JP2017537221A5 - - Google Patents
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- Publication number
- JP2017537221A5 JP2017537221A5 JP2017518134A JP2017518134A JP2017537221A5 JP 2017537221 A5 JP2017537221 A5 JP 2017537221A5 JP 2017518134 A JP2017518134 A JP 2017518134A JP 2017518134 A JP2017518134 A JP 2017518134A JP 2017537221 A5 JP2017537221 A5 JP 2017537221A5
- Authority
- JP
- Japan
- Prior art keywords
- leaching
- lithium
- salt
- solution
- monovalent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 23
- 238000002386 leaching Methods 0.000 claims 21
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 9
- 229910052744 lithium Inorganic materials 0.000 claims 9
- 239000012535 impurity Substances 0.000 claims 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 6
- 239000000706 filtrate Substances 0.000 claims 6
- 150000003839 salts Chemical class 0.000 claims 6
- 229940037003 alum Drugs 0.000 claims 5
- 238000001914 filtration Methods 0.000 claims 4
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 4
- 239000010445 mica Substances 0.000 claims 4
- 229910052618 mica group Inorganic materials 0.000 claims 4
- 239000011707 mineral Substances 0.000 claims 4
- 239000000047 product Substances 0.000 claims 4
- 239000002002 slurry Substances 0.000 claims 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 239000002253 acid Substances 0.000 claims 3
- 238000010908 decantation Methods 0.000 claims 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims 2
- FLJPGEWQYJVDPF-UHFFFAOYSA-L caesium sulfate Chemical compound [Cs+].[Cs+].[O-]S([O-])(=O)=O FLJPGEWQYJVDPF-UHFFFAOYSA-L 0.000 claims 2
- -1 cation salt Chemical class 0.000 claims 2
- 238000001816 cooling Methods 0.000 claims 2
- 238000001704 evaporation Methods 0.000 claims 2
- 230000008020 evaporation Effects 0.000 claims 2
- 238000000605 extraction Methods 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 229910052751 metal Inorganic materials 0.000 claims 2
- 239000002184 metal Substances 0.000 claims 2
- 150000002739 metals Chemical class 0.000 claims 2
- 238000001556 precipitation Methods 0.000 claims 2
- 238000010298 pulverizing process Methods 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- 239000000377 silicon dioxide Substances 0.000 claims 2
- IRPGOXJVTQTAAN-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanal Chemical compound FC(F)(F)C(F)(F)C=O IRPGOXJVTQTAAN-UHFFFAOYSA-N 0.000 claims 1
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminum fluoride Inorganic materials F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 claims 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- 241000560556 Cardites Species 0.000 claims 1
- BDAGIHXWWSANSR-UHFFFAOYSA-M Formate Chemical compound [O-]C=O BDAGIHXWWSANSR-UHFFFAOYSA-M 0.000 claims 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims 1
- 239000004115 Sodium Silicate Substances 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims 1
- 239000010953 base metal Substances 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 238000002425 crystallisation Methods 0.000 claims 1
