JPS6125694B2 - - Google Patents
Info
- Publication number
- JPS6125694B2 JPS6125694B2 JP58075574A JP7557483A JPS6125694B2 JP S6125694 B2 JPS6125694 B2 JP S6125694B2 JP 58075574 A JP58075574 A JP 58075574A JP 7557483 A JP7557483 A JP 7557483A JP S6125694 B2 JPS6125694 B2 JP S6125694B2
- Authority
- JP
- Japan
- Prior art keywords
- hexafluoroacetone
- hydrate
- reaction
- catalyst
- palladium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003054 catalyst Substances 0.000 claims description 15
- BYEAHWXPCBROCE-UHFFFAOYSA-N 1,1,1,3,3,3-hexafluoropropan-2-ol Chemical compound FC(F)(F)C(O)C(F)(F)F BYEAHWXPCBROCE-UHFFFAOYSA-N 0.000 claims description 9
- HEBNOKIGWWEWCN-UHFFFAOYSA-N 1,1,1,3,3,3-hexafluoropropan-2-one;hydrate Chemical compound O.FC(F)(F)C(=O)C(F)(F)F HEBNOKIGWWEWCN-UHFFFAOYSA-N 0.000 claims description 9
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 9
- UKVIEHSSVKSQBA-UHFFFAOYSA-N methane;palladium Chemical compound C.[Pd] UKVIEHSSVKSQBA-UHFFFAOYSA-N 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- 239000007791 liquid phase Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 description 10
- VBZWSGALLODQNC-UHFFFAOYSA-N hexafluoroacetone Chemical compound FC(F)(F)C(=O)C(F)(F)F VBZWSGALLODQNC-UHFFFAOYSA-N 0.000 description 9
- 238000005984 hydrogenation reaction Methods 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 238000009835 boiling Methods 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000012071 phase Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000007787 solid Substances 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 150000004677 hydrates Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- OJUUDWYPNQALHZ-UHFFFAOYSA-N 1-chloro-1,1,3,3,3-pentafluoropropan-2-one Chemical compound FC(F)(F)C(=O)C(F)(F)Cl OJUUDWYPNQALHZ-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 239000002156 adsorbate Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000004682 monohydrates Chemical class 0.000 description 1
- 229910052763 palladium Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 150000004684 trihydrates Chemical class 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58075574A JPS59204142A (ja) | 1983-04-28 | 1983-04-28 | ヘキサフルオロイソプロピルアルコ−ルの製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58075574A JPS59204142A (ja) | 1983-04-28 | 1983-04-28 | ヘキサフルオロイソプロピルアルコ−ルの製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59204142A JPS59204142A (ja) | 1984-11-19 |
| JPS6125694B2 true JPS6125694B2 (ko) | 1986-06-17 |
Family
ID=13580092
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58075574A Granted JPS59204142A (ja) | 1983-04-28 | 1983-04-28 | ヘキサフルオロイソプロピルアルコ−ルの製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59204142A (ko) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007142110A1 (ja) | 2006-06-05 | 2007-12-13 | Daikin Industries, Ltd. | 新規カルボン酸化合物、その用途及びその製造方法 |
| WO2008004466A1 (fr) | 2006-07-06 | 2008-01-10 | Daikin Industries, Ltd. | NOUVEL ESTER α-FLUOROMÉTHOXYCARBOXYLIQUE, PROCÉDÉ DE FABRICATION DE L'ESTER α-FLUOROMÉTHOXYCARBOXYLIQUE ET PROCÉDÉ DE FABRICATION DE SÉVOFLURANE |
| WO2009063783A1 (ja) | 2007-11-13 | 2009-05-22 | Daikin Industries, Ltd. | 新規カルボン酸エステル、その用途及びその製造方法 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6069047A (ja) * | 1983-09-27 | 1985-04-19 | Central Glass Co Ltd | １．１．１．３．３．３−ヘキサフルオロプロパン−２−オ−ルの製造法 |
