JPH0150272B2 - - Google Patents
Info
- Publication number
- JPH0150272B2 JPH0150272B2 JP56054305A JP5430581A JPH0150272B2 JP H0150272 B2 JPH0150272 B2 JP H0150272B2 JP 56054305 A JP56054305 A JP 56054305A JP 5430581 A JP5430581 A JP 5430581A JP H0150272 B2 JPH0150272 B2 JP H0150272B2
- Authority
- JP
- Japan
- Prior art keywords
- pitch
- raw material
- temperature
- carbonization
- heat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002994 raw material Substances 0.000 claims description 36
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 30
- 239000004917 carbon fiber Substances 0.000 claims description 30
- 238000010438 heat treatment Methods 0.000 claims description 20
- 238000003763 carbonization Methods 0.000 claims description 16
- 239000002243 precursor Substances 0.000 claims description 16
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 14
- 238000011282 treatment Methods 0.000 claims description 14
- 239000000295 fuel oil Substances 0.000 claims description 11
- 238000005087 graphitization Methods 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- 238000002074 melt spinning Methods 0.000 claims description 8
- 239000003208 petroleum Substances 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 7
- 150000004678 hydrides Chemical class 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 5
- 238000000354 decomposition reaction Methods 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 239000011295 pitch Substances 0.000 description 69
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 25
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 10
- 208000012886 Vertigo Diseases 0.000 description 9
- 238000009987 spinning Methods 0.000 description 9
- 239000003921 oil Substances 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 239000000835 fiber Substances 0.000 description 6
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 5
- 239000011302 mesophase pitch Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000004231 fluid catalytic cracking Methods 0.000 description 4
- 239000011261 inert gas Substances 0.000 description 4
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
- 230000002411 adverse Effects 0.000 description 3
- 239000012298 atmosphere Substances 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000004973 liquid crystal related substance Substances 0.000 description 3
- 230000001590 oxidative effect Effects 0.000 description 3
- 229920002239 polyacrylonitrile Polymers 0.000 description 3
- NHCREQREVZBOCH-UHFFFAOYSA-N 1-methyl-1,2,3,4,4a,5,6,7,8,8a-decahydronaphthalene Chemical compound C1CCCC2C(C)CCCC21 NHCREQREVZBOCH-UHFFFAOYSA-N 0.000 description 2
- YBYIRNPNPLQARY-UHFFFAOYSA-N 1H-indene Chemical compound C1=CC=C2CC=CC2=C1 YBYIRNPNPLQARY-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 238000004523 catalytic cracking Methods 0.000 description 2
- 239000011294 coal tar pitch Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- -1 decahydrobiphenyl Chemical compound 0.000 description 2
- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 description 2
- XXPBFNVKTVJZKF-UHFFFAOYSA-N dihydrophenanthrene Natural products C1=CC=C2CCC3=CC=CC=C3C2=C1 XXPBFNVKTVJZKF-UHFFFAOYSA-N 0.000 description 2
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- PQNFLJBBNBOBRQ-UHFFFAOYSA-N indane Chemical compound C1=CC=C2CCCC2=C1 PQNFLJBBNBOBRQ-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- YNPNZTXNASCQKK-UHFFFAOYSA-N phenanthrene Chemical compound C1=CC=C2C3=CC=CC=C3C=CC2=C1 YNPNZTXNASCQKK-UHFFFAOYSA-N 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000005979 thermal decomposition reaction Methods 0.000 description 2