- 230000008025 crystallization Effects 0.000 claims 1
- 239000011777 magnesium Substances 0.000 claims 1
- 229910052749 magnesium Inorganic materials 0.000 claims 1
- 230000014759 maintenance of location Effects 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 claims 1
- 239000011572 manganese Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 239000002244 precipitate Substances 0.000 claims 1
- 230000001376 precipitating effect Effects 0.000 claims 1
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 claims 1
- 229910000344 rubidium sulfate Inorganic materials 0.000 claims 1
- 239000011833 salt mixture Substances 0.000 claims 1
- 238000010956 selective crystallization Methods 0.000 claims 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims 1
- 229910052911 sodium silicate Inorganic materials 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU2014904050A AU2014904050A0 (en) | 2014-10-10 | Recovery Process | |
| AU2014904050 | 2014-10-10 | ||
| PCT/AU2015/000608 WO2016054683A1 (en) | 2014-10-10 | 2015-10-09 | Recovery process |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017537221A JP2017537221A (ja) | 2017-12-14 |
| JP2017537221A5 true JP2017537221A5 (enExample) | 2018-05-31 |
| JP6687608B2 JP6687608B2 (ja) | 2020-04-22 |
Family
ID=55652390
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017518134A Active JP6687608B2 (ja) | 2014-10-10 | 2015-10-09 | 回収方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10450630B2 (enExample) |
| EP (1) | EP3204528B1 (enExample) |
| JP (1) | JP6687608B2 (enExample) |
| AU (1) | AU2015330958B2 (enExample) |
| CA (1) | CA2962070C (enExample) |
| ES (1) | ES2806425T3 (enExample) |
| PT (1) | PT3204528T (enExample) |
| WO (1) | WO2016054683A1 (enExample) |
Families Citing this family (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RS65609B1 (sr) | 2012-05-30 | 2024-07-31 | Nemaska Lithium Inc | Postupci za dobijanje litijum karbonata |
| RS61656B1 (sr) | 2013-03-15 | 2021-04-29 | Nemaska Lithium Inc | Postupak za dobijanje litijum hidroksida |
| KR102614113B1 (ko) | 2013-10-23 | 2023-12-13 | 네마스카 리튬 인코포레이션 | 리튬 카보네이트의 제조방법 |
| CA3086843C (en) | 2014-02-24 | 2021-06-22 | Nemaska Lithium Inc. | Methods for treating lithium-containing materials |
| WO2017031595A1 (en) | 2015-08-27 | 2017-03-02 | Nemaska Lithium Inc. | Methods for treating lithium-containing materials |
| AU2017220394B2 (en) * | 2016-02-18 | 2021-12-23 | Cornish Lithium plc | Lithium recovery from phosphate minerals |
| PT109396A (pt) * | 2016-05-18 | 2017-11-20 | Inst Superior Tecnico | Processo de extração de lítio de minérios e concentrados por ativação mecânica e reação com ácido sulfúrico |
| CN107475513B (zh) * | 2016-07-11 | 2019-04-23 | 光鼎国际控股集团有限公司 | 从含铷云母矿中浸出铷钾铝的方法 |
| CA2940509A1 (en) | 2016-08-26 | 2018-02-26 | Nemaska Lithium Inc. | Processes for treating aqueous compositions comprising lithium sulfate and sulfuric acid |
