JP7296880B2 - 骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む組成物の可塑性を低下させるための酸処理の使用方法 - Google Patents

骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む組成物の可塑性を低下させるための酸処理の使用方法 Download PDF

Info

Publication number
JP7296880B2
JP7296880B2 JP2019527183A JP2019527183A JP7296880B2 JP 7296880 B2 JP7296880 B2 JP 7296880B2 JP 2019527183 A JP2019527183 A JP 2019527183A JP 2019527183 A JP2019527183 A JP 2019527183A JP 7296880 B2 JP7296880 B2 JP 7296880B2
Authority
JP
Japan
Prior art keywords
titanium
zeolitic material
mww
framework
composition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2019527183A
Other languages
English (en)
Japanese (ja)
Other versions
JP2020502304A (ja
JP2020502304A5 (cg-RX-API-DMAC7.html
Inventor
パルフレスク，アンドレイ－ニコラエ
ミュラー，ウルリヒ
リュッツェル，ハンス－ユルゲン
ウール，ゲオルク
ヘンリケ テレス，ジョアキム
リーデル，ドミニク
ウルバンクツィク，ダニエル
ヴェゲルレ，ウルリケ
ヴェーバー，マルクス
トニオ ヴェルツ，ニコライ
ミュラー，クリスティアン
シュミット，リュディガー
フェルナンデス，シアナ ロマニ
ヴュルツ，ハラルト
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2020502304A publication Critical patent/JP2020502304A/ja
Publication of JP2020502304A5 publication Critical patent/JP2020502304A5/ja
Application granted granted Critical
Publication of JP7296880B2 publication Critical patent/JP7296880B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7049—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing rare earth elements, titanium, zirconium, hafnium, zinc, cadmium, mercury, gallium, indium, thallium, tin or lead
    • B01J29/7088—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/223—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material containing metals, e.g. organo-metallic compounds, coordination complexes
    • B01J20/226—Coordination polymers, e.g. metal-organic frameworks [MOF], zeolitic imidazolate frameworks [ZIF]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B01J20/28021—Hollow particles, e.g. hollow spheres, microspheres or cenospheres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3071—Washing or leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/37—Acid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2019527183A 2016-12-20 2017-12-20 骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む組成物の可塑性を低下させるための酸処理の使用方法 Active JP7296880B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP16205266.6 2016-12-20
EP16205266 2016-12-20
PCT/EP2017/083810 WO2018115118A1 (en) 2016-12-20 2017-12-20 Use of an acid treatment to decrease the plasticity of a composition comprising a titanium-containing zeolitic material having framework type mww

Publications (3)

Publication Number Publication Date
JP2020502304A JP2020502304A (ja) 2020-01-23
JP2020502304A5 JP2020502304A5 (cg-RX-API-DMAC7.html) 2021-02-04
JP7296880B2 true JP7296880B2 (ja) 2023-06-23

Family

ID=57838133

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2019527183A Active JP7296880B2 (ja) 2016-12-20 2017-12-20 骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む組成物の可塑性を低下させるための酸処理の使用方法

Country Status (10)

Country Link
US (1) US11351525B2 (cg-RX-API-DMAC7.html)
EP (1) EP3558517A1 (cg-RX-API-DMAC7.html)
JP (1) JP7296880B2 (cg-RX-API-DMAC7.html)
KR (1) KR102555075B1 (cg-RX-API-DMAC7.html)
CN (2) CN110087768B (cg-RX-API-DMAC7.html)
BR (1) BR112019011059B1 (cg-RX-API-DMAC7.html)
MY (1) MY199977A (cg-RX-API-DMAC7.html)
RU (1) RU2761301C2 (cg-RX-API-DMAC7.html)
WO (1) WO2018115118A1 (cg-RX-API-DMAC7.html)
ZA (1) ZA201903192B (cg-RX-API-DMAC7.html)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX2018016297A (es) 2016-06-29 2019-09-16 Basf Se Proceso para la preparacion de aldehidos alfa, beta insaturados mediante oxidacion de alcoholes en presencia de una fase liquida.
CN110582481A (zh) 2017-05-03 2019-12-17 巴斯夫欧洲公司 用沸石将氧化乙烯转化为单乙醇胺和乙二胺的方法
CN115477310B (zh) * 2021-06-16 2023-11-28 中国石油化工股份有限公司 P-Ti-MWW分子筛及其制备方法与应用

