JP7475917B2 - ダニ用忌避剤及びこれを用いるダニの忌避方法 - Google Patents
ダニ用忌避剤及びこれを用いるダニの忌避方法 Download PDFInfo
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- JP7475917B2 JP7475917B2 JP2020054554A JP2020054554A JP7475917B2 JP 7475917 B2 JP7475917 B2 JP 7475917B2 JP 2020054554 A JP2020054554 A JP 2020054554A JP 2020054554 A JP2020054554 A JP 2020054554A JP 7475917 B2 JP7475917 B2 JP 7475917B2
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- Prior art keywords
- repellent
- house dust
- mites
- oil
- mite repellent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000005871 repellent Substances 0.000 title claims description 89
- 230000002940 repellent Effects 0.000 title claims description 89
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- -1 aromatic ketone compound Chemical class 0.000 claims description 26
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- VXSIXFKKSNGRRO-MXOVTSAMSA-N [(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate;[(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-3-[(e)-3-methoxy-2-methyl-3-oxoprop-1-enyl Chemical class CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1.CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VXSIXFKKSNGRRO-MXOVTSAMSA-N 0.000 claims description 3
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- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 description 1
- 229940029339 inulin Drugs 0.000 description 1
- 230000001678 irradiating effect Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- VJCLZQUHGQSTMZ-UHFFFAOYSA-N isothiocyanatoethene Chemical compound C=CN=C=S VJCLZQUHGQSTMZ-UHFFFAOYSA-N 0.000 description 1
- NZKIRHFOLVYKFT-VUMXUWRFSA-N jasmolin I Chemical compound C1C(=O)C(C\C=C/CC)=C(C)[C@H]1OC(=O)[C@H]1C(C)(C)[C@@H]1C=C(C)C NZKIRHFOLVYKFT-VUMXUWRFSA-N 0.000 description 1
- WKNSDDMJXANVMK-XIGJTORUSA-N jasmolin II Chemical compound C1C(=O)C(C\C=C/CC)=C(C)[C@H]1OC(=O)[C@H]1C(C)(C)[C@@H]1\C=C(/C)C(=O)OC WKNSDDMJXANVMK-XIGJTORUSA-N 0.000 description 1
- WKNSDDMJXANVMK-UHFFFAOYSA-N jasmolin II Natural products C1C(=O)C(CC=CCC)=C(C)C1OC(=O)C1C(C)(C)C1C=C(C)C(=O)OC WKNSDDMJXANVMK-UHFFFAOYSA-N 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 239000000711 locust bean gum Chemical class 0.000 description 1
- 235000010420 locust bean gum Nutrition 0.000 description 1
- 229960000453 malathion Drugs 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229940041616 menthol Drugs 0.000 description 1
- 229940116837 methyleugenol Drugs 0.000 description 1
- PRHTXAOWJQTLBO-UHFFFAOYSA-N methyleugenol Natural products COC1=CC=C(C(C)=C)C=C1OC PRHTXAOWJQTLBO-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 150000002832 nitroso derivatives Chemical class 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- VECVSKFWRQYTAL-UHFFFAOYSA-N octyl benzoate Chemical compound CCCCCCCCOC(=O)C1=CC=CC=C1 VECVSKFWRQYTAL-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 230000017448 oviposition Effects 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920001277 pectin Chemical class 0.000 description 1
