JPS5879818A - 結晶質ジルコニアのコロイドゾル及びその製造方法 - Google Patents
結晶質ジルコニアのコロイドゾル及びその製造方法Info
- Publication number
- JPS5879818A JPS5879818A JP17769481A JP17769481A JPS5879818A JP S5879818 A JPS5879818 A JP S5879818A JP 17769481 A JP17769481 A JP 17769481A JP 17769481 A JP17769481 A JP 17769481A JP S5879818 A JPS5879818 A JP S5879818A
- Authority
- JP
- Japan
- Prior art keywords
- zirconia
- solution
- particles
- hydrogen peroxide
- colloidal sol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 title claims abstract description 108
- 239000000843 powder Substances 0.000 title claims abstract description 19
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 46
- 239000000243 solution Substances 0.000 claims abstract description 29
- 239000002245 particle Substances 0.000 claims abstract description 26
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000007864 aqueous solution Substances 0.000 claims abstract description 13
- 150000003754 zirconium Chemical class 0.000 claims abstract description 11
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 9
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 8
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003456 ion exchange resin Substances 0.000 claims abstract description 7
- 229920003303 ion-exchange polymer Polymers 0.000 claims abstract description 7
- 238000004519 manufacturing process Methods 0.000 claims description 23
- 238000000034 method Methods 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 8
- 239000011882 ultra-fine particle Substances 0.000 claims description 8
- 239000012266 salt solution Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 abstract description 17
- IPCAPQRVQMIMAN-UHFFFAOYSA-L zirconyl chloride Chemical compound Cl[Zr](Cl)=O IPCAPQRVQMIMAN-UHFFFAOYSA-L 0.000 abstract description 12
- 239000013078 crystal Substances 0.000 abstract description 11
- 239000011369 resultant mixture Substances 0.000 abstract 2
- -1 zirconyl chloride Chemical class 0.000 abstract 1
- 239000010419 fine particle Substances 0.000 description 10
- 238000009835 boiling Methods 0.000 description 8
- 230000000694 effects Effects 0.000 description 7
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 5
- 235000011114 ammonium hydroxide Nutrition 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000001737 promoting effect Effects 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000001133 acceleration Effects 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 238000000634 powder X-ray diffraction Methods 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 230000006911 nucleation Effects 0.000 description 2
- 238000010899 nucleation Methods 0.000 description 2
- 239000011163 secondary particle Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- SPAGIJMPHSUYSE-UHFFFAOYSA-N Magnesium peroxide Chemical compound [Mg+2].[O-][O-] SPAGIJMPHSUYSE-UHFFFAOYSA-N 0.000 description 1
- 238000011276 addition treatment Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229920001429 chelating resin Polymers 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- CJNBYAVZURUTKZ-UHFFFAOYSA-N hafnium(IV) oxide Inorganic materials O=[Hf]=O CJNBYAVZURUTKZ-UHFFFAOYSA-N 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229960004995 magnesium peroxide Drugs 0.000 description 1
- 239000006224 matting agent Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 239000003495 polar organic solvent Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- PFUVRDFDKPNGAV-UHFFFAOYSA-N sodium peroxide Chemical compound [Na+].[Na+].[O-][O-] PFUVRDFDKPNGAV-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17769481A JPS5879818A (ja) | 1981-11-05 | 1981-11-05 | 結晶質ジルコニアのコロイドゾル及びその製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP17769481A JPS5879818A (ja) | 1981-11-05 | 1981-11-05 | 結晶質ジルコニアのコロイドゾル及びその製造方法 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60266830A Division JPH0764563B2 (ja) | 1985-11-27 | 1985-11-27 | 結晶質ジルコニアの微粉末及びその製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5879818A true JPS5879818A (ja) | 1983-05-13 |
| JPS6143286B2 JPS6143286B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1986-09-26 |
Family
ID=16035467
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP17769481A Granted JPS5879818A (ja) | 1981-11-05 | 1981-11-05 | 結晶質ジルコニアのコロイドゾル及びその製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5879818A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62128924A (ja) * | 1985-11-29 | 1987-06-11 | Denki Kagaku Kogyo Kk | 酸化ジルコニウム系微粉末の製法 |
| US4722833A (en) * | 1985-12-10 | 1988-02-02 | Nissan Chemical Industries, Ltd. | Fine coagulated particles of ultrafine monoclinic zirconia crystals oriented in a fiber bundle-like form and method of manufacturing them |
| JPS63156086A (ja) * | 1986-12-19 | 1988-06-29 | 日産化学工業株式会社 | セラミツクス成型物の改質法 |
| US4788045A (en) * | 1985-03-01 | 1988-11-29 | Rhone-Poulenc Specialites Chimiques | Stabilized zirconia a process for its preparation and its application in ceramic compositions |