| FR2567875B1 (fr) * | 1984-07-18 | 1986-08-08 | Atochem | Procede de synthese du trifluoro-2,2,2 ethanol et de l'alcool hexafluoro-1,1,1,3,3,3 isopropylique |
| JPH01301631A (ja) * | 1988-05-31 | 1989-12-05 | Central Glass Co Ltd | １，１，１，３，３，３−ヘキサフルオロプロパン−２−オールの製造法 |
| DE60216117T8 (de) | 2001-07-19 | 2007-08-30 | Daikin Industries, Ltd. | Verfahren zur herstellung von hexafluoraceton und dessen hydrat |
| JP5028731B2 (ja) * | 2001-09-18 | 2012-09-19 | 旭硝子株式会社 | ハロゲン化アルコ−ルの製造方法 |
| US7524995B1 (en) | 2008-06-12 | 2009-04-28 | E.I. Du Pont De Nemours And Company | Continuous process to produce hexafluoroisopropanol |
| JP5434236B2 (ja) | 2009-04-28 | 2014-03-05 | セントラル硝子株式会社 | フルオロメチルヘキサフルオロイソプロピルエーテルの製造方法 |
| JP5585291B2 (ja) * | 2010-08-12 | 2014-09-10 | セントラル硝子株式会社 | ヘキサフルオロアセトン一水和物の製造方法 |
| JP6237862B1 (ja) | 2016-11-16 | 2017-11-29 | セントラル硝子株式会社 | ヘキサフルオロイソプロパノール及び、フルオロメチル ヘキサフルオロイソプロピルエーテル（セボフルラン）の製造方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3607952A (en) * | 1969-03-28 | 1971-09-21 | Du Pont | Process for preparation of hexafluoroisopropanol |
| JPS5781424A (en) * | 1980-11-11 | 1982-05-21 | Central Glass Co Ltd | Preparation of 1,1,1,3,3,3-hexafluoropropane-2-ol |
-
1983
- 1983-04-28 JP JP58075574A patent/JPS59204142A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3607952A (en) * | 1969-03-28 | 1971-09-21 | Du Pont | Process for preparation of hexafluoroisopropanol |
| JPS5781424A (en) * | 1980-11-11 | 1982-05-21 | Central Glass Co Ltd | Preparation of 1,1,1,3,3,3-hexafluoropropane-2-ol |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007142110A1 (ja) | 2006-06-05 | 2007-12-13 | Daikin Industries, Ltd. | 新規カルボン酸化合物、その用途及びその製造方法 |
| EP2479161A1 (en) | 2006-06-05 | 2012-07-25 | Daikin Industries, Ltd. | A novel process for producing 1,1,1,3,3,3-hexafluoro-2-methoxypropane |
| WO2008004466A1 (fr) | 2006-07-06 | 2008-01-10 | Daikin Industries, Ltd. | NOUVEL ESTER α-FLUOROMÉTHOXYCARBOXYLIQUE, PROCÉDÉ DE FABRICATION DE L'ESTER α-FLUOROMÉTHOXYCARBOXYLIQUE ET PROCÉDÉ DE FABRICATION DE SÉVOFLURANE |
| WO2009063783A1 (ja) | 2007-11-13 | 2009-05-22 | Daikin Industries, Ltd. | 新規カルボン酸エステル、その用途及びその製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS59204142A (ja) | 1984-11-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPS6125694B2 (ko) | ||
| JPS638929B2 (ko) | ||
| US5523501A (en) | Catalytic hydrogenolysis | |
| JP2523753B2 (ja) | ２，３―ジクロロピリジンの製造法 | |
| JPS6069047A (ja) | １．１．１．３．３．３−ヘキサフルオロプロパン−２−オ−ルの製造法 | |
| JPH0441495A (ja) | シクロペンチルトリクロロシランの製造方法 | |
| US4164616A (en) | Production of dihydroxy alkane | |
| JP4312334B2 (ja) | インダンの製造方法 | |
| JPH0710808A (ja) | 塩素不含シクロプロパンカルボン酸メチルエステルの製造方法 | |
| JPH02279643A (ja) | イソプロピルアルコールの製造方法 | |
| JP2811065B2 (ja) | ベンジルアミンの製造法 | |
| US3364261A (en) | Preparation of cyclohexylamine from phenol | |
| JP4288451B2 (ja) | １，１，１，３，３，３−ヘキサフルオロプロパン−２−オールの製造方法 | |
| JP3904854B2 (ja) | 含フッ素脂環式ジカルボン酸化合物の製造方法 | |
| JPH11335309A (ja) | フッ素化不飽和炭化水素の製造方法 | |
| JP3682805B2 (ja) | 飽和脂肪族カルボン酸アミドの製造方法 | |
| WO2018139654A1 (ja) | １，１，２，２－テトラフルオロプロパンの製造方法 | |
| JP2738042B2 (ja) | ３，３―ジクロロ‐１，１，１，２，２，‐ペンタフルオロプロパンの製造方法 | |
| EP0149905A2 (en) | Method for the preparation of 2,2,2-trifluoroethanol | |
| CA1256452A (en) | Process for preparing aminobenzylamine | |
| JP3937186B2 (ja) | シクロプロパンカルバルデヒドの精製方法 | |
| JPH0749385B2 (ja) | ３，３，５−トリメチルシクロヘキサノンの製造方法 | |
| JPH075490B2 (ja) | １，１，１，３，３，３‐ヘキサフルオロプロパン‐２‐ｄ‐２‐オール‐ｄの製造法 | |
| JPH02121946A (ja) | コハク酸の連続製造法 | |
| JPS6094968A (ja) | デカヒドロイソキノリンの製造法 |