| RU2634559C1 (ru) * | 2016-09-19 | 2017-10-31 | Федеральное государственное автономное образовательное учреждение высшего образования "Уральский федеральный университет имени первого Президента России Б.Н. Ельцина | Способ переработки лепидолитового концентрата |
| CN108002410B (zh) * | 2016-10-31 | 2019-10-18 | 湖南金源新材料股份有限公司 | 从低含量萃取尾水中回收锂及萃取尾水的循环利用方法 |
| AU2018276326B2 (en) | 2017-05-30 | 2021-07-15 | Li-Cycle Corp. | A process, apparatus, and system for recovering materials from batteries |
| CN107815557A (zh) * | 2017-10-16 | 2018-03-20 | 福州大学 | 一种锂辉石管道反应提锂工艺 |
| CN107974565B (zh) * | 2017-11-21 | 2022-03-29 | 东北大学 | 一种铝电解质中锂元素选择性硝酸浸出的方法 |
| JP7194185B2 (ja) | 2017-11-22 | 2022-12-21 | ネマスカ リチウム インコーポレーテッド | 様々な金属の水酸化物および酸化物ならびにそれらの誘導体の調製プロセス |
| AU2019262079B2 (en) * | 2018-04-30 | 2024-02-22 | Cornish Lithium plc | Processing of silicate minerals |
| WO2019210351A1 (en) * | 2018-04-30 | 2019-11-07 | Silica Technology Pty Ltd | Improved mica processing |
| AU2019271388B2 (en) | 2018-05-18 | 2023-05-18 | California Institute Of Technology | Process to convert reduced sulfur species and water into hydrogen and sulfuric acid |
| EP3802892B1 (en) * | 2018-05-30 | 2023-08-30 | Lithium Australia NL | Process for recovering lithium phosphate and lithium sulfate from lithium-bearing silicates |
| CN109055737A (zh) * | 2018-09-03 | 2018-12-21 | 核工业北京化工冶金研究院 | 一种硫酸浸出锂云母矿的方法 |
| CN109052436B (zh) * | 2018-09-21 | 2022-01-07 | 深圳市德方纳米科技股份有限公司 | 一种由锂磷铝石制备含锂化合物的方法 |
| EP3670686A1 (en) * | 2018-12-21 | 2020-06-24 | A.C.N. 630 589 507 Pty Ltd | Battery recycling process |
| WO2020232556A1 (en) | 2019-05-22 | 2020-11-26 | Nemaska Lithium Inc. | Processes for preparing hydroxides and oxides of various metals and derivatives thereof |
| KR20220058908A (ko) | 2019-08-13 | 2022-05-10 | 캘리포니아 인스티튜트 오브 테크놀로지 | 칼슘 보유 암석 및 광물로부터 칼슘 산화물 또는 일반 포틀랜드 시멘트를 제조하는 방법 |
| US10995014B1 (en) | 2020-07-10 | 2021-05-04 | Northvolt Ab | Process for producing crystallized metal sulfates |
| CN113955777A (zh) * | 2020-07-21 | 2022-01-21 | 承德石油高等专科学校 | 一种土壤湿法提取铷盐的方法 |
| CN111996392B (zh) * | 2020-07-22 | 2022-07-15 | 中国地质科学院郑州矿产综合利用研究所 | 从锂云母中提取铯和铷的方法 |
| CN112129744B (zh) * | 2020-09-07 | 2022-01-11 | 长沙矿冶研究院有限责任公司 | 一种矿石中锂的化学物相分析方法 |
| EP4230754A4 (en) * | 2020-10-19 | 2025-07-16 | Kanto Denka Kogyo Kk | LITHIUM RECOVERY PROCESS |
| RU2749598C1 (ru) * | 2020-11-30 | 2021-06-15 | Общество с ограниченной ответственностью "Объединенная Компания РУСАЛ Инженерно-технологический центр" | Способ переработки слюдяного концентрата |
| CN112551555A (zh) * | 2020-12-30 | 2021-03-26 | 广西天源新能源材料有限公司 | 一种基于盐湖矿石与锂聚合物的元明粉制备方法 |
| JP7243749B2 (ja) * | 2021-02-17 | 2023-03-22 | 三菱マテリアル株式会社 | 有価金属の回収方法及び回収装置 |
| CN117062778A (zh) * | 2021-04-01 | 2023-11-14 | 锂科技有限公司 | 碳酸锂回收工艺 |
| EP4409048A4 (en) * | 2021-10-01 | 2025-07-16 | Li Tech Pty Ltd | PREPARATION OF ALKALINE SALT SOLUTIONS |
| CN114751434B (zh) * | 2022-04-28 | 2023-11-24 | 中国地质科学院郑州矿产综合利用研究所 | 一种沉积型锂资源的综合回收利用方法 |
| CN115287469B (zh) * | 2022-07-21 | 2024-03-29 | 湖北金泉新材料有限公司 | 一种从黏土型锂矿中选择性提锂的方法 |
