JP2015532275A5 - - Google Patents
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- JP2015532275A5 JP2015532275A5 JP2015533630A JP2015533630A JP2015532275A5 JP 2015532275 A5 JP2015532275 A5 JP 2015532275A5 JP 2015533630 A JP2015533630 A JP 2015533630A JP 2015533630 A JP2015533630 A JP 2015533630A JP 2015532275 A5 JP2015532275 A5 JP 2015532275A5
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- Prior art keywords
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- 125000001424 substituent group Chemical group 0.000 claims 90
- 229910052739 hydrogen Inorganic materials 0.000 claims 25
- 239000001257 hydrogen Substances 0.000 claims 25
- GBXQPDCOMJJCMJ-UHFFFAOYSA-M trimethyl-[6-(trimethylazaniumyl)hexyl]azanium;bromide Chemical compound [Br-].C[N+](C)(C)CCCCCC[N+](C)(C)C GBXQPDCOMJJCMJ-UHFFFAOYSA-M 0.000 claims 24
- 238000004519 manufacturing process Methods 0.000 claims 20
- 150000001875 compounds Chemical class 0.000 claims 18
- 150000002431 hydrogen Chemical group 0.000 claims 18
- 125000003118 aryl group Chemical group 0.000 claims 16
- 125000000217 alkyl group Chemical group 0.000 claims 15
- 125000000524 functional group Chemical group 0.000 claims 15
- 125000004093 cyano group Chemical group *C#N 0.000 claims 14
- 125000000623 heterocyclic group Chemical group 0.000 claims 13
- 125000006656 (C2-C4) alkenyl group Chemical group 0.000 claims 12
- 125000003342 alkenyl group Chemical group 0.000 claims 12
- 125000004356 hydroxy functional group Chemical group O* 0.000 claims 12
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 9
- 229910052736 halogen Inorganic materials 0.000 claims 9
- 150000002367 halogens Chemical class 0.000 claims 9
- 229910052799 carbon Inorganic materials 0.000 claims 8
- 125000004432 carbon atom Chemical group C* 0.000 claims 8
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 7
- 125000004437 phosphorous atom Chemical group 0.000 claims 6
- 229910052698 phosphorus Inorganic materials 0.000 claims 6
- 150000001450 anions Chemical class 0.000 claims 5
- 125000000592 heterocycloalkyl group Chemical group 0.000 claims 5
- 125000004105 2-pyridyl group Chemical group N1=C([*])C([H])=C([H])C([H])=C1[H] 0.000 claims 4
- 125000000852 azido group Chemical group *N=[N+]=[N-] 0.000 claims 4
- 150000001721 carbon Chemical group 0.000 claims 4
- -1 guanidinium ions Chemical class 0.000 claims 4
- 229910021645 metal ion Inorganic materials 0.000 claims 4
- 150000001336 alkenes Chemical class 0.000 claims 3
- VILAVOFMIJHSJA-UHFFFAOYSA-N dicarbon monoxide Chemical compound [C]=C=O VILAVOFMIJHSJA-UHFFFAOYSA-N 0.000 claims 3
- 125000004648 C2-C8 alkenyl group Chemical group 0.000 claims 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 2
- 125000002091 cationic group Chemical group 0.000 claims 2
- 150000001768 cations Chemical class 0.000 claims 2
- ISNICOKBNZOJQG-UHFFFAOYSA-O guanidinium ion Chemical compound C[NH+]=C(N(C)C)N(C)C ISNICOKBNZOJQG-UHFFFAOYSA-O 0.000 claims 2
- 238000000034 method Methods 0.000 claims 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 2
- 125000004043 oxo group Chemical group O=* 0.000 claims 2
- 229910052760 oxygen Inorganic materials 0.000 claims 2
- 239000001301 oxygen Substances 0.000 claims 2
