JP6445438B2 - アシルホスファン類の製造方法 - Google Patents
アシルホスファン類の製造方法 Download PDFInfo
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- JP6445438B2 JP6445438B2 JP2015533630A JP2015533630A JP6445438B2 JP 6445438 B2 JP6445438 B2 JP 6445438B2 JP 2015533630 A JP2015533630 A JP 2015533630A JP 2015533630 A JP2015533630 A JP 2015533630A JP 6445438 B2 JP6445438 B2 JP 6445438B2
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- formula
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/505—Preparation; Separation; Purification; Stabilisation
- C07F9/5063—Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds
- C07F9/5072—Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds from starting materials having the structure P-H
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/572—Five-membered rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/576—Six-membered rings
- C07F9/58—Pyridine rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/655—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
- C07F9/65515—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a five-membered ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/46—Polymerisation initiated by wave energy or particle radiation
- C08F2/48—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
- C08F2/50—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light with sensitising agents
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F218/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid or of a haloformic acid
- C08F218/02—Esters of monocarboxylic acids
- C08F218/04—Vinyl esters
- C08F218/08—Vinyl acetate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Polymerisation Methods In General (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12006822 | 2012-10-01 | ||
| EP12006822.6 | 2012-10-01 | ||
| EP13003616 | 2013-07-18 | ||
| EP13003616.3 | 2013-07-18 | ||
| PCT/EP2013/070378 WO2014053455A1 (en) | 2012-10-01 | 2013-09-30 | A process for the preparation of acylphosphanes |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015532275A JP2015532275A (ja) | 2015-11-09 |
| JP2015532275A5 JP2015532275A5 (enExample) | 2018-03-08 |
| JP6445438B2 true JP6445438B2 (ja) | 2018-12-26 |
Family
ID=49301475
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015533630A Active JP6445438B2 (ja) | 2012-10-01 | 2013-09-30 | アシルホスファン類の製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US9701700B2 (enExample) |
| EP (2) | EP2903995B1 (enExample) |
| JP (1) | JP6445438B2 (enExample) |
| KR (1) | KR102135300B1 (enExample) |
| CN (2) | CN108383874B (enExample) |
| BR (1) | BR112015007295B1 (enExample) |
| ES (2) | ES2881686T3 (enExample) |
| RU (1) | RU2719592C2 (enExample) |
| WO (1) | WO2014053455A1 (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3031798B1 (en) | 2014-12-10 | 2017-09-27 | Belenos Clean Power Holding AG | A novel cross-linker for the preparation of a new family of single ion conduction polymers for electrochemical devices and such polymers |
| EP3296301A1 (en) | 2016-09-19 | 2018-03-21 | ETH Zürich | A versatile process for the preparation of acylphosphines |
| JP2020500092A (ja) | 2016-11-16 | 2020-01-09 | エコール・ポリテクニーク・フェデラル・ドゥ・ローザンヌ （ウ・ペ・エフ・エル）Ｅｃｏｌｅ Ｐｏｌｙｔｅｃｈｎｉｑｕｅ Ｆｅｄｅｒａｌｅ Ｄｅ Ｌａｕｓａｎｎｅ （Ｅｐｆｌ） | 光重合性骨充填材材料 |
| EP3409680B1 (en) * | 2017-05-30 | 2021-01-06 | IGM Group B.V. | Synthesis of bis(acyl)phosphines by activation of unreactive metal phosphides |
| CN107400144B (zh) * | 2017-08-03 | 2020-04-14 | 深圳有为技术控股集团有限公司 | 酰基膦(氧)化合物及其制备方法和应用 |
| EP3539924A1 (en) | 2018-03-14 | 2019-09-18 | ETH Zurich | Novel vinyl phosphines and photo-initiators obtainable therefrom |
| EP3539969A1 (en) | 2018-03-14 | 2019-09-18 | ETH Zurich | Novel photo-initiators and their application |
| EP3847179A1 (en) | 2018-09-07 | 2021-07-14 | IGM Resins Italia S.r.l. | Multifunctional bisacylphosphine oxide photoinitiators |
| EP3747942A1 (en) | 2019-06-05 | 2020-12-09 | EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt | Bridged phosphorus based flame retardants |
| CN114728520B (zh) * | 2019-11-11 | 2024-03-08 | 富士胶片株式会社 | 活性能量射线固化型油墨及图像记录方法 |
| EP4114339A1 (en) | 2020-05-29 | 2023-01-11 | Lumendo AG | Crosslinkable prepolymers for chemically stable polymer gels |
| CN112547122A (zh) * | 2020-12-18 | 2021-03-26 | 商河知济新材料技术中心 | 叔丁醇盐和吡啶盐在制备一种光引发剂中的用途 |
| CN120187778A (zh) | 2022-09-15 | 2025-06-20 | 埃肯有机硅法国简易股份公司 | 用于生产有机硅弹性体制品的增材制造方法 |
