JPH0336872B2 - - Google Patents
Info
- Publication number
- JPH0336872B2 JPH0336872B2 JP59236174A JP23617484A JPH0336872B2 JP H0336872 B2 JPH0336872 B2 JP H0336872B2 JP 59236174 A JP59236174 A JP 59236174A JP 23617484 A JP23617484 A JP 23617484A JP H0336872 B2 JPH0336872 B2 JP H0336872B2
- Authority
- JP
- Japan
- Prior art keywords
- cellulosic biomass
- acetone
- temperature
- water
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002028 Biomass Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 10
- 239000003960 organic solvent Substances 0.000 claims description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 8
- 230000007935 neutral effect Effects 0.000 claims description 8
- 239000001301 oxygen Substances 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 7
- 239000011261 inert gas Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 37
- 239000007788 liquid Substances 0.000 description 15
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 14
- 239000002023 wood Substances 0.000 description 13
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 12
- 235000013312 flour Nutrition 0.000 description 10
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 8
- 229910052786 argon Inorganic materials 0.000 description 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 244000184734 Pyrus japonica Species 0.000 description 6
- 241000219492 Quercus Species 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 229910000027 potassium carbonate Inorganic materials 0.000 description 6
- 235000011181 potassium carbonates Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000012263 liquid product Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000001913 cellulose Substances 0.000 description 3
- 229920002678 cellulose Polymers 0.000 description 3
- 239000000446 fuel Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 241001480065 Quercus serrata Species 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 239000013064 chemical raw material Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- 241000609240 Ambelania acida Species 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
- 239000004280 Sodium formate Substances 0.000 description 1
- WZSHAZVYZXZOPZ-UHFFFAOYSA-L [Ca+2].[Ar].C([O-])([O-])=O Chemical compound [Ca+2].[Ar].C([O-])([O-])=O WZSHAZVYZXZOPZ-UHFFFAOYSA-L 0.000 description 1
- JPTQGBTXAMWSMU-UHFFFAOYSA-L [Na+].[Ar].C([O-])([O-])=O.[Na+] Chemical compound [Na+].[Ar].C([O-])([O-])=O.[Na+] JPTQGBTXAMWSMU-UHFFFAOYSA-L 0.000 description 1
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000010905 bagasse Substances 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 235000011116 calcium hydroxide Nutrition 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 235000012255 calcium oxide Nutrition 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000010893 paper waste Substances 0.000 description 1
- 239000003415 peat Substances 0.000 description 1
- 239000011736 potassium bicarbonate Substances 0.000 description 1
- 229910000028 potassium bicarbonate Inorganic materials 0.000 description 1
- 235000015497 potassium bicarbonate Nutrition 0.000 description 1
- WFIZEGIEIOHZCP-UHFFFAOYSA-M potassium formate Chemical compound [K+].[O-]C=O WFIZEGIEIOHZCP-UHFFFAOYSA-M 0.000 description 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 1
- 229940086066 potassium hydrogencarbonate Drugs 0.000 description 1
- 235000011118 potassium hydroxide Nutrition 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 description 1
- 235000019254 sodium formate Nutrition 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/04—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Processing Of Solid Wastes (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59236174A JPS61115994A (ja) | 1984-11-09 | 1984-11-09 | セルロ−ス系バイオマスの液化方法 |
| US06/873,257 US4935567A (en) | 1984-11-09 | 1986-06-06 | Process for liquefying cellulose-containing biomass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59236174A JPS61115994A (ja) | 1984-11-09 | 1984-11-09 | セルロ−ス系バイオマスの液化方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61115994A JPS61115994A (ja) | 1986-06-03 |
