JPH0225864B2 - - Google Patents
Info
- Publication number
- JPH0225864B2 JPH0225864B2 JP61110864A JP11086486A JPH0225864B2 JP H0225864 B2 JPH0225864 B2 JP H0225864B2 JP 61110864 A JP61110864 A JP 61110864A JP 11086486 A JP11086486 A JP 11086486A JP H0225864 B2 JPH0225864 B2 JP H0225864B2
- Authority
- JP
- Japan
- Prior art keywords
- mol
- powder
- tio
- sintered body
- zro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 32
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 26
- 238000004519 manufacturing process Methods 0.000 claims description 23
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 14
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 10
- 239000001301 oxygen Substances 0.000 claims description 10
- 229910052760 oxygen Inorganic materials 0.000 claims description 10
- 229910052746 lanthanum Inorganic materials 0.000 claims description 7
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 7
- 229910001404 rare earth metal oxide Inorganic materials 0.000 claims description 7
- 239000012298 atmosphere Substances 0.000 claims description 4
- 238000010304 firing Methods 0.000 claims description 4
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 239000012300 argon atmosphere Substances 0.000 claims 1
- 239000000843 powder Substances 0.000 description 51
- 238000002834 transmittance Methods 0.000 description 13
- 239000002245 particle Substances 0.000 description 12
- 238000005245 sintering Methods 0.000 description 10
- 238000012360 testing method Methods 0.000 description 8
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000002994 raw material Substances 0.000 description 6
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- OBOSXEWFRARQPU-UHFFFAOYSA-N 2-n,2-n-dimethylpyridine-2,5-diamine Chemical compound CN(C)C1=CC=C(N)C=N1 OBOSXEWFRARQPU-UHFFFAOYSA-N 0.000 description 2
- 229910017493 Nd 2 O 3 Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000000149 argon plasma sintering Methods 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000001000 micrograph Methods 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 239000006104 solid solution Substances 0.000 description 2
- MBULCFMSBDQQQT-UHFFFAOYSA-N (3-carboxy-2-hydroxypropyl)-trimethylazanium;2,4-dioxo-1h-pyrimidine-6-carboxylate Chemical compound C[N+](C)(C)CC(O)CC(O)=O.[O-]C(=O)C1=CC(=O)NC(=O)N1 MBULCFMSBDQQQT-UHFFFAOYSA-N 0.000 description 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000005253 cladding Methods 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000008094 contradictory effect Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000012769 display material Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- -1 titanium alkoxide Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/876,410 US4758541A (en) | 1985-06-20 | 1986-06-20 | Zirconia sintered body of improved light transmittance |
| EP86304759A EP0206780B1 (en) | 1985-06-20 | 1986-06-20 | Zirconia sintered body of improved light transmittance |
| DE8686304759T DE3683959D1 (de) | 1985-06-20 | 1986-06-20 | Zirkoniumdioxidsinterkoerper mit verbesserter lichtdurchlaessigkeit. |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60-132971 | 1985-06-20 | ||
| JP13297185 | 1985-06-20 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6291467A JPS6291467A (ja) | 1987-04-25 |
