JP6844538B2 - ニッケルペースト及びニッケルペーストの製造方法 - Google Patents
ニッケルペースト及びニッケルペーストの製造方法 Download PDFInfo
- Publication number
- JP6844538B2 JP6844538B2 JP2017531136A JP2017531136A JP6844538B2 JP 6844538 B2 JP6844538 B2 JP 6844538B2 JP 2017531136 A JP2017531136 A JP 2017531136A JP 2017531136 A JP2017531136 A JP 2017531136A JP 6844538 B2 JP6844538 B2 JP 6844538B2
- Authority
- JP
- Japan
- Prior art keywords
- nickel
- vehicle
- paste
- dispersion migration
- migration accelerator
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 388
- 229910052759 nickel Inorganic materials 0.000 title claims description 148
- 238000004519 manufacturing process Methods 0.000 title claims description 31
- 239000006185 dispersion Substances 0.000 claims description 104
- 238000013508 migration Methods 0.000 claims description 102
- 230000005012 migration Effects 0.000 claims description 102
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 88
- 239000002002 slurry Substances 0.000 claims description 47
- 239000011347 resin Substances 0.000 claims description 45
- 229920005989 resin Polymers 0.000 claims description 45
- 239000011230 binding agent Substances 0.000 claims description 43
- 239000002253 acid Substances 0.000 claims description 24
- 238000004898 kneading Methods 0.000 claims description 22
- 239000002994 raw material Substances 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 238000012546 transfer Methods 0.000 claims description 2
- 238000000034 method Methods 0.000 description 54
- 239000003960 organic solvent Substances 0.000 description 24
- 239000000843 powder Substances 0.000 description 24
- 229920000642 polymer Polymers 0.000 description 15
- 239000002184 metal Substances 0.000 description 14
- 229910052751 metal Inorganic materials 0.000 description 14
- 239000003945 anionic surfactant Substances 0.000 description 13
- 239000002245 particle Substances 0.000 description 13
- 230000008569 process Effects 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- UODXCYZDMHPIJE-UHFFFAOYSA-N menthanol Chemical compound CC1CCC(C(C)(C)O)CC1 UODXCYZDMHPIJE-UHFFFAOYSA-N 0.000 description 12
- 239000003985 ceramic capacitor Substances 0.000 description 11
- 150000001875 compounds Chemical class 0.000 description 9
- 238000000926 separation method Methods 0.000 description 9
- 238000011156 evaluation Methods 0.000 description 8
- BMGPYWJNOIMZNC-KHPPLWFESA-N 2-[methyl-[(z)-octadec-9-enyl]amino]acetic acid Chemical compound CCCCCCCC\C=C/CCCCCCCCN(C)CC(O)=O BMGPYWJNOIMZNC-KHPPLWFESA-N 0.000 description 7
- 239000001856 Ethyl cellulose Substances 0.000 description 7
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 7
- 230000002776 aggregation Effects 0.000 description 7
- 239000002270 dispersing agent Substances 0.000 description 7
- 229920001249 ethyl cellulose Polymers 0.000 description 7
- 235000019325 ethyl cellulose Nutrition 0.000 description 7
- 230000009467 reduction Effects 0.000 description 7
- FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical compound C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 238000004220 aggregation Methods 0.000 description 5
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 description 5
- 125000002811 oleoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])/C([H])=C([H])\C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 5
- BACYUWVYYTXETD-UHFFFAOYSA-N N-Lauroylsarcosine Chemical compound CCCCCCCCCCCC(=O)N(C)CC(O)=O BACYUWVYYTXETD-UHFFFAOYSA-N 0.000 description 4
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 125000000524 functional group Chemical group 0.000 description 4
- 150000002815 nickel Chemical class 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000004925 Acrylic resin Substances 0.000 description 3
- 229920000178 Acrylic resin Polymers 0.000 description 3