- 229910052717 sulfur Chemical group 0.000 claims 2
- 239000011593 sulfur Chemical group 0.000 claims 2
- XTFIVUDBNACUBN-UHFFFAOYSA-N 1,3,5-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)C1 XTFIVUDBNACUBN-UHFFFAOYSA-N 0.000 claims 1
- PCHXZXKMYCGVFA-UHFFFAOYSA-N 1,3-diazetidine-2,4-dione Chemical compound O=C1NC(=O)N1 PCHXZXKMYCGVFA-UHFFFAOYSA-N 0.000 claims 1
- ZMTAQDWIPRSXOY-UHFFFAOYSA-N 3-bis(2,4,6-trimethylbenzoyl)phosphanylpropanoic acid 2-ethyl-2-(hydroxymethyl)propane-1,3-diol Chemical compound CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.C(O)C(CC)(CO)CO ZMTAQDWIPRSXOY-UHFFFAOYSA-N 0.000 claims 1
- BBCVASXKVWMCRO-UHFFFAOYSA-N 3-bis(2,4,6-trimethylbenzoyl)phosphorylpropanoic acid 2-ethyl-2-(hydroxymethyl)propane-1,3-diol prop-2-enoic acid Chemical compound CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.C(C=C)(=O)O.C(O)C(CC)(CO)CO BBCVASXKVWMCRO-UHFFFAOYSA-N 0.000 claims 1
- QHMRXWRXXYQGLJ-UHFFFAOYSA-N CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.C(C=C)(=O)O.C(C=C)(=O)O.C(O)C(CC)(CO)CO Chemical compound CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.C(C=C)(=O)O.C(C=C)(=O)O.C(O)C(CC)(CO)CO QHMRXWRXXYQGLJ-UHFFFAOYSA-N 0.000 claims 1
- XBSDBWCSLFTVST-UHFFFAOYSA-N CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.C(O)C(CC)(CO)CO Chemical compound CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.CC1=C(C(=O)P(=O)(C(C2=C(C=C(C=C2C)C)C)=O)CCC(=O)O)C(=CC(=C1)C)C.C(O)C(CC)(CO)CO XBSDBWCSLFTVST-UHFFFAOYSA-N 0.000 claims 1
- GPCTWKMATYKSET-UHFFFAOYSA-N CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.C(C=C)(=O)O.C(C=C)(=O)O.C(O)C(CC)(CO)CO Chemical compound CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.C(C=C)(=O)O.C(C=C)(=O)O.C(O)C(CC)(CO)CO GPCTWKMATYKSET-UHFFFAOYSA-N 0.000 claims 1
- NAXXTFDPUTUROV-UHFFFAOYSA-N CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.C(C=C)(=O)O.C(O)C(CC)(CO)CO Chemical compound CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.CC1=C(C(=O)P(CCC(=O)O)C(C2=C(C=C(C=C2C)C)C)=O)C(=CC(=C1)C)C.C(C=C)(=O)O.C(O)C(CC)(CO)CO NAXXTFDPUTUROV-UHFFFAOYSA-N 0.000 claims 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical group [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical group [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- REDXJYDRNCIFBQ-UHFFFAOYSA-N aluminium(3+) Chemical compound [Al+3] REDXJYDRNCIFBQ-UHFFFAOYSA-N 0.000 claims 1
- 230000001548 androgenic effect Effects 0.000 claims 1
- OHJMTUPIZMNBFR-UHFFFAOYSA-N biuret Chemical compound NC(=O)NC(N)=O OHJMTUPIZMNBFR-UHFFFAOYSA-N 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- KWEDUNSJJZVRKR-UHFFFAOYSA-N carbononitridic azide Chemical compound [N-]=[N+]=NC#N KWEDUNSJJZVRKR-UHFFFAOYSA-N 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- 125000001072 heteroaryl group Chemical group 0.000 claims 1
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 claims 1
- 229910052744 lithium Inorganic materials 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 125000004433 nitrogen atom Chemical group N* 0.000 claims 1