- 238000009423 ventilation Methods 0.000 description 2
- BDAGIAXQQBRORQ-UHFFFAOYSA-N 1,2,3,3a,4,5-hexahydroacenaphthylene Chemical compound C1CCC2CCC3=CC=CC1=C32 BDAGIAXQQBRORQ-UHFFFAOYSA-N 0.000 description 1
- ARPANWHHRGVXBN-UHFFFAOYSA-N 1,2,3,4,4a,10-hexahydroanthracene Chemical compound C1=CC=C2CC(CCCC3)C3=CC2=C1 ARPANWHHRGVXBN-UHFFFAOYSA-N 0.000 description 1
- GNMCGMFNBARSIY-UHFFFAOYSA-N 1,2,3,4,4a,4b,5,6,7,8,8a,9,10,10a-tetradecahydrophenanthrene Chemical compound C1CCCC2C3CCCCC3CCC21 GNMCGMFNBARSIY-UHFFFAOYSA-N 0.000 description 1
- JSGPEEFAPXBVCG-UHFFFAOYSA-N 1,2,3,4,4a,4b,5,6,7,8,8a,9-dodecahydrophenanthrene Chemical compound C1CCCC2C3CCCCC3CC=C21 JSGPEEFAPXBVCG-UHFFFAOYSA-N 0.000 description 1
- PJDWNSYGMXODTB-UHFFFAOYSA-N 1,2,3,4,4a,4b,5,6-octahydrophenanthrene Chemical compound C1=CCCC2C(CCCC3)C3=CC=C21 PJDWNSYGMXODTB-UHFFFAOYSA-N 0.000 description 1
- MPUIANDHWHNPJY-UHFFFAOYSA-N 1,2,3,4,4a,4b-hexahydrophenanthrene Chemical compound C1=CC=CC2C(CCCC3)C3=CC=C21 MPUIANDHWHNPJY-UHFFFAOYSA-N 0.000 description 1
- VTIBBOHXBURHMD-UHFFFAOYSA-N 1,2,3,4,4a,5,10,10a-octahydroanthracene Chemical compound C1=CCC2CC(CCCC3)C3=CC2=C1 VTIBBOHXBURHMD-UHFFFAOYSA-N 0.000 description 1
- GVJFFQYXVOJXFI-UHFFFAOYSA-N 1,2,3,4,4a,5,6,7,8,8a,9,9a,10,10a-tetradecahydroanthracene Chemical compound C1C2CCCCC2CC2C1CCCC2 GVJFFQYXVOJXFI-UHFFFAOYSA-N 0.000 description 1
- SJXINMCGKMERBY-UHFFFAOYSA-N 1,2,3,4,4a,5,6,7,8,8a,9,9a-dodecahydroanthracene Chemical compound C1=C2CCCCC2CC2C1CCCC2 SJXINMCGKMERBY-UHFFFAOYSA-N 0.000 description 1
- PUNXVEAWLAVABA-UHFFFAOYSA-N 1,2,3,4-tetrahydroanthracene;1,2,5,6-tetrahydroanthracene Chemical compound C1=CC=C2C=C(CCCC3)C3=CC2=C1.C1=CCCC2=C1C=C1CCC=CC1=C2 PUNXVEAWLAVABA-UHFFFAOYSA-N 0.000 description 1
- UXNCDAQNSQBHEN-UHFFFAOYSA-N 1,2,3,4-tetrahydrophenanthrene Chemical compound C1=CC2=CC=CC=C2C2=C1CCCC2 UXNCDAQNSQBHEN-UHFFFAOYSA-N 0.000 description 1
- AXLCNVVQTVIXDG-UHFFFAOYSA-N 1-ethyl-1,2,3,4-tetrahydronaphthalene Chemical compound C1=CC=C2C(CC)CCCC2=C1 AXLCNVVQTVIXDG-UHFFFAOYSA-N 0.000 description 1
- APBBTKKLSNPFDP-UHFFFAOYSA-N 1-methyl-1,2,3,4-tetrahydronaphthalene Chemical compound C1=CC=C2C(C)CCCC2=C1 APBBTKKLSNPFDP-UHFFFAOYSA-N 0.000 description 1
- XSRADQOBRZHEOB-UHFFFAOYSA-N 1-methyl-1,2-dihydroacenaphthylene Chemical compound C1=CC(C(C)C2)=C3C2=CC=CC3=C1 XSRADQOBRZHEOB-UHFFFAOYSA-N 0.000 description 1
- LRCMZPVVFRECQR-UHFFFAOYSA-N 1-propan-2-yl-1,2,3,4-tetrahydronaphthalene Chemical compound C1=CC=C2C(C(C)C)CCCC2=C1 LRCMZPVVFRECQR-UHFFFAOYSA-N 0.000 description 1
- ABIPNDAVRBMCHV-UHFFFAOYSA-N 4,4-dimethyl-2,3-dihydro-1h-naphthalene Chemical compound C1=CC=C2C(C)(C)CCCC2=C1 ABIPNDAVRBMCHV-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- XBDYBAVJXHJMNQ-UHFFFAOYSA-N Tetrahydroanthracene Natural products C1=CC=C2C=C(CCCC3)C3=CC2=C1 XBDYBAVJXHJMNQ-UHFFFAOYSA-N 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- CWRYPZZKDGJXCA-UHFFFAOYSA-N acenaphthene Chemical compound C1=CC(CC2)=C3C2=CC=CC3=C1 CWRYPZZKDGJXCA-UHFFFAOYSA-N 0.000 description 1
- 125000004054 acenaphthylenyl group Chemical group C1(=CC2=CC=CC3=CC=CC1=C23)* 0.000 description 1
