JP6687608B2 - 回収方法 - Google Patents

回収方法 Download PDF

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Publication number
JP6687608B2
JP6687608B2 JP2017518134A JP2017518134A JP6687608B2 JP 6687608 B2 JP6687608 B2 JP 6687608B2 JP 2017518134 A JP2017518134 A JP 2017518134A JP 2017518134 A JP2017518134 A JP 2017518134A JP 6687608 B2 JP6687608 B2 JP 6687608B2
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Japan
Prior art keywords
leaching
lithium
salt
filtrate
monovalent
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JP2017518134A
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English (en)
Japanese (ja)
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JP2017537221A5 (enExample
JP2017537221A (ja
Inventor
ドナルド ジョンソン，ゲイリー
ドナルド ジョンソン，ゲイリー
ダニエル ウルバーニ，マーク
ダニエル ウルバーニ，マーク
ジョン ヴァインズ，ニコラス
ジョン ヴァインズ，ニコラス
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Li Technology Pty Ltd
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Li Technology Pty Ltd
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Priority claimed from AU2014904050A external-priority patent/AU2014904050A0/en
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Publication of JP2017537221A publication Critical patent/JP2017537221A/ja
Publication of JP2017537221A5 publication Critical patent/JP2017537221A5/ja
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/08—Carbonates; Bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/04—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
    • C01F7/06—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom by treating aluminous minerals or waste-like raw materials with alkali hydroxide, e.g. leaching of bauxite according to the Bayer process
    • C01F7/0686—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom by treating aluminous minerals or waste-like raw materials with alkali hydroxide, e.g. leaching of bauxite according to the Bayer process from sulfate-containing minerals, e.g. alunite
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/08—Sulfuric acid, other sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Removal Of Specific Substances (AREA)
  • Silicon Compounds (AREA)
JP2017518134A 2014-10-10 2015-10-09 回収方法 Active JP6687608B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
AU2014904050 2014-10-10
AU2014904050A AU2014904050A0 (en) 2014-10-10 Recovery Process
PCT/AU2015/000608 WO2016054683A1 (en) 2014-10-10 2015-10-09 Recovery process

Publications (3)

Publication Number Publication Date
JP2017537221A JP2017537221A (ja) 2017-12-14
JP2017537221A5 JP2017537221A5 (enExample) 2018-05-31
JP6687608B2 true JP6687608B2 (ja) 2020-04-22

Family

ID=55652390

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2017518134A Active JP6687608B2 (ja) 2014-10-10 2015-10-09 回収方法

Country Status (8)

Country Link
US (1) US10450630B2 (enExample)
EP (1) EP3204528B1 (enExample)
JP (1) JP6687608B2 (enExample)
AU (1) AU2015330958B2 (enExample)
CA (1) CA2962070C (enExample)
ES (1) ES2806425T3 (enExample)
PT (1) PT3204528T (enExample)
WO (1) WO2016054683A1 (enExample)

