/887,389 patent/US4786325A/en not_active Expired - Lifetime
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0359894U (cg-RX-API-DMAC10.html) * | 1989-08-21 | 1991-06-12 | ||
| US6887289B2 (en) | 2000-12-25 | 2005-05-03 | Nissan Chemical Industries, Ltd. | Cerium oxide sol and abrasive |
| WO2012101871A1 (ja) * | 2011-01-25 | 2012-08-02 | コニカミノルタホールディングス株式会社 | 研磨材微粒子及びその製造方法 |
| JP2015120844A (ja) * | 2013-12-24 | 2015-07-02 | 旭硝子株式会社 | 研磨剤の製造方法、研磨方法および半導体集積回路装置の製造方法 |
| WO2017183290A1 (ja) * | 2016-04-20 | 2017-10-26 | 信越化学工業株式会社 | 合成石英ガラス基板用研磨剤及び合成石英ガラス基板の研磨方法 |
| JP2017193621A (ja) * | 2016-04-20 | 2017-10-26 | 信越化学工業株式会社 | 合成石英ガラス基板用研磨剤及び合成石英ガラス基板の研磨方法 |
| US11180677B2 (en) | 2016-04-20 | 2021-11-23 | Shin-Etsu Chemical Co., Ltd. | Polishing agent for synthetic quartz glass substrate and method for polishing synthetic quartz glass substrate |
| WO2018190077A1 (ja) * | 2017-04-10 | 2018-10-18 | 信越化学工業株式会社 | 合成石英ガラス基板用研磨剤及びその製造方法並びに合成石英ガラス基板の研磨方法 |
| JP2018177923A (ja) * | 2017-04-10 | 2018-11-15 | 信越化学工業株式会社 | 合成石英ガラス基板用研磨剤及びその製造方法並びに合成石英ガラス基板の研磨方法 |
| US12173193B2 (en) | 2017-11-17 | 2024-12-24 | Shin-Etsu Chemical Co., Ltd. | Polishing agent for synthetic quartz glass substrate and method for polishing synthetic quartz glass substrate |
| US12187920B2 (en) | 2020-05-21 | 2025-01-07 | Shin-Etsu Chemical Co., Ltd. | Polishing agent for synthetic quartz glass substrate and producing method for polishing agent, and method for polishing synthetic quartz glass substrate |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2545830A1 (fr) | 1984-11-16 |
| ATE37896T1 (de) | 1988-10-15 |
| US4786325A (en) | 1988-11-22 |
| BR8402229A (pt) | 1984-12-18 |
| JPS6035075A (ja) | 1985-02-22 |
| AU2795584A (en) | 1984-11-15 |
| EP0126675B1 (fr) | 1988-10-12 |
| DE3474563D1 (en) | 1988-11-17 |
| AU571518B2 (en) | 1988-04-21 |
| FR2545830B1 (fr) | 1986-01-03 |
| EP0126675A1 (fr) | 1984-11-28 |
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