| CN115448318B (zh) * | 2022-09-13 | 2024-01-26 | 湖南绿脉环保科技股份有限公司 | 一种锂渣提取硅铝的综合回收利用方法 |
| CN115478176A (zh) * | 2022-10-10 | 2022-12-16 | 河北铸合集团兴隆县矿业有限公司 | 一种锂云母矿物中锂铷铯盐的高效共同提取方法 |
| CN115725857A (zh) * | 2022-11-25 | 2023-03-03 | 昆明理工大学 | 低品位云母矿微波氯化焙烧水浸提铷的方法 |
| CN115744942A (zh) * | 2022-11-28 | 2023-03-07 | 江西永兴特钢新能源科技有限公司 | 一种利用沉锂母液除去锂云母浸出卤水杂质的方法 |
| CN116770097B (zh) * | 2023-06-27 | 2025-08-08 | 中南大学 | 一种利用铝电解槽大修渣协同提锂的方法 |
| CN120648917A (zh) * | 2024-03-15 | 2025-09-16 | 美卓芬兰有限公司 | 未煅烧的锂精矿的新型大气压浸出方法 |
| CN120648918A (zh) * | 2024-03-15 | 2025-09-16 | 美卓芬兰有限公司 | 锂精矿的新型大气压浸出方法 |
| WO2025226431A1 (en) * | 2024-04-25 | 2025-10-30 | Albemarle Corporation | Method of alkaline leaching of useful metals from lithium-ion batteries |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2044018A (en) * | 1933-11-09 | 1936-06-16 | Rosett Walter | Separation of lithium salts |
| US2940820A (en) | 1958-03-10 | 1960-06-14 | American Lithium Chemicals Inc | Process for recovering alkali metal values from lepidolite |
| FR1256646A (fr) | 1960-02-11 | 1961-03-24 | Saint Gobain | Procédé d'extraction du lithium du lépidolite |
| NO143583C (no) | 1979-02-13 | 1983-01-06 | Elkem Spigerverket As | Fremgangsmaate for utluting av silikater med syre. |
| CN1003008B (zh) * | 1985-04-01 | 1989-01-04 | 广州有色金属研究院 | 用硫酸钾法处理锂云母制取碳酸锂的工艺方法 |
| DE3622105A1 (de) * | 1986-07-02 | 1988-01-07 | Metallgesellschaft Ag | Verfahren zur gewinnung von lithiumcarbonat |
| CN100503849C (zh) * | 2006-11-24 | 2009-06-24 | 江西赣锋锂业股份有限公司 | 硫酸法锂云母提锂工艺中精硫酸锂溶液的生产方法 |
| JP2009270189A (ja) * | 2008-05-07 | 2009-11-19 | Kee:Kk | 高純度水酸化リチウムの製法 |
| AU2010341402B2 (en) * | 2010-01-07 | 2014-01-30 | Tianqi Lithium Corporation | Process for the production of lithium carbonate |
| CN101974684B (zh) * | 2010-11-26 | 2012-04-11 | 山东明瑞化工集团有限公司 | 锂云母浸取液除杂工艺 |
| CN102173438A (zh) * | 2011-01-25 | 2011-09-07 | 宜春学院 | 一种利用钽铌尾矿锂云母制备碳酸锂获得副产物石膏的方法 |
| CN102139894A (zh) * | 2011-01-25 | 2011-08-03 | 宜春银锂新能源有限责任公司 | 一种利用钽铌尾矿锂云母制备电池级碳酸锂的新方法 |
| AU2013237292B2 (en) * | 2012-03-19 | 2015-09-10 | Metso Finland Oy | Method for recovering lithium carbonate |
| CN102649996A (zh) | 2012-05-24 | 2012-08-29 | 张韵 | 一种锂云母循环酸浸提取工艺 |
| CN102718234B (zh) * | 2012-07-12 | 2014-05-14 | 张勇 | 从锂云母中提取碳酸锂的方法 |
| AU2013201833B2 (en) * | 2012-08-13 | 2014-07-17 | Reed Advanced Materials Pty Ltd | Processing of Lithium Containing Ore |
| CN102849759B (zh) * | 2012-10-11 | 2014-07-23 | 江西本源新材料科技有限公司 | 氟化锂的提取方法 |
-
2015
- 2015-10-09 AU AU2015330958A patent/AU2015330958B2/en active Active
- 2015-10-09 EP EP15848288.5A patent/EP3204528B1/en active Active
- 2015-10-09 WO PCT/AU2015/000608 patent/WO2016054683A1/en not_active Ceased
- 2015-10-09 PT PT158482885T patent/PT3204528T/pt unknown
- 2015-10-09 CA CA2962070A patent/CA2962070C/en active Active
- 2015-10-09 JP JP2017518134A patent/JP6687608B2/ja active Active
- 2015-10-09 US US15/514,688 patent/US10450630B2/en active Active
- 2015-10-09 ES ES15848288T patent/ES2806425T3/es active Active
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