| US4873064A (en) * | 1985-03-04 | 1989-10-10 | Nissan Chemical Industries, Ltd. | Powder of coagulated spherical zirconia particles and process for producing them |
| US5037579A (en) * | 1990-02-12 | 1991-08-06 | Nalco Chemical Company | Hydrothermal process for producing zirconia sol |
| US5223176A (en) * | 1988-09-30 | 1993-06-29 | Nissan Chemical Industries, Ltd. | Zirconia sol and method for making the same |
| US6899948B2 (en) | 1999-10-28 | 2005-05-31 | 3M Innovative Properties Company | Dental materials with nano-sized silica particles |
| EP1570999A2 (en) | 2004-03-01 | 2005-09-07 | Fuji Photo Film Co., Ltd. | Ink jet recording medium |
| WO2006115043A1 (ja) | 2005-04-18 | 2006-11-02 | Nissan Chemical Industries, Ltd. | 酸性ジルコニアゾル及びその製造方法 |
| JP2007031192A (ja) * | 2005-07-25 | 2007-02-08 | Taki Chem Co Ltd | セリア−ジルコニア固溶体ゾル及びその製造方法 |
| US7393882B2 (en) | 2002-01-31 | 2008-07-01 | 3M Innovative Properties Company | Dental pastes, dental articles, and methods |
| JP2009167085A (ja) * | 2007-12-20 | 2009-07-30 | Jgc Catalysts & Chemicals Ltd | ジルコニアゾルの製造方法 |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5889261B2 (ja) | 2013-10-18 | 2016-03-22 | 第一稀元素化学工業株式会社 | 酸化ジルコニウム−酸化チタン複合ゾル及びその製造方法 |
-
1981
- 1981-11-05 JP JP17769481A patent/JPS5879818A/ja active Granted
Non-Patent Citations (1)
| Title |
|---|
| POWDER TECHNOLOGY=1980 * |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4788045A (en) * | 1985-03-01 | 1988-11-29 | Rhone-Poulenc Specialites Chimiques | Stabilized zirconia a process for its preparation and its application in ceramic compositions |
| US4873064A (en) * | 1985-03-04 | 1989-10-10 | Nissan Chemical Industries, Ltd. | Powder of coagulated spherical zirconia particles and process for producing them |
| JPS62128924A (ja) * | 1985-11-29 | 1987-06-11 | Denki Kagaku Kogyo Kk | 酸化ジルコニウム系微粉末の製法 |
| US4722833A (en) * | 1985-12-10 | 1988-02-02 | Nissan Chemical Industries, Ltd. | Fine coagulated particles of ultrafine monoclinic zirconia crystals oriented in a fiber bundle-like form and method of manufacturing them |
| JPS63156086A (ja) * | 1986-12-19 | 1988-06-29 | 日産化学工業株式会社 | セラミツクス成型物の改質法 |
| US5223176A (en) * | 1988-09-30 | 1993-06-29 | Nissan Chemical Industries, Ltd. | Zirconia sol and method for making the same |
| US5037579A (en) * | 1990-02-12 | 1991-08-06 | Nalco Chemical Company | Hydrothermal process for producing zirconia sol |
| US6899948B2 (en) | 1999-10-28 | 2005-05-31 | 3M Innovative Properties Company | Dental materials with nano-sized silica particles |
| US7393882B2 (en) | 2002-01-31 | 2008-07-01 | 3M Innovative Properties Company | Dental pastes, dental articles, and methods |
| EP1570999A2 (en) | 2004-03-01 | 2005-09-07 | Fuji Photo Film Co., Ltd. | Ink jet recording medium |
| WO2006115043A1 (ja) | 2005-04-18 | 2006-11-02 | Nissan Chemical Industries, Ltd. | 酸性ジルコニアゾル及びその製造方法 |
| US7691910B2 (en) | 2005-04-18 | 2010-04-06 | Nissan Chemical Industries, Ltd. | Acidic zirconia sol and production method of the same |
| US8058318B2 (en) | 2005-04-18 | 2011-11-15 | Nissan Chemical Industries, Ltd. | Acidic zirconia sol and production method of the same |
| JP2007031192A (ja) * | 2005-07-25 | 2007-02-08 | Taki Chem Co Ltd | セリア−ジルコニア固溶体ゾル及びその製造方法 |
| JP2009167085A (ja) * | 2007-12-20 | 2009-07-30 | Jgc Catalysts & Chemicals Ltd | ジルコニアゾルの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6143286B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1986-09-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AU596390B2 (en) | High-dispersion sol or gel of monoclinic zirconia supermicrocrystals and production of the same | |
| JP2540880B2 (ja) | 酸化ジルコニウム微粉体の製造法 | |
| JPS5879818A (ja) | 結晶質ジルコニアのコロイドゾル及びその製造方法 | |
| US4810680A (en) | Preparation of high purity, homogeneous zirconia mixtures | |
| JP2005519020A (ja) | ナノサイズの安定化ジルコニアを製造する方法 | |
| DE3633309C2 (de) | Zusammensetzung auf der Basis von Zirkoniumdioxid und Verfahren zu ihrer Herstellung | |
| JPH0524844A (ja) | 水和ジルコニアゾルおよびジルコニア粉末の製造方法 | |
| JPH0472774B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| JP2005255450A (ja) | 酸化ジルコニウム結晶粒子とその製造方法 | |
| JPH0346407B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| JP2004051390A (ja) | 板状アルミナ粒子およびその製造方法 | |
| JP2006240928A (ja) | ジルコニア微粉末及びその製造方法 | |
| JPH0764563B2 (ja) | 結晶質ジルコニアの微粉末及びその製造方法 | |
| JPS6197134A (ja) | ジルコニア系凝集粒子粉末および製造方法 | |
| JP2528462B2 (ja) | 六チタン酸ナトリウム微細粒子粉末の製造法 | |
| JPH03141115A (ja) | 酸化イットリウム微粉末の製造方法 | |
| JPS58217430A (ja) | ジルコニア系微粉末および製造方法 | |
| JPH06321541A (ja) | ジルコニア単分散球状超微粒子粉末の製造方法 | |
| JPH0558633A (ja) | チタン酸ストロンチウムの製造方法 | |
| JPS58213633A (ja) | 酸化アルミニウムの製造方法 | |
| JPH0472775B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| JP3265597B2 (ja) | ジルコニア微粉末の製造方法 | |
| JP2882040B2 (ja) | 水和ジルコニアゾルの製造方法 | |
| JP3257095B2 (ja) | ジルコニア粉末の製造方法 | |
| JPH04367512A (ja) | 球形多孔質アナターゼ型二酸化チタン微粒子及びその製造方法 |