| JPH0225864B2 true JPH0225864B2 (ru) | 1990-06-06 |
Family
ID=15093774
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61110864A Granted JPS6291467A (ja) | 1985-06-20 | 1986-05-16 | 透光性ジルコニア焼結体の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6291467A (ru) |
Families Citing this family (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2616773B2 (ja) * | 1987-05-22 | 1997-06-04 | 株式会社デンソー | ジルコニアセラミックスの製造方法 |
| JP2616772B2 (ja) * | 1987-05-22 | 1997-06-04 | 株式会社デンソー | プロトン導電性セラミックスの製造方法 |
| JP2607519B2 (ja) * | 1987-05-26 | 1997-05-07 | 株式会社デンソー | 光学セラミックスの製造方法 |
| JP2608558B2 (ja) * | 1987-05-26 | 1997-05-07 | 株式会社デンソー | 光学セラミックスの製造方法 |
| JP2607520B2 (ja) * | 1987-05-26 | 1997-05-07 | 株式会社デンソー | 光学セラミックスの製造方法 |
| JP2607518B2 (ja) * | 1987-05-26 | 1997-05-07 | 株式会社デンソー | 光学セラミックスの製造方法 |
| CN100418919C (zh) | 2000-12-20 | 2008-09-17 | 株式会社村田制作所 | 透光性陶瓷及其制造方法和光学元件 |
| JP2007108734A (ja) * | 2005-09-21 | 2007-04-26 | Schott Ag | 光学素子及び同光学素子から成る撮像光学素子 |
| JP5125065B2 (ja) | 2006-02-17 | 2013-01-23 | 東ソー株式会社 | 透明ジルコニア焼結体 |
| EP2045222B1 (en) * | 2006-07-25 | 2015-09-23 | Tosoh Corporation | Sintered zirconia having high light transmission and high strength, use of the same and process for production thereof |
| EP2263988B1 (en) | 2008-04-09 | 2016-03-30 | Tosoh Corporation | Light-transmitting sintered zirconia compact, process for producing the same, and use thereof |
| JP5325518B2 (ja) | 2008-07-22 | 2013-10-23 | ショット アクチエンゲゼルシャフト | 透明セラミック及びその製造方法ならびにその透明セラミックスを用いた光学素子 |
| WO2010140644A1 (ja) * | 2009-06-04 | 2010-12-09 | 東ソー株式会社 | 高強度透明ジルコニア焼結体及びその製造方法、並びにその用途 |
| JP5505063B2 (ja) * | 2009-06-04 | 2014-05-28 | 東ソー株式会社 | 高透明ジルコニア焼結体 |
| EP2463257B1 (en) | 2009-08-07 | 2018-06-06 | Tosoh Corporation | Transparent zirconia sintered body and method for producing same |
| JP5770431B2 (ja) * | 2009-10-16 | 2015-08-26 | 東ソー株式会社 | 高強度透明ジルコニア焼結体 |
| US9249057B2 (en) | 2010-03-09 | 2016-02-02 | Tosoh Corporation | Red light transmitting zirconia sintered body, method for producing the same, member comprising the sintered body, and jewelry goods and exterior component using the member |
| JP5655512B2 (ja) * | 2010-11-05 | 2015-01-21 | 東ソー株式会社 | 着色透光性ジルコニア焼結体及びその製造方法並びにその用途 |
| JP5861397B2 (ja) * | 2010-11-11 | 2016-02-16 | 東ソー株式会社 | 着色透光性ジルコニア焼結体及びその製造方法並びにその用途 |
| DE112013006623T5 (de) * | 2013-02-08 | 2015-10-22 | Shin-Etsu Chemical Co., Ltd. | Herstellungsverfahren für einen lichtdurchlässigen Metalloxidsinterkörper und lichtdurchlässiger Metalloxidsinterkörper |
| JP6340879B2 (ja) * | 2013-04-10 | 2018-06-13 | 東ソー株式会社 | ジルコニア焼結体及びその製造方法 |
| JP6340880B2 (ja) * | 2014-04-01 | 2018-06-13 | 東ソー株式会社 | ジルコニア焼結体及びその製造法 |
| JP6326363B2 (ja) * | 2014-12-22 | 2018-05-16 | クラレノリタケデンタル株式会社 | ジルコニア組成物、ジルコニア仮焼体、ジルコニア焼結体及びジルコニア焼結体の製造方法、並びに歯科用製品 |
| CN107108374B (zh) | 2015-01-15 | 2021-02-02 | 东曹株式会社 | 透光性氧化锆烧结体和其制造方法以及其用途 |
| JP6698417B2 (ja) * | 2016-04-27 | 2020-05-27 | 京セラ株式会社 | ビーム検出用の蛍光性ジルコニア材の製造方法 |
| JP7473094B2 (ja) * | 2022-01-18 | 2024-04-23 | 東ソー株式会社 | 焼結体及びその製造方法 |
-
1986
- 1986-05-16 JP JP61110864A patent/JPS6291467A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6291467A (ja) | 1987-04-25 |
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