- 239000001814 pectin Chemical class 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- BOTNYLSAWDQNEX-UHFFFAOYSA-N phenoxymethylbenzene Chemical compound C=1C=CC=CC=1COC1=CC=CC=C1 BOTNYLSAWDQNEX-UHFFFAOYSA-N 0.000 description 1
- NBFNGRDFKUJVIN-VAWYXSNFSA-N phenyl (e)-3-phenylprop-2-enoate Chemical compound C=1C=CC=CC=1/C=C/C(=O)OC1=CC=CC=C1 NBFNGRDFKUJVIN-VAWYXSNFSA-N 0.000 description 1
- USVNNHYNCCJCCP-UHFFFAOYSA-N phenyl 2-phenylacetate Chemical compound C=1C=CC=CC=1OC(=O)CC1=CC=CC=C1 USVNNHYNCCJCCP-UHFFFAOYSA-N 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- 229940117953 phenylisothiocyanate Drugs 0.000 description 1
- 239000001738 pogostemon cablin oil Substances 0.000 description 1
- 239000003495 polar organic solvent Substances 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- KRIOVPPHQSLHCZ-UHFFFAOYSA-N propiophenone Chemical compound CCC(=O)C1=CC=CC=C1 KRIOVPPHQSLHCZ-UHFFFAOYSA-N 0.000 description 1
- ROVGZAWFACYCSP-VUMXUWRFSA-N pyrethrin I Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 ROVGZAWFACYCSP-VUMXUWRFSA-N 0.000 description 1
- 229940015367 pyrethrum Drugs 0.000 description 1
- 230000000384 rearing effect Effects 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 235000011803 sesame oil Nutrition 0.000 description 1
- 239000008159 sesame oil Substances 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229940047670 sodium acrylate Drugs 0.000 description 1
- 239000000661 sodium alginate Chemical class 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 235000021012 strawberries Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- DQFBYFPFKXHELB-VAWYXSNFSA-N trans-chalcone Chemical compound C=1C=CC=CC=1C(=O)\C=C\C1=CC=CC=C1 DQFBYFPFKXHELB-VAWYXSNFSA-N 0.000 description 1
- DDVNRFNDOPPVQJ-HQJQHLMTSA-N transfluthrin Chemical compound CC1(C)[C@H](C=C(Cl)Cl)[C@H]1C(=O)OCC1=C(F)C(F)=CC(F)=C1F DDVNRFNDOPPVQJ-HQJQHLMTSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000010679 vetiver oil Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
- 229920001285 xanthan gum Chemical class 0.000 description 1
- 239000000230 xanthan gum Chemical class 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical class [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Description
(A)天然ピレトリン
(B)(B-1)フェランドレン、(B-2)バジルオイル、(B-3)月桃オイル、(B-4)クローブリーフオイル、(B-5)ブラックペッパーオイル、(B-6)次の一般式(1)で表される芳香族ケトン化合物、
(B―7)次の一般式(2)で表されるイソチオシアネート化合物、
(B-8)マツ科モミ属に属する植物の圧搾液、抽出物または蒸留物、よりなる群から選ばれる1種または2種以上
を有効成分として含有することを特徴とするダニ用忌避剤。
除虫菊から常法に従って抽出されるものを用いることも可能であるし、それぞれの合成物を単独または混合して用いることも可能である。市販品として、住友天然ピレトリン(住友化学社製)が挙げられる。
することにより、ブラックペッパーオイルが得られる。
することにより入手することができるものである。
もできる。
月桃オイルの製造:
原料として、月桃の葉を用い、以下のようにして月桃オイルを得た。すなわち、月桃の葉100gを5mm角程度の小片となる様に小さく刻み、約80℃の500mLの湯に2時間浸したのち、水蒸気蒸留装置の蒸留槽に投入し水蒸気蒸留を行った。その後、蒸留液より精油を分離し月桃オイルを得た。