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CA2874917C (en) 2012-05-30 2016-06-21 Nemaska Lithium Inc. Processes for preparing lithium carbonate
DK2971252T3 (da) 2013-03-15 2021-03-29 Nemaska Lithium Inc Fremgangsmåde til fremstilling af lithiumhydroxid
KR102445712B1 (ko) 2013-10-23 2022-09-20 네마스카 리튬 인코포레이션 리튬 카보네이트의 제조방법
PT3110988T (pt) 2014-02-24 2019-09-10 Nemaska Lithium Inc Métodos para o tratamento de materiais que contêm lítio
CA2996651C (en) 2015-08-27 2021-06-01 Nemaska Lithium Inc. Method for preparing lithium hydroxide and lithium sulfate monohydrate using hydrogen depolarized anode
CA3014623C (en) * 2016-02-18 2023-08-22 Gary Donald Johnson Lithium recovery from phosphate minerals
PT109396A (pt) * 2016-05-18 2017-11-20 Inst Superior Tecnico Processo de extração de lítio de minérios e concentrados por ativação mecânica e reação com ácido sulfúrico
CN107475513B (zh) * 2016-07-11 2019-04-23 光鼎国际控股集团有限公司 从含铷云母矿中浸出铷钾铝的方法
CA2940509A1 (en) 2016-08-26 2018-02-26 Nemaska Lithium Inc. Processes for treating aqueous compositions comprising lithium sulfate and sulfuric acid
RU2634559C1 (ru) * 2016-09-19 2017-10-31 Федеральное государственное автономное образовательное учреждение высшего образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина Способ переработки лепидолитового концентрата
CN108002410B (zh) * 2016-10-31 2019-10-18 湖南金源新材料股份有限公司 从低含量萃取尾水中回收锂及萃取尾水的循环利用方法
KR102701451B1 (ko) 2017-05-30 2024-09-03 리-싸이클 코포레이션 배터리로부터 물질을 회수하기 위한 방법, 장치 및 시스템
CN107815557A (zh) * 2017-10-16 2018-03-20 福州大学 一种锂辉石管道反应提锂工艺
CN107974565B (zh) * 2017-11-21 2022-03-29 东北大学 一种铝电解质中锂元素选择性硝酸浸出的方法
AU2018373507B2 (en) 2017-11-22 2024-02-22 Nemaska Lithium Inc. Processes for preparing hydroxides and oxides of various metals and derivatives thereof
AU2019262080B2 (en) * 2018-04-30 2024-02-22 Cornish Lithium plc Improved mica processing
AU2019262079B2 (en) * 2018-04-30 2024-02-22 Cornish Lithium plc Processing of silicate minerals
US11180860B2 (en) 2018-05-18 2021-11-23 California Institute Of Technology Process to convert reduced sulfur species and water into hydrogen and sulfuric acid
EP3802892B1 (en) * 2018-05-30 2023-08-30 Lithium Australia NL Process for recovering lithium phosphate and lithium sulfate from lithium-bearing silicates
CN109055737A (zh) * 2018-09-03 2018-12-21 核工业北京化工冶金研究院 一种硫酸浸出锂云母矿的方法
CN109052436B (zh) * 2018-09-21 2022-01-07 深圳市德方纳米科技股份有限公司 一种由锂磷铝石制备含锂化合物的方法
EP3670686A1 (en) * 2018-12-21 2020-06-24 A.C.N. 630 589 507 Pty Ltd Battery recycling process
CN113825848A (zh) * 2019-03-29 2021-12-21 锂业美洲公司 从沉积粘土中提取锂的方法
CA3141478A1 (en) 2019-05-22 2020-11-26 Nemaska Lithium Inc. Processes for preparing hydroxides and oxides of various metals and derivatives thereof
WO2021030529A1 (en) 2019-08-13 2021-02-18 California Institute Of Technology Process to make calcium oxide or ordinary portland cement from calcium bearing rocks and minerals
US10995014B1 (en) 2020-07-10 2021-05-04 Northvolt Ab Process for producing crystallized metal sulfates
CN113955777A (zh) * 2020-07-21 2022-01-21 承德石油高等专科学校 一种土壤湿法提取铷盐的方法
CN111996392B (zh) * 2020-07-22 2022-07-15 中国地质科学院郑州矿产综合利用研究所 从锂云母中提取铯和铷的方法
CN112129744B (zh) * 2020-09-07 2022-01-11 长沙矿冶研究院有限责任公司 一种矿石中锂的化学物相分析方法
EP4230754A4 (en) * 2020-10-19 2025-07-16 Kanto Denka Kogyo Kk LITHIUM RECOVERY PROCESS
RU2749598C1 (ru) * 2020-11-30 2021-06-15 Общество с ограниченной ответственностью "Объединенная Компания РУСАЛ Инженерно-технологический центр" Способ переработки слюдяного концентрата
CN112551555A (zh) * 2020-12-30 2021-03-26 广西天源新能源材料有限公司 一种基于盐湖矿石与锂聚合物的元明粉制备方法
JP7243749B2 (ja) * 2021-02-17 2023-03-22 三菱マテリアル株式会社 有価金属の回収方法及び回収装置
AU2022251147A1 (en) * 2021-04-01 2023-02-23 Cornish Lithium plc Lithium carbonate recovery process
EP4409048A4 (en) * 2021-10-01 2025-07-16 Li Tech Pty Ltd PREPARATION OF ALKALINE SALT SOLUTIONS
CN114751434B (zh) * 2022-04-28 2023-11-24 中国地质科学院郑州矿产综合利用研究所 一种沉积型锂资源的综合回收利用方法
CN115287469B (zh) * 2022-07-21 2024-03-29 湖北金泉新材料有限公司 一种从黏土型锂矿中选择性提锂的方法
CN115448318B (zh) * 2022-09-13 2024-01-26 湖南绿脉环保科技股份有限公司 一种锂渣提取硅铝的综合回收利用方法
CN115478176A (zh) * 2022-10-10 2022-12-16 河北铸合集团兴隆县矿业有限公司 一种锂云母矿物中锂铷铯盐的高效共同提取方法
CN115725857A (zh) * 2022-11-25 2023-03-03 昆明理工大学 低品位云母矿微波氯化焙烧水浸提铷的方法
CN115744942A (zh) * 2022-11-28 2023-03-07 江西永兴特钢新能源科技有限公司 一种利用沉锂母液除去锂云母浸出卤水杂质的方法
CN116590539B (zh) * 2023-06-06 2026-04-28 贵州省地质矿产中心实验室(贵州省矿产品黄金宝石制品质量检验站) 一种锂铝酸热一体化提取方法
CN116770097B (zh) * 2023-06-27 2025-08-08 中南大学 一种利用铝电解槽大修渣协同提锂的方法
CN120648918A (zh) * 2024-03-15 2025-09-16 美卓芬兰有限公司 锂精矿的新型大气压浸出方法
CN120648917A (zh) * 2024-03-15 2025-09-16 美卓芬兰有限公司 未煅烧的锂精矿的新型大气压浸出方法
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Also Published As

Publication number Publication date
US10450630B2 (en) 2019-10-22
PT3204528T (pt) 2020-07-15
US20170233848A1 (en) 2017-08-17
EP3204528B1 (en) 2020-07-01
WO2016054683A1 (en) 2016-04-14
ES2806425T3 (es) 2021-02-17
CA2962070A1 (en) 2016-04-14
EP3204528A1 (en) 2017-08-16
JP2017537221A (ja) 2017-12-14
CA2962070C (en) 2023-10-24
EP3204528A4 (en) 2018-05-23
AU2015330958A1 (en) 2017-03-23
AU2015330958B2 (en) 2019-11-28

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