- HXSACZWWBYWLIS-UHFFFAOYSA-N oxadiazine-4,5,6-trione Chemical compound O=C1ON=NC(=O)C1=O HXSACZWWBYWLIS-UHFFFAOYSA-N 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 239000011591 potassium Chemical group 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011734 sodium Chemical group 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- AVWRKZWQTYIKIY-UHFFFAOYSA-N urea-1-carboxylic acid Chemical group NC(=O)NC(O)=O AVWRKZWQTYIKIY-UHFFFAOYSA-N 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12006822 | 2012-10-01 | ||
| EP12006822.6 | 2012-10-01 | ||
| EP13003616 | 2013-07-18 | ||
| EP13003616.3 | 2013-07-18 | ||
| PCT/EP2013/070378 WO2014053455A1 (en) | 2012-10-01 | 2013-09-30 | A process for the preparation of acylphosphanes |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015532275A JP2015532275A (ja) | 2015-11-09 |
| JP2015532275A5 true JP2015532275A5 (enExample) | 2018-03-08 |
| JP6445438B2 JP6445438B2 (ja) | 2018-12-26 |
Family
ID=49301475
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015533630A Active JP6445438B2 (ja) | 2012-10-01 | 2013-09-30 | アシルホスファン類の製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US9701700B2 (enExample) |
| EP (2) | EP2903995B1 (enExample) |
| JP (1) | JP6445438B2 (enExample) |
| KR (1) | KR102135300B1 (enExample) |
| CN (2) | CN108383874B (enExample) |
| BR (1) | BR112015007295B1 (enExample) |
| ES (2) | ES2881686T3 (enExample) |
| RU (1) | RU2719592C2 (enExample) |
| WO (1) | WO2014053455A1 (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3031798B1 (en) | 2014-12-10 | 2017-09-27 | Belenos Clean Power Holding AG | A novel cross-linker for the preparation of a new family of single ion conduction polymers for electrochemical devices and such polymers |
| EP3296301A1 (en) * | 2016-09-19 | 2018-03-21 | ETH Zürich | A versatile process for the preparation of acylphosphines |
| EP3541440A1 (en) | 2016-11-16 | 2019-09-25 | Ecole Polytechnique Federale de Lausanne (EPFL) | Photopolymerizable bone filler material |
| EP3409680B1 (en) * | 2017-05-30 | 2021-01-06 | IGM Group B.V. | Synthesis of bis(acyl)phosphines by activation of unreactive metal phosphides |
| CN107400144B (zh) * | 2017-08-03 | 2020-04-14 | 深圳有为技术控股集团有限公司 | 酰基膦(氧)化合物及其制备方法和应用 |
| EP3539924A1 (en) | 2018-03-14 | 2019-09-18 | ETH Zurich | Novel vinyl phosphines and photo-initiators obtainable therefrom |
| EP3539969A1 (en) | 2018-03-14 | 2019-09-18 | ETH Zurich | Novel photo-initiators and their application |
| EP3847179A1 (en) | 2018-09-07 | 2021-07-14 | IGM Resins Italia S.r.l. | Multifunctional bisacylphosphine oxide photoinitiators |
| EP3747942A1 (en) | 2019-06-05 | 2020-12-09 | EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt | Bridged phosphorus based flame retardants |
| CN114728520B (zh) * | 2019-11-11 | 2024-03-08 | 富士胶片株式会社 | 活性能量射线固化型油墨及图像记录方法 |
| JP7570714B2 (ja) | 2020-05-29 | 2024-10-22 | オドネ エージー | 化学的に安定したポリマーゲルのための架橋性プレポリマー |
| CN112547122A (zh) * | 2020-12-18 | 2021-03-26 | 商河知济新材料技术中心 | 叔丁醇盐和吡啶盐在制备一种光引发剂中的用途 |
| WO2024056948A1 (fr) | 2022-09-15 | 2024-03-21 | Elkem Silicones France Sas | Méthode de fabrication additive pour produire un article en élastomère silicone |
| CN120365331B (zh) * | 2025-06-26 | 2025-11-04 | 北京大学深圳研究生院 | 一种光引发剂及其制备方法 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2957931A (en) * | 1949-07-28 | 1960-10-25 | Socony Mobil Oil Co Inc | Synthesis