JPS58203940A - メタクリル酸メチルの回収方法 - Google Patents
メタクリル酸メチルの回収方法Info
- Publication number
- JPS58203940A JPS58203940A JP8723882A JP8723882A JPS58203940A JP S58203940 A JPS58203940 A JP S58203940A JP 8723882 A JP8723882 A JP 8723882A JP 8723882 A JP8723882 A JP 8723882A JP S58203940 A JPS58203940 A JP S58203940A
- Authority
- JP
- Japan
- Prior art keywords
- methanol
- organic solvent
- methyl methacrylate
- column
- azeotropic mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 238000000034 method Methods 0.000 title claims description 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 152
- 239000003960 organic solvent Substances 0.000 claims abstract description 28
- 239000000203 mixture Substances 0.000 claims abstract description 23
- 238000000926 separation method Methods 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims description 4
- -1 and distilled Chemical compound 0.000 claims description 3
- 238000004821 distillation Methods 0.000 abstract description 6
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 abstract description 4
- 239000007791 liquid phase Substances 0.000 abstract description 3
- 230000005484 gravity Effects 0.000 abstract description 2
- 238000009835 boiling Methods 0.000 abstract 2
- 239000011369 resultant mixture Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 1
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 238000010586 diagram Methods 0.000 description 4
- 238000005809 transesterification reaction Methods 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 3
- 125000001931 aliphatic group Chemical group 0.000 description 3
- 239000013040 bath agent Substances 0.000 description 3
- UWNADWZGEHDQAB-UHFFFAOYSA-N 2,5-dimethylhexane Chemical compound CC(C)CCC(C)C UWNADWZGEHDQAB-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 150000004696 coordination complex Chemical class 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229930195734 saturated hydrocarbon Natural products 0.000 description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 238000010533 azeotropic distillation Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- ZMVHTLOQSTVDFE-UHFFFAOYSA-N methanol;methyl 2-methylprop-2-enoate Chemical compound OC.COC(=O)C(C)=C ZMVHTLOQSTVDFE-UHFFFAOYSA-N 0.000 description 1
- QRMPKOFEUHIBNM-UHFFFAOYSA-N p-dimethylcyclohexane Natural products CC1CCC(C)CC1 QRMPKOFEUHIBNM-UHFFFAOYSA-N 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8723882A JPS58203940A (ja) | 1982-05-25 | 1982-05-25 | メタクリル酸メチルの回収方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP8723882A JPS58203940A (ja) | 1982-05-25 | 1982-05-25 | メタクリル酸メチルの回収方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS58203940A true JPS58203940A (ja) | 1983-11-28 |
| JPH0119374B2 JPH0119374B2 (https=) | 1989-04-11 |
Family
ID=13909238
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP8723882A Granted JPS58203940A (ja) | 1982-05-25 | 1982-05-25 | メタクリル酸メチルの回収方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS58203940A (https=) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5028735A (en) * | 1989-03-31 | 1991-07-02 | Mitsui Toatsu Chemicals, Inc. | Purification and preparation processes for methyl methacrylate |
| US5435892A (en) * | 1993-08-30 | 1995-07-25 | Mitsubishi Rayon Co., Ltd. | Process for separating methanol and methyl acrylate or methyl methacrylate |
| JPH08268938A (ja) * | 1995-03-29 | 1996-10-15 | Osaka Organic Chem Ind Ltd | アクリル酸メチルまたはメタクリル酸メチルとメタノールの分離方法 |
| JP2014043414A (ja) * | 2012-08-27 | 2014-03-13 | Osaka Organic Chem Ind Ltd | （メタ）アクリル酸エステルの製造方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2916512A (en) * | 1953-08-27 | 1959-12-08 | Celanese Corp | Esterification of acrylic acid with methanol |
| JPS579740A (en) * | 1980-06-20 | 1982-01-19 | Asahi Chem Ind Co Ltd | Purification of methyl methacrylate |
| JPS579739A (en) * | 1980-06-20 | 1982-01-19 | Asahi Chem Ind Co Ltd | Purification of methyl methacrylate |
| JPS58180457A (ja) * | 1982-03-31 | 1983-10-21 | バスフ アクチェン ゲゼルシャフト | メチルメタクリレ−ト及びメタノ−ルの水含有混合物からメタノ−ルを分離する方法 |
-
1982
- 1982-05-25 JP JP8723882A patent/JPS58203940A/ja active Granted
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2916512A (en) * | 1953-08-27 | 1959-12-08 | Celanese Corp | Esterification of acrylic acid with methanol |
| JPS579740A (en) * | 1980-06-20 | 1982-01-19 | Asahi Chem Ind Co Ltd | Purification of methyl methacrylate |
| JPS579739A (en) * | 1980-06-20 | 1982-01-19 | Asahi Chem Ind Co Ltd | Purification of methyl methacrylate |
| JPS58180457A (ja) * | 1982-03-31 | 1983-10-21 | バスフ アクチェン ゲゼルシャフト | メチルメタクリレ−ト及びメタノ−ルの水含有混合物からメタノ−ルを分離する方法 |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5028735A (en) * | 1989-03-31 | 1991-07-02 | Mitsui Toatsu Chemicals, Inc. | Purification and preparation processes for methyl methacrylate |
| US5435892A (en) * | 1993-08-30 | 1995-07-25 | Mitsubishi Rayon Co., Ltd. | Process for separating methanol and methyl acrylate or methyl methacrylate |
| JPH08268938A (ja) * | 1995-03-29 | 1996-10-15 | Osaka Organic Chem Ind Ltd | アクリル酸メチルまたはメタクリル酸メチルとメタノールの分離方法 |
| JP2014043414A (ja) * | 2012-08-27 | 2014-03-13 | Osaka Organic Chem Ind Ltd | （メタ）アクリル酸エステルの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0119374B2 (https=) | 1989-04-11 |
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