JP6800316B2 - シリカ粒子の製造方法 - Google Patents

シリカ粒子の製造方法 Download PDF

Info

Publication number
JP6800316B2
JP6800316B2 JP2019511304A JP2019511304A JP6800316B2 JP 6800316 B2 JP6800316 B2 JP 6800316B2 JP 2019511304 A JP2019511304 A JP 2019511304A JP 2019511304 A JP2019511304 A JP 2019511304A JP 6800316 B2 JP6800316 B2 JP 6800316B2
Authority
JP
Japan
Prior art keywords
mass
meth
less
silica
silica particles
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2019511304A
Other languages
English (en)
Japanese (ja)
Other versions
JPWO2018186468A1 (ja
Inventor
仁希 西村
仁希 西村
勇二 小野
勇二 小野
将一 芝▲崎▼
将一 芝▲崎▼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Shokubai Co Ltd
Original Assignee
Nippon Shokubai Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd
Publication of JPWO2018186468A1 publication Critical patent/JPWO2018186468A1/ja
Application granted granted Critical
Publication of JP6800316B2 publication Critical patent/JP6800316B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3045—Treatment with inorganic compounds
    • C09C1/3054—Coating
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F292/00—Macromolecular compounds obtained by polymerising monomers on to inorganic materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C08K3/36—Silica
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L101/00—Compositions of unspecified macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3063—Treatment with low-molecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/28—Compounds of silicon
    • C09C1/30—Silicic acid
    • C09C1/3081—Treatment with organo-silicon compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/002—Physical properties
    • C08K2201/005—Additives being defined by their particle size in general
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/002—Physical properties
    • C08K2201/006—Additives being defined by their surface area
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Silicon Compounds (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Graft Or Block Polymers (AREA)
JP2019511304A 2017-04-06 2018-04-05 シリカ粒子の製造方法 Active JP6800316B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP2017076024 2017-04-06
JP2017076024 2017-04-06
JP2017126981 2017-06-29
JP2017126981 2017-06-29
PCT/JP2018/014577 WO2018186468A1 (ja) 2017-04-06 2018-04-05 シリカ粒子

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2020191953A Division JP7128250B2 (ja) 2017-04-06 2020-11-18 シリカ粒子分散体およびシリカ粒子含有樹脂組成物の製造方法

Publications (2)

Publication Number Publication Date
JPWO2018186468A1 JPWO2018186468A1 (ja) 2019-11-07
JP6800316B2 true JP6800316B2 (ja) 2020-12-16

Family

ID=63712173

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2019511304A Active JP6800316B2 (ja) 2017-04-06 2018-04-05 シリカ粒子の製造方法
JP2020191953A Active JP7128250B2 (ja) 2017-04-06 2020-11-18 シリカ粒子分散体およびシリカ粒子含有樹脂組成物の製造方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2020191953A Active JP7128250B2 (ja) 2017-04-06 2020-11-18 シリカ粒子分散体およびシリカ粒子含有樹脂組成物の製造方法

Country Status (6)