| JPH0336872B2 true JPH0336872B2 (enFirst) | 1991-06-03 |
Family
ID=16996862
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59236174A Granted JPS61115994A (ja) | 1984-11-09 | 1984-11-09 | セルロ−ス系バイオマスの液化方法 |
Country Status (2)
| Country | Link |
|---|---|
| US (1) | US4935567A (enFirst) |
| JP (1) | JPS61115994A (enFirst) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009014225A1 (ja) | 2007-07-25 | 2009-01-29 | Toyota Jidosha Kabushiki Kaisha | バイオマスを原料とする液化燃料油の製造方法 |
Families Citing this family (48)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0629438B2 (ja) * | 1988-10-07 | 1994-04-20 | 工業技術院長 | セルロース系バイオマスの液化方法 |
| US5264623A (en) * | 1993-01-04 | 1993-11-23 | Energy Mines & Resources Canada | Method of producing calcium salts from biomass |
| DE19742266A1 (de) * | 1997-09-25 | 1999-05-06 | Ludger Dr Steinmann | Aufwertung von Chemie- und Energierohstoffen durch Reaktion mit geringwertigen Rohstoffen |
| EP1268717A4 (en) * | 2000-03-23 | 2004-03-17 | Univ West Virginia | METHOD FOR CONVERTING AGRICULTURAL WASTE IN LIQUID FUEL AND RELATED DEVICE |
| AU2003261191A1 (en) * | 2002-07-26 | 2004-02-16 | Regents Of The University Of Minnesota | Methods for producing biopolymers |
| AU2012202587B2 (en) * | 2005-04-29 | 2014-10-09 | Altaca Insaat Ve Dis Ticaret A.S. | Method and apparatus for converting organic material |
| US7678163B2 (en) * | 2005-04-29 | 2010-03-16 | Scf Technologies A/S | Method and apparatus for converting organic material |
| US8299315B2 (en) * | 2005-04-29 | 2012-10-30 | Altaca Insaat Ve Dis Ticaret A.S. | Method and apparatus for converting organic material |
| US20070022653A1 (en) * | 2005-08-01 | 2007-02-01 | Gokel Dean E | Method and system for efficiently disposing of dead animal parts and for converting animal parts and biomass to fuels |
| US20070227062A1 (en) * | 2006-03-30 | 2007-10-04 | West Virginia University | Method of converting animal waste into a multi-phase fuel |
| DE102006016684A1 (de) * | 2006-04-08 | 2007-10-11 | Forschungszentrum Karlsruhe Gmbh | Verfahren zur Verflüssigung von Biomasse |
| US20080209796A1 (en) * | 2007-01-09 | 2008-09-04 | Stiller Alfred H | Method of converting animal waste inot a multi-phase fuel |
| US20080274022A1 (en) * | 2007-05-04 | 2008-11-06 | Boykin Jack W | Combined reactor and method for the production of synthetic fuels |
| US8158842B2 (en) * | 2007-06-15 | 2012-04-17 | Uop Llc | Production of chemicals from pyrolysis oil |
| US7960520B2 (en) * | 2007-06-15 | 2011-06-14 | Uop Llc | Conversion of lignocellulosic biomass to chemicals and fuels |
| US8013195B2 (en) * | 2007-06-15 | 2011-09-06 | Uop Llc | Enhancing conversion of lignocellulosic biomass |
| JP2011529091A (ja) * | 2008-07-28 | 2011-12-01 | チャイナ フューエル バイオエナジー テクノロジー デベロップメント コーポレイティッド リミテッド | セルロースバイオマスの直接液化方法 |
| US8653312B2 (en) | 2009-06-05 | 2014-02-18 | Toyota Jidosha Kabushiki Kaisha | Method for producing water-insoluble liquefied fuel oil from biomass |
| US8022257B2 (en) * | 2009-09-03 | 2011-09-20 | The Ohio State University Research Foundation | Methods for producing polyols using crude glycerin |
| NZ603011A (en) | 2010-04-07 | 2015-07-31 | Licella Pty Ltd | Methods for biofuel production |
| CN103124780A (zh) * | 2010-07-07 | 2013-05-29 | 凯奇莱特能源有限公司 | 溶剂增强的生物质液化 |
| CN101962562B (zh) * | 2010-10-08 | 2013-05-15 | 华东理工大学 | 一种木醋液在制备燃料油中的应用 |
| BR112013031803A2 (pt) * | 2011-06-10 | 2017-01-31 | Steeper Energy Aps | processo e aparelho para a produção de hidrocarbonetos líquidos |
| US9758729B2 (en) | 2011-06-10 | 2017-09-12 | Steeper Energy Aps | Process and apparatus for producing liquid hydrocarbon |
| JP5803860B2 (ja) * | 2011-09-16 | 2015-11-04 | 新日鐵住金株式会社 | バイオマスの改質方法、バイオマス及び褐炭の改質方法、コークス及び焼結鉱の製造方法並びに高炉の操業方法 |
| AU2012332804B2 (en) * | 2011-10-31 | 2015-08-20 | Shell Internationale Research Maatschappij B.V. | Process to produce biofuels via organic phase thermal hydrocatalytic treatment of biomass |
| US8921629B2 (en) | 2011-10-31 | 2014-12-30 | Shell Oil Company | Process to produce biofuels via organic phase thermal hydrocatalytic treatment of biomass |
| TWI462778B (zh) | 2011-12-06 | 2014-12-01 | Ind Tech Res Inst | 生質物的液化方法與有機銨鹽溶液用於將生質物液化的用途 |