- 108010077895 Sarcosine Proteins 0.000 description 3
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 239000013067 intermediate product Substances 0.000 description 3
- 108700004121 sarkosyl Proteins 0.000 description 3
- UNWFFCPRJXMCNV-UHFFFAOYSA-N 3-[dodecanoyl(methyl)amino]propanoic acid Chemical compound CCCCCCCCCCCC(=O)N(C)CCC(O)=O UNWFFCPRJXMCNV-UHFFFAOYSA-N 0.000 description 2
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 2
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 239000005456 alcohol based solvent Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 2
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 description 2
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 2
- 238000000518 rheometry Methods 0.000 description 2
- 229940043230 sarcosine Drugs 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 229940116411 terpineol Drugs 0.000 description 2
- 239000011882 ultra-fine particle Substances 0.000 description 2
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 1
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 description 1
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 1
- 239000001716 (4-methyl-1-propan-2-yl-1-cyclohex-2-enyl) acetate Substances 0.000 description 1
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 1
- BBOPKBHSDDSVFS-UHFFFAOYSA-N 1-chloro-4-ethoxy-2-fluorobenzene Chemical compound CCOC1=CC=C(Cl)C(F)=C1 BBOPKBHSDDSVFS-UHFFFAOYSA-N 0.000 description 1
- LFJJOPDNPVFCNZ-UHFFFAOYSA-N 2-[hexadecanoyl(methyl)amino]acetic acid Chemical compound CCCCCCCCCCCCCCCC(=O)N(C)CC(O)=O LFJJOPDNPVFCNZ-UHFFFAOYSA-N 0.000 description 1
- 229920002799 BoPET Polymers 0.000 description 1
- 208000005156 Dehydration Diseases 0.000 description 1
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- IGODOXYLBBXFDW-UHFFFAOYSA-N alpha-Terpinyl acetate Chemical compound CC(=O)OC(C)(C)C1CCC(C)=CC1 IGODOXYLBBXFDW-UHFFFAOYSA-N 0.000 description 1
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 description 1
- 229910002113 barium titanate Inorganic materials 0.000 description 1
- 229940000635 beta-alanine Drugs 0.000 description 1
- 229940116229 borneol Drugs 0.000 description 1
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 125000002843 carboxylic acid group Chemical group 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920003086 cellulose ether Polymers 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 238000005443 coulometric titration Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 description 1
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- 150000002148 esters Chemical group 0.000 description 1
- 125000001033 ether group Chemical group 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 125000000400 lauroyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000693 micelle Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000007498 myristoylation Effects 0.000 description 1
- 229940094933 n-dodecane Drugs 0.000 description 1
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 description 1
- 108700009886 palmitoyl sarcosine Proteins 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000004034 viscosity adjusting agent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
-
- B22F1/0003—
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/20—Conductive material dispersed in non-conductive organic material
- H01B1/22—Conductive material dispersed in non-conductive organic material the conductive material comprising metals or alloys
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B13/00—Apparatus or processes specially adapted for manufacturing conductors or cables
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2301/00—Metallic composition of the powder or its coating
- B22F2301/15—Nickel or cobalt