Country Link
US (1) US11214492B2 (https=)
EP (1) EP3608292B1 (https=)
JP (2) JP6800316B2 (https=)
KR (1) KR102450033B1 (https=)
CN (1) CN110461768B (https=)
WO (1) WO2018186468A1 (https=)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7254475B2 (ja) * 2018-10-10 2023-04-10 株式会社日本触媒 表面処理シリカ粒子、これを含む分散体及び樹脂組成物、並びに樹脂組成物の硬化物
JP6564517B1 (ja) 2018-12-17 2019-08-21 株式会社アドマテックス 電子材料用フィラー及びその製造方法、電子材料用樹脂組成物の製造方法、高周波用基板、並びに電子材料用スラリー
CN114127605B (zh) * 2019-07-26 2025-03-04 住友电气工业株式会社 光纤带和光纤缆线
JP7333225B2 (ja) * 2019-08-23 2023-08-24 株式会社日本触媒 （メタ）アクリル樹脂の製造方法及び（メタ）アクリル樹脂
JP7516763B2 (ja) * 2020-01-28 2024-07-17 三菱ケミカル株式会社 シリカ粒子の製造方法、シリカゾルの製造方法、中間生成物の除去方法及び研磨方法
CN115397775B (zh) * 2020-03-31 2024-08-06 日产化学株式会社 表面改性二氧化硅粒子的有机溶剂分散溶胶的制造方法
US12265270B2 (en) * 2021-03-08 2025-04-01 Corning Research & Development Corporation Flame retardant compositions for buffer tubes and method of making same
CN113698554B (zh) * 2021-09-16 2024-05-07 西安热工研究院有限公司 一种以纳米SiO2为内核的阴离子交换树脂及其制备方法
US20240383760A1 (en) * 2021-10-18 2024-11-21 Mitsubishi Materials Electronic Chemicals Co., Ltd. Surface-treated silica particle dispersion sol and production method therefor
CN113861812B (zh) * 2021-12-02 2022-03-29 富维薄膜（山东）有限公司 一种聚酯薄膜用涂布液及其应用
TWI815246B (zh) * 2021-12-16 2023-09-11 臺灣塑膠工業股份有限公司 矽基粉體及其製造方法
JP2023108405A (ja) * 2022-01-25 2023-08-04 日揮触媒化成株式会社 有機無機複合微粒子分散液およびその製造方法、並びに砥粒分散液
JP2023170440A (ja) * 2022-05-19 2023-12-01 株式会社日本触媒 表面処理シリカ粒子分散体
CN119585316A (zh) * 2022-07-22 2025-03-07 株式会社日本触媒 组合物
JP2024029655A (ja) * 2022-08-22 2024-03-06 株式会社日本触媒 無機粒子含有分散体
KR20250077453A (ko) * 2022-09-30 2025-05-30 닛산 가가쿠 가부시키가이샤 아민함유 중공 실리카입자의 유기용매 졸 및 그의 제조방법
DE112023004572T5 (de) * 2022-10-31 2025-09-04 Nissan Chemical Corporation Organosilica-sol und herstellungsverfahren hierfür

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2829091A1 (de) 1978-07-03 1980-01-17 Dynamit Nobel Ag Insolubilisierte reagenzien enthaltene kieselgele
DE3616133A1 (de) 1985-09-25 1987-11-19 Merck Patent Gmbh Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel
US5221497A (en) * 1988-03-16 1993-06-22 Nissan Chemical Industries, Ltd. Elongated-shaped silica sol and method for preparing the same
JP2856259B2 (ja) 1990-01-31 1999-02-10 富士通株式会社 自己学習システムの安定化方式
JP3225553B2 (ja) 1991-10-11 2001-11-05 日産化学工業株式会社 高純度の水性シリカゾルの製造方法
JP4631119B2 (ja) * 2000-01-28 2011-02-16 Ｊｓｒ株式会社 疎水化コロイダルシリカの製造方法
KR101237822B1 (ko) * 2003-08-28 2013-02-28 니끼 쇼꾸바이 카세이 가부시키가이샤 반사 방지 적층체
JP4805156B2 (ja) * 2004-09-02 2011-11-02 日揮触媒化成株式会社 チタニウム含有シリカゾルおよびその製造方法、防汚被膜およびインク受容層付基材、ならびに記録用基材の再生方法
US7771782B2 (en) 2005-07-29 2010-08-10 Intercast Europe, srl Method of manufacturing a high impact polarized optical element and polarized optical element including an integrally bonded polarizing film
JP2007070578A (ja) 2005-09-09 2007-03-22 Mitsubishi Rayon Co Ltd 活性エネルギー線硬化型塗料組成物
US20080261400A1 (en) * 2005-12-21 2008-10-23 Asahi Glass Company, Limited Polishing composition, polishing method, and method for forming copper wiring for semiconductor integrated circuit
JP5186768B2 (ja) 2006-06-16 2013-04-24 東洋インキＳｃホールディングス株式会社 帯電防止用硬化性組成物、硬化膜及び積層体
KR20090104029A (ko) * 2007-01-18 2009-10-05 니폰 가가쿠 고교 가부시키가이샤 개질 페로브스카이트형 복합 산화물, 그 제조 방법 및 복합 유전체 재료
JP2008273780A (ja) 2007-04-27 2008-11-13 Jgc Catalysts & Chemicals Ltd 改質シリカ系ゾルおよびその製造方法
JP2009263484A (ja) * 2008-04-24 2009-11-12 Nippon Chem Ind Co Ltd 半導体ウエハ研磨用コロイダルシリカおよびその製造方法
JP5084670B2 (ja) * 2008-09-01 2012-11-28 日揮触媒化成株式会社 シリカゾルおよびその製造方法
JP2011206762A (ja) 2010-03-10 2011-10-20 Konica Minolta Business Technologies Inc 粒子の疎水化処理方法
JP5622277B2 (ja) 2010-08-25 2014-11-12 関西ペイント株式会社 複層塗膜形成方法及び塗装物品
JP5404568B2 (ja) 2010-09-21 2014-02-05 日揮触媒化成株式会社 シリカ系微粒子、被膜形成用塗料および被膜付基材
JP5787705B2 (ja) 2011-10-11 2015-09-30 扶桑化学工業株式会社 高純度単分散シリカ粒子及びその製造方法
KR102172825B1 (ko) 2013-06-10 2020-11-02 닛산 가가쿠 가부시키가이샤 실리카 함유 수지 조성물 및 그 제조 방법 그리고 실리카 함유 수지 조성물의 성형품
US10239758B2 (en) 2013-06-10 2019-03-26 Nissan Chemical Industries, Ltd. Silica sol and method for producing silica sol
JP6195524B2 (ja) 2014-01-28 2017-09-13 日揮触媒化成株式会社 疎水性シリカ粉末およびその製造方法
JP2016175981A (ja) 2015-03-19 2016-10-06 セイコーインスツル株式会社 有機無機ハイブリッドコーティング剤およびその製造方法
JP6509704B2 (ja) 2015-10-14 2019-05-08 日本特殊陶業株式会社 ペリクル枠およびペリクル枠の製造方法
EP3422464B1 (en) 2015-12-29 2021-02-24 Synergy Microwave Corporation Microwave mems phase shifter