| CN120365331B (zh) * | 2025-06-26 | 2025-11-04 | 北京大学深圳研究生院 | 一种光引发剂及其制备方法 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2957931A (en) * | 1949-07-28 | 1960-10-25 | Socony Mobil Oil Co Inc | Synthesis of compounds having a carbonphosphorus linkage |
| US2822376A (en) * | 1957-02-27 | 1958-02-04 | American Cyanamid Co | Reaction of phosphine with alpha, beta-unsatu-rated compounds |
| TW303379B (enExample) * | 1994-03-02 | 1997-04-21 | Ciba Sc Holding Ag | |
| DE59506142D1 (de) * | 1994-07-29 | 1999-07-15 | Ciba Sc Pfersee Gmbh | Verfahren zur Herstellung von Diestern von Phosphonocarbonsäurederivaten |
| SG53043A1 (en) | 1996-08-28 | 1998-09-28 | Ciba Geigy Ag | Molecular complex compounds as photoinitiators |
| AU760237B2 (en) | 1998-11-30 | 2003-05-08 | Igm Group B.V. | Process for preparing acylphosphines and derivatives |
| JP2001200007A (ja) * | 2000-01-19 | 2001-07-24 | Shin Etsu Chem Co Ltd | 光硬化性樹脂組成物及び光ファイバー用被覆材 |
| GB2360283B (en) | 2000-02-08 | 2002-08-21 | Ciba Sc Holding Ag | Monoacylarylphosphines and acylphosphine oxides and sulphides |
| KR20050044549A (ko) | 2001-11-20 | 2005-05-12 | 시바 스페셜티 케미칼스 홀딩 인크. | 아실포스핀 및 이의 유도체의 멀티머 형태 |
| JP2003228150A (ja) * | 2002-02-04 | 2003-08-15 | Konica Corp | 光熱写真画像形成材料 |
| BR0312133A (pt) | 2002-06-11 | 2005-04-05 | Ciba Sc Holding Ag | Formas dìmeras e multìmeras de óxidos de monoacifosfinas e bis-acifosfinas, processo para a preparação das mesmas, bem como composição fotopolimerizável |
| WO2005014605A1 (en) | 2003-07-18 | 2005-02-17 | Ciba Specialty Chemicals Holding Inc. | Process for preparing acylphosphanes and derivatives thereof |
| EP1765878B1 (en) * | 2004-04-15 | 2010-12-08 | Basf Se | Process for photocuring with light emitting diodes |
| EP1814891B1 (en) * | 2004-11-23 | 2011-01-26 | Basf Se | Bisacylphosphanes and their use as photoinitiators; process for preparing acylphosphanes |
| WO2006074983A1 (en) | 2005-01-17 | 2006-07-20 | Ciba Specialty Chemicals Holding Inc. | Process for preparing acylphosphanes and their oxides and sulphides |
| JP2007272106A (ja) * | 2006-03-31 | 2007-10-18 | Fujifilm Corp | ホログラム記録媒体用組成物及びホログラム記録媒体 |
| WO2008003601A1 (en) | 2006-07-04 | 2008-01-10 | Ciba Holding Inc. | Water based concentrated product forms of photoinitiators made by a heterophase polymerization technique |
| EP2451847B1 (en) | 2009-07-06 | 2021-11-24 | IGM Group B.V. | Polymer-bound bisacylphosphine oxides |
| EP2558427B1 (en) | 2010-06-30 | 2017-05-31 | DSM IP Assets B.V. | D1492 liquid bapo photoinitiator and its use in radiation curable compositions |
-
2013
- 2013-09-30 CN CN201810249476.7A patent/CN108383874B/zh active Active
- 2013-09-30 EP EP13771462.2A patent/EP2903995B1/en active Active
- 2013-09-30 JP JP2015533630A patent/JP6445438B2/ja active Active
- 2013-09-30 KR KR1020157011628A patent/KR102135300B1/ko active Active
- 2013-09-30 CN CN201380051352.3A patent/CN104703995B/zh active Active
- 2013-09-30 BR BR112015007295-0A patent/BR112015007295B1/pt active IP Right Grant
- 2013-09-30 WO PCT/EP2013/070378 patent/WO2014053455A1/en not_active Ceased
- 2013-09-30 US US14/432,212 patent/US9701700B2/en active Active
- 2013-09-30 RU RU2015116292A patent/RU2719592C2/ru active
- 2013-09-30 ES ES19151535T patent/ES2881686T3/es active Active
- 2013-09-30 ES ES13771462T patent/ES2720760T3/es active Active
- 2013-09-30 EP EP19151535.2A patent/EP3508489B1/en active Active
-
2017
- 2017-05-24 US US15/603,467 patent/US10273258B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| US9701700B2 (en) | 2017-07-11 |
| CN108383874B (zh) | 2021-10-08 |
| ES2720760T3 (es) | 2019-07-24 |
| RU2015116292A (ru) | 2016-11-27 |
| ES2881686T3 (es) | 2021-11-30 |
| US10273258B2 (en) | 2019-04-30 |
| KR102135300B1 (ko) | 2020-08-27 |
| JP2015532275A (ja) | 2015-11-09 |
| WO2014053455A1 (en) | 2014-04-10 |
| EP2903995A1 (en) | 2015-08-12 |
| EP3508489A1 (en) | 2019-07-10 |
| KR20150064747A (ko) | 2015-06-11 |
| US20180002357A1 (en) | 2018-01-04 |
| BR112015007295B1 (pt) | 2021-12-14 |
| CN108383874A (zh) | 2018-08-10 |
| BR112015007295A2 (pt) | 2017-07-04 |
| CN104703995A (zh) | 2015-06-10 |
| CN104703995B (zh) | 2018-04-20 |
| EP3508489B1 (en) | 2021-04-14 |
| RU2719592C2 (ru) | 2020-04-21 |
| EP2903995B1 (en) | 2019-01-16 |
| US20150299231A1 (en) | 2015-10-22 |
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