- HXGDTGSAIMULJN-UHFFFAOYSA-N acetnaphthylene Natural products C1=CC(C=C2)=C3C2=CC=CC3=C1 HXGDTGSAIMULJN-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000005273 aeration Methods 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000010000 carbonizing Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000011280 coal tar Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000007380 fibre production Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- 229910052811 halogen oxide Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000003350 kerosene Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000011301 petroleum pitch Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 150000003248 quinolines Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000011318 synthetic pitch Substances 0.000 description 1
- PXXNTAGJWPJAGM-UHFFFAOYSA-N vertaline Natural products C1C2C=3C=C(OC)C(OC)=CC=3OC(C=C3)=CC=C3CCC(=O)OC1CC1N2CCCC1 PXXNTAGJWPJAGM-UHFFFAOYSA-N 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P30/00—Technologies relating to oil refining and petrochemical industry
- Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
Landscapes
- Carbon And Carbon Compounds (AREA)
- Working-Up Tar And Pitch (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Inorganic Fibers (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56054305A JPS57168988A (en) | 1981-04-13 | 1981-04-13 | Raw pitch for carbon fiber |
| US06/366,937 US4521294A (en) | 1981-04-13 | 1982-04-09 | Starting pitches for carbon fibers |
| EP82301912A EP0063052B1 (en) | 1981-04-13 | 1982-04-13 | Starting pitches for carbon fibers |
| DE8282301912T DE3272976D1 (en) | 1981-04-13 | 1982-04-13 | Starting pitches for carbon fibers |
| CA000400889A CA1181708A (en) | 1981-04-13 | 1982-04-13 | Starting pitches for carbon fibers |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56054305A JPS57168988A (en) | 1981-04-13 | 1981-04-13 | Raw pitch for carbon fiber |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS57168988A JPS57168988A (en) | 1982-10-18 |
| JPH0150272B2 true JPH0150272B2 (zh) | 1989-10-27 |
Family
ID=12966853
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP56054305A Granted JPS57168988A (en) | 1981-04-13 | 1981-04-13 | Raw pitch for carbon fiber |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS57168988A (zh) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014227545A (ja) * | 2013-05-27 | 2014-12-08 | ジーエス カルテックス コーポレイション | 炭素繊維用ピッチの製造方法 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5829885A (ja) * | 1981-08-18 | 1983-02-22 | Mitsubishi Oil Co Ltd | 炭素繊維原料用ピツチの製造法 |
| JPS5876523A (ja) * | 1981-10-29 | 1983-05-09 | Nippon Oil Co Ltd | ピツチ系炭素繊維の製造方法 |
| JPS58115120A (ja) * | 1981-12-28 | 1983-07-08 | Nippon Oil Co Ltd | ピツチ系炭素繊維の製造方法 |
| JPS59136383A (ja) * | 1983-01-26 | 1984-08-04 | Agency Of Ind Science & Technol | 炭素繊維製造用ピツチの調製方法 |
| JPS59136384A (ja) * | 1983-01-26 | 1984-08-04 | Agency Of Ind Science & Technol | 炭素繊維用ピツチの製造法 |
| JPS59147081A (ja) * | 1983-02-14 | 1984-08-23 | Nippon Oil Co Ltd | 炭素繊維の製造方法 |
| JPS59155493A (ja) * | 1983-02-23 | 1984-09-04 | Mitsubishi Petrochem Co Ltd | メソフエ−ズピツチの製造方法 |
| JPS61241392A (ja) * | 1985-12-26 | 1986-10-27 | Toa Nenryo Kogyo Kk | メソ相ピツチの製造方法 |
| CN116096839A (zh) * | 2020-09-03 | 2023-05-09 | 株式会社力森诺科 | 沥青的制造方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS585227A (ja) * | 1981-07-03 | 1983-01-12 | Teijin Ltd | 易接着性ポリエステルフイルムの製造法 |
-
1981
- 1981-04-13 JP JP56054305A patent/JPS57168988A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS585227A (ja) * | 1981-07-03 | 1983-01-12 | Teijin Ltd | 易接着性ポリエステルフイルムの製造法 |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014227545A (ja) * | 2013-05-27 | 2014-12-08 | ジーエス カルテックス コーポレイション | 炭素繊維用ピッチの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS57168988A (en) | 1982-10-18 |
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