Also Published As

Publication number Publication date
CN110461768B (zh) 2022-11-29
EP3608292B1 (en) 2024-11-27
EP3608292A1 (en) 2020-02-12
JP7128250B2 (ja) 2022-08-30
JP2021042122A (ja) 2021-03-18
EP3608292A4 (en) 2020-12-23
KR102450033B1 (ko) 2022-09-30
US11214492B2 (en) 2022-01-04
KR20190120827A (ko) 2019-10-24
US20200131044A1 (en) 2020-04-30
WO2018186468A1 (ja) 2018-10-11
CN110461768A (zh) 2019-11-15
JPWO2018186468A1 (ja) 2019-11-07

Similar Documents

Publication Publication Date Title
JP6800316B2 (ja) シリカ粒子の製造方法
JP6565923B2 (ja) 表面修飾金属酸化物粒子分散液及びその製造方法、表面修飾金属酸化物粒子−シリコーン樹脂複合組成物、表面修飾金属酸化物粒子−シリコーン樹脂複合体、光学部材、及び発光装置
US8298456B2 (en) Silicone resin composition
JP5627662B2 (ja) 表面処理シリカ系粒子の製造方法
CN101312909A (zh) 中空二氧化硅微粒、含有该微粒的透明涂膜形成用组合物、及覆有透明涂膜的基材
JP7007982B2 (ja) コロイダルシリカ
JPWO2019044929A1 (ja) 表面処理ゾルゲルシリカ及びその製造方法
JP5754884B2 (ja) リン酸（ただし、リン酸の塩を除く）処理金属酸化物微粒子およびその製造方法、該リン酸（ただし、リン酸の塩を除く）処理金属酸化物微粒子を含む透明被膜形成用塗布液ならびに透明被膜付基材
JP7254475B2 (ja) 表面処理シリカ粒子、これを含む分散体及び樹脂組成物、並びに樹脂組成物の硬化物
JP7061000B2 (ja) シリカ粒子又はその分散体の製造方法
TW201139535A (en) Modified cerium(IV) oxide colloidal particles and production method thereof
KR101244205B1 (ko) 산화알루미늄 및 주기율표의 제ⅰ 및 제ⅱ 주족 원소의산화물로부터의 표면-개질 나노입자 및 이의 제법
JP7464385B2 (ja) 中空樹脂粒子及びその製造方法
US11535756B2 (en) Method for producing silica composite particle
JP2014196216A (ja) 改質金属酸化物微粒子粉末、改質金属酸化物微粒子分散体およびその製造方法
CN1934138A (zh) 包含表面改性粒子的可固化组合物
JP7796496B2 (ja) シリカ粒子含有組成物及びその硬化物
JP2014196215A (ja) 改質金属酸化物微粒子粉末およびその製造方法
WO2024019139A1 (ja) 組成物
JP6654424B2 (ja) シリカ粒子及びシリカ粒子分散液
JP2023170440A (ja) 表面処理シリカ粒子分散体
WO2024019140A1 (ja) 組成物

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20190508

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200121

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20200319

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200804

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20200930

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20201110

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20201124

R150 Certificate of patent or registration of utility model

Ref document number: 6800316

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150