ブラックペッパーオイルの製造:
以下のようにしてブラックペッパーオイルを得た。すなわち、ブラックペッパーの実100gを市販のすり鉢とすり棒で十分にすり砕いたものを1Lのビーカーに入れ、約80℃の500mLの湯を入れ蓋をして2時間浸したのち、砕いた実ごと水蒸気蒸留装置の蒸留槽に投入し水蒸気蒸留を行った。その後、蒸留液より精油を分離しブラックペッパーオイルを得た。
原料として、トドマツの葉を用い、圧砕式粉砕機(KYB製作所製)で粉砕したもの約50kgを、マイクロ波蒸留装置の蒸留槽に投入し、攪拌しながら蒸留槽内の圧力を、約20KPaの減圧条件下に保持し、(蒸気温度は約67℃)1時間マイクロ波照射して蒸留した後、油性画分を分離してトドマツ精油を得た。
コナヒョウヒダニの忌避試験:
JIS L 1920「繊維製品の防ダニ性能試験方法」に準じて、ダニの飼育、密度の調整等を行い、図1及び2に示す装置で忌避試験を行った。
死亡率(%)=(A3/A2)×100
A1:ブランクの綿布上及び誘因用培地のダニ数
A2:薬剤処理区の供試片上及び誘因用培地のダニ数
A3:薬剤処理区の供試片上及び誘因用培地の死亡ダニ数
ゲル状ダニ忌避剤:
イソパラフィン85gに、0.1%の天然ピレトリンと1%のバジルオイルを配合したエタノール溶液10gを混合し、これに更にオクチル酸アルミニウム5gを加え、60℃に加熱して攪拌した。これを縦35mm×横35mm×高さ75mmの容器に充填し、室温で3時間静置し、ゲル状のダニ忌避剤を得た。
常温揮散性ダニ忌避剤:
0.1%の天然ピレトリンと1%のフェランドレンを配合したエタノール溶液0.6gを30mm×40mmのパルプ製ろ紙に含浸させ、これを、9mm×22mmの通気孔を設けた、通気性を有するプラスチックケース(38mm×52mm×5mm)に収納して固型忌避剤を調製した。
エアゾール剤:
以下の処方を、市販の200mlエアゾール缶に充填することによって、エアゾール剤
を調製した。
有効成分:天然ピレトリン 0.4ml
:アセトフェノン 1.0ml
溶媒 :エタノール 38.6ml
噴射剤 :LPG 30.0ml
噴射剤 :イソペンタン 30.0ml
スプレー剤:
以下の処方を、市販の150ml容トリガー製容器に収納してスプレー剤を調製した。
有効成分:天然ピレトリン 0.1g
:トドマツ精油 1g
溶剤 :エタノール 10g
香料 0.05g
界面活性剤 0.1g
イオン交換水 88.75g
燻蒸剤:
0.1%の天然ピレトリンと1%のクローブリーフオイルを配合したエタノール溶液10g、アゾジカルボンアミド55g及びタルク35gを混練し、常法に従って造粒、乾燥して燻蒸剤を調製した。
加熱蒸散剤:
0.1%の天然ピレトリンと1%の月桃オイルを配合したエタノール溶液100mgを3cm×3cmのパルプ製マットに含浸させ加熱蒸散剤を得た。このものは、加熱ヒーターに接置させることにより有効成分を蒸散する。
粒状忌避剤:
パルプ製の粒状含浸体(平均粒径5mm)50gに、0.1%の天然ピレトリンと1%のアリルイソチオシアネートを配合したエタノール溶液50mLを含浸させ、通気性の不織布の袋に入れて粒状の忌避剤を得た。
常温揮散性ダニ忌避剤:
0.1%の天然ピレトリンと1%のフェランドレンを配合したエタノール溶液0.5g及びエンペントリン0.01gを9.6mm×110mmのパルプ製ろ紙に含浸させた。これを、88mm×100mmの通気孔を設けた、通気性を有するプラスチックケース(130mm×138mm×9.5mm)に収納して固形忌避剤を調製した。
徐放性ダニ忌避剤:
0.1%の天然ピレトリンと1%のトドマツ精油を配合したエタノール溶液3gを上面開口のプラスチック製容器(直径30mm、深さ10mm)に入れ、開口部を薬剤透過性フィルムで覆い、徐放性ダニ忌避剤を得た。
製剤例2で得られた常温揮散性ダニ忌避剤2個を衣類とともにポリエチレン製の衣類収納袋(75cm×80cm×32cm)に入れたところ、約1か月間衣類にダニがつかなかった。
製剤例8で得られた常温揮散性ダニ忌避剤2個を寝具とともにポリエチレン製の布団収納袋(150cm×100cm)に入れたところ、約6か月間寝具にダニがつかなかった。
製剤例2で得られた常温揮散性ダニ忌避剤2個を衣類とともに75L(40cm×75cm×25cm)の衣装ケースに入れたところ、約3か月間衣類にダニがつかなかった。
製剤例4で得られたスプレー剤のダニ忌避剤を衣類にまんべんなく噴霧したところ、約1週間衣類にダニがつかなかった。
製剤例3で得られたエアゾール剤のダニ忌避剤をカーペットにまんべんなく噴霧したところ、約1か月間、カーペットにダニがつかなかった。
製剤例9で得られた徐放性ダニ忌避剤を30リットルのポリプロピレン製食品用保存容器(355mm×472mm×253mm)に入れたところ、約1年間、保存容器内にダニの侵入はなかった。
21 … … ダニ培地
22 … … 小シャーレ
23 … … 供試片
24 … … 誘引用飼料
25 … … プラスチック製容器
26 … … 飽和食塩水
Claims (9)
- 成分(B)が(B-3)月桃オイルであって、(B-3)月桃オイルが月桃の葉より抽出されたオイルである請求項1に記載の室内塵性ダニ用忌避剤。
- 成分(B)が(B-6)芳香族ケトン化合物であって、(B-6)芳香族ケトン化合物がアセトフェノンである請求項1に記載の室内塵性ダニ用忌避剤。
- 請求項1~3のいずれかの項記載の室内塵性ダニ用忌避剤を環境中に放出することを特徴とする室内塵性ダニの忌避方法。
- 環境中への放出を、常温での自然蒸散により行う請求項4記載の室内塵性ダニの忌避方法。
- 環境中への放出を、加熱による蒸散、送風による蒸散または薫蒸による蒸散により強制的に行う請求項4記載の室内塵性ダニの忌避方法。
- 環境中への放出を、噴霧により行う請求項4記載の室内塵性ダニの忌避方法。
- 請求項1~3のいずれかの項記載の室内塵性ダニ用忌避剤を繊維製品に適用することを特徴とする室内塵性ダニの忌避方法。
- 請求項1~3のいずれかの項記載の室内塵性ダニ用忌避剤をダニに接触させて作用させることを特徴とするダニの室内塵性忌避方法。
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Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2001031508A (ja) | 1999-07-16 | 2001-02-06 | Hattori Medical Service:Kk | ヒョウヒダニの忌避剤 |
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