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006525283A (ja) 2003-05-08 2006-11-09 ビーエーエスエフ　アクチェンゲゼルシャフト プロピレンオキシドの製造方法
JP2013518796A (ja) 2010-02-01 2013-05-23 ライオンデル ケミカル テクノロジー、 エル．ピー． チタン−ｍｗｗゼオライトの製造方法
JP2015512845A (ja) 2012-02-07 2015-04-30 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ＴｉおよびＺｎを含有するゼオライト材料を含有する微小粉末および成形物
JP2016506904A (ja) 2013-02-05 2016-03-07 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Ｍｗｗフレームワーク構造を有するチタン含有ゼオライト材料を製造するための方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0689170B2 (ja) * 1985-09-24 1994-11-09 日本化学工業株式会社 樹脂組成物
JP3706457B2 (ja) * 1997-02-28 2005-10-12 帝人化成株式会社 熱可塑性樹脂組成物
MY169039A (en) * 2012-10-18 2019-02-07 Basf Se Post-treatment of deboronated mww zeolite
CN103934039A (zh) * 2013-01-23 2014-07-23 中国石油化工股份有限公司 提高分子筛催化剂强度的方法
CN105848781B (zh) * 2013-10-23 2020-07-17 巴斯夫欧洲公司 疏水性沸石材料的模制品及其制备方法
CN104437616B (zh) * 2014-11-21 2017-10-10 武汉工程大学 层状含介孔钛硅分子筛催化剂及其制备方法和应用

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006525283A (ja) 2003-05-08 2006-11-09 ビーエーエスエフ　アクチェンゲゼルシャフト プロピレンオキシドの製造方法
JP2013518796A (ja) 2010-02-01 2013-05-23 ライオンデル ケミカル テクノロジー、 エル．ピー． チタン−ｍｗｗゼオライトの製造方法
JP2015512845A (ja) 2012-02-07 2015-04-30 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ＴｉおよびＺｎを含有するゼオライト材料を含有する微小粉末および成形物
JP2016506904A (ja) 2013-02-05 2016-03-07 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Ｍｗｗフレームワーク構造を有するチタン含有ゼオライト材料を製造するための方法

Also Published As

Publication number Publication date
US11351525B2 (en) 2022-06-07
JP2020502304A (ja) 2020-01-23
BR112019011059B1 (pt) 2022-08-09
CN110087768B (zh) 2023-09-01
KR20190089913A (ko) 2019-07-31
CN117046513A (zh) 2023-11-14
RU2019122860A (ru) 2021-01-25
KR102555075B1 (ko) 2023-07-12
CN110087768A (zh) 2019-08-02
RU2761301C2 (ru) 2021-12-07
ZA201903192B (en) 2024-09-25
WO2018115118A1 (en) 2018-06-28
RU2019122860A3 (cg-RX-API-DMAC7.html) 2021-04-21
EP3558517A1 (en) 2019-10-30
US20190321811A1 (en) 2019-10-24
BR112019011059A2 (pt) 2019-10-08
MY199977A (en) 2023-12-01

Similar Documents

Publication Publication Date Title
JP6598789B2 (ja) Ｂｅａ骨格構造を有するスズ含有ゼオライト材料
JP6775491B2 (ja) ホウ素およびチタンを含むｍｗｗゼオライト系材料の製造のための方法
ES2637839T3 (es) Micropolvos y moldeados que contienen un material zeolítico que contiene Ti y Zn
JP2018518467A (ja) メロナールの調製方法
JP6267211B2 (ja) 脱ホウ素化ｍｗｗゼオライトの後処理
JP7362830B2 (ja) 骨格型ｍｗｗを有するチタン含有ゼオライト材料を含む押出成形性組成物を製造する方法
JP6306029B2 (ja) 脱ホウ素化ゼオライトベータの後処理
CN106495178B (zh) 一种制备介孔分子筛型钛酸钕环境净化材料的方法
KR102555075B1 (ko) Mww형 골격을 갖는 티타늄-함유 제올라이트 재료를 포함하는 조성물의 소성도를 감소시키기 위한 산 처리의 용도
JP7796069B2 (ja) 亜鉛とチタン含有ゼオライトとを含む成形物の製造方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20201217

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20201217

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20211116

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20211124

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20220218

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20220510

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20220802

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20221206

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20230208

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20230516

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20230613

R150 Certificate of patent or registration of utility model

Ref document number: 7296880

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250