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Dispersion Chemistry (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Manufacturing & Machinery (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Conductive Materials (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Ceramic Capacitors (AREA)
- Powder Metallurgy (AREA)
- Fixed Capacitors And Capacitor Manufacturing Machines (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2015146929 | 2015-07-24 | ||
| JP2015146929 | 2015-07-24 | ||
| PCT/JP2016/070833 WO2017018228A1 (ja) | 2015-07-24 | 2016-07-14 | ニッケルペースト及びニッケルペーストの製造方法 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2020219408A Division JP7207391B2 (ja) | 2015-07-24 | 2020-12-28 | ニッケルペースト及びニッケルペーストの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPWO2017018228A1 JPWO2017018228A1 (ja) | 2018-06-14 |
| JP6844538B2 true JP6844538B2 (ja) | 2021-03-17 |
Family
ID=57886823
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017531136A Active JP6844538B2 (ja) | 2015-07-24 | 2016-07-14 | ニッケルペースト及びニッケルペーストの製造方法 |
| JP2020219408A Active JP7207391B2 (ja) | 2015-07-24 | 2020-12-28 | ニッケルペースト及びニッケルペーストの製造方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2020219408A Active JP7207391B2 (ja) | 2015-07-24 | 2020-12-28 | ニッケルペースト及びニッケルペーストの製造方法 |
Country Status (5)
| Country | Link |
|---|---|
| JP (2) | JP6844538B2 (ko) |
| KR (1) | KR102095331B1 (ko) |
| CN (1) | CN107851479B (ko) |
| TW (1) | TWI696508B (ko) |
| WO (1) | WO2017018228A1 (ko) |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004200449A (ja) * | 2002-12-19 | 2004-07-15 | Sumitomo Metal Mining Co Ltd | 積層セラミックコンデンサ内部電極用導電性ペースト組成物 |
| JP2004319353A (ja) * | 2003-04-18 | 2004-11-11 | Toray Ind Inc | 固体電解質およびそれを用いた燃料電池 |
| US20070034841A1 (en) * | 2003-09-30 | 2007-02-15 | Tdk Corporation | Method for preparing conductive paste for inner electrode of multi-layered ceramic electronic component |
| JP4916107B2 (ja) * | 2004-03-10 | 2012-04-11 | 株式会社村田製作所 | 導電性ペーストおよびこれを用いたセラミック電子部品 |
| JP4495644B2 (ja) | 2004-07-30 | 2010-07-07 | Ｊｆｅミネラル株式会社 | 金属超微粉スラリー |
| TWI310570B (en) * | 2004-07-30 | 2009-06-01 | Jfe Mineral Co Ltd | Ultrafine metal powder slurry |
| JP5018154B2 (ja) * | 2007-03-15 | 2012-09-05 | Ｔｄｋ株式会社 | 内部電極形成ペースト、積層型セラミック型電子部品、およびその製造方法 |
| JP4960210B2 (ja) * | 2007-12-12 | 2012-06-27 | 東邦チタニウム株式会社 | ニッケル粉末およびニッケル粉末の製造方法 |
| JP5262445B2 (ja) * | 2008-08-28 | 2013-08-14 | 住友金属鉱山株式会社 | 積層セラミックコンデンサ内部電極用導電性ペースト |
| JP5820200B2 (ja) * | 2010-10-29 | 2015-11-24 | 積水化学工業株式会社 | 変性ポリビニルアセタール樹脂及び変性ポリビニルアセタール樹脂組成物 |
| JP2014029845A (ja) * | 2012-06-28 | 2014-02-13 | Nippon Steel & Sumikin Chemical Co Ltd | 導電性ペーストの製造方法 |
| JP6179274B2 (ja) | 2013-08-27 | 2017-08-16 | 住友金属鉱山株式会社 | ニッケルペーストの製造方法及びニッケルペースト |
| JP6244921B2 (ja) * | 2014-01-09 | 2017-12-13 | 株式会社村田製作所 | 導電ペースト |
| CN107077911B (zh) * | 2014-09-26 | 2019-08-20 | 住友金属矿山株式会社 | 镍膏及镍膏的制造方法 |
| JP6222373B2 (ja) * | 2014-09-26 | 2017-11-01 | 住友金属鉱山株式会社 | ニッケルペースト及びニッケルペーストの製造方法 |
-
2016
- 2016-07-14 WO PCT/JP2016/070833 patent/WO2017018228A1/ja active Application Filing
- 2016-07-14 KR KR1020187001787A patent/KR102095331B1/ko active IP Right Grant
- 2016-07-14 JP JP2017531136A patent/JP6844538B2/ja active Active
- 2016-07-14 CN CN201680043154.6A patent/CN107851479B/zh active Active
- 2016-07-18 TW TW105122548A patent/TWI696508B/zh active
-
2020
- 2020-12-28 JP JP2020219408A patent/JP7207391B2/ja active Active
Also Published As
| Publication number | Publication date |
|---|---|
| JP7207391B2 (ja) | 2023-01-18 |
| CN107851479B (zh) | 2019-12-17 |
| JPWO2017018228A1 (ja) | 2018-06-14 |
| JP2021057352A (ja) | 2021-04-08 |
| KR20180020231A (ko) | 2018-02-27 |
| CN107851479A (zh) | 2018-03-27 |
| KR102095331B1 (ko) | 2020-03-31 |
| WO2017018228A1 (ja) | 2017-02-02 |
| TWI696508B (zh) | 2020-06-21 |
| TW201718132A (zh) | 2017-06-01 |
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