| AU2011383243B2 (en) * | 2011-12-16 | 2015-09-10 | Shell Internationale Research Maatschappij B.V. | Biomass conversion systems having a fluid circulation loop containing a separation mechanism consisting in a cyclone for control of cellulosis fines and methods for use thereof |
| ES2412241B1 (es) * | 2012-03-22 | 2014-01-28 | Eduardo Pérez Lebeña | Método de licuefacción de biomasa lignocelulósica e instalación para realizar dicho método |
| JP6274478B2 (ja) * | 2012-07-11 | 2018-02-07 | 出光興産株式会社 | リグニン分解物の製造方法 |
| EP2890767A1 (en) | 2012-08-30 | 2015-07-08 | Steeper Energy ApS | Improved method for controlling cleaning of an apparatus for producing liquid hydrocarbons |
| WO2014032671A1 (en) | 2012-08-30 | 2014-03-06 | Steeper Energy Aps | Improved method for preparing start up of process and equipment for producing liquid hydrocarbons |
| MY173178A (en) | 2012-08-30 | 2020-01-02 | Steeper Energy Aps | Improved method for preparing shut down of process and equipment for producing liquid hydrocarbons |
| CN103387840B (zh) * | 2013-06-27 | 2015-07-08 | 中国矿业大学 | 一种秸秆分级催化液化制备生物油的方法 |
| PT107143B (pt) * | 2013-09-05 | 2020-04-22 | Inst Superior Tecnico | Colas poliméricas naturais de base aquosa, de dois componentes, obtidas a partir de derivados da cortiça |
| CA2931672C (en) * | 2013-11-27 | 2022-04-12 | Kat2Biz Ab | Depolymerisation of lignin in biomass |
| WO2015135046A1 (pt) * | 2014-03-13 | 2015-09-17 | Petróleo Brasileiro S.A. - Petrobras | Processo de obtenção de bio-óleo solúvel em hidrocarbonetos |
| US10428276B2 (en) | 2014-05-05 | 2019-10-01 | Steeper Energy Aps | Feed mixture for producing hydrocarbons |
| JP6692024B2 (ja) * | 2014-07-30 | 2020-05-13 | 出光興産株式会社 | ペンタノールの製造方法 |
| CN109328224A (zh) * | 2016-06-24 | 2019-02-12 | 西安大略大学 | 木质纤维素生物质至具有受控分子量的生物油的水热液化 |
| CA2935825A1 (en) | 2016-07-11 | 2018-01-11 | Steeper Energy Aps | Process for producing low sulphur renewable oil |
| CA3082681C (en) * | 2016-10-27 | 2023-07-04 | The University Of Western Ontario | Hydrothermal liquefaction co-processing of wastewater sludge and lignocellulosic biomass for co-production of bio-gas and bio-oils |
| BR112020008915A2 (pt) | 2017-11-07 | 2020-10-20 | Kiram Ab | processo para produção de um singás. |
| MY208134A (en) | 2017-11-10 | 2025-04-17 | Steeper Energy Aps | Recovery system for high pressure processing system |
| US10392565B2 (en) * | 2017-12-14 | 2019-08-27 | Savannah River Nuclear Solutions, Llc | Conversion of biomass by efficient base-catalyzed decarboxylation reaction |
| FI129548B2 (en) * | 2020-06-26 | 2025-11-25 | Upm Kymmene Corp | Controlling hydrothermal liquefaction |
| WO2023002453A1 (es) * | 2021-07-22 | 2023-01-26 | Cementos Argos S.A. | Proceso de licuefacción solvotérmica para producción de biocrudo a partir de biomasa |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2177557A (en) * | 1937-02-24 | 1939-10-24 | Method of treating wood or lignine | |
| US2551579A (en) * | 1944-06-30 | 1951-05-08 | Berl Walter George | Production of valuable organic compounds from plant material |
| DE2737118A1 (de) * | 1977-08-17 | 1979-03-01 | Projektierung Chem Verfahrenst | Verfahren zur gewinnung von zuckern, gegebenenfalls cellulose und gegebenenfalls lignin aus lignocellulosischen pflanzlichen rohstoffen |
| CA1100266A (en) * | 1977-08-31 | 1981-05-05 | Laszlo Paszner | Organosolv delignification and saccharification process for lignocellulosic plant materials |
| DD154451A3 (de) * | 1980-05-12 | 1982-03-24 | Mihalne Atomyr | Verfahren zur herstellung von zellstoff aus einjahrespflanzen,insbesondere stroh |
| US4470851A (en) * | 1981-03-26 | 1984-09-11 | Laszlo Paszner | High efficiency organosolv saccharification process |
-
1984
- 1984-11-09 JP JP59236174A patent/JPS61115994A/ja active Granted
-
1986
- 1986-06-06 US US06/873,257 patent/US4935567A/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009014225A1 (ja) | 2007-07-25 | 2009-01-29 | Toyota Jidosha Kabushiki Kaisha | バイオマスを原料とする液化燃料油の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| US4935567A (en) | 1990-06-19 |
| JPS61115994A (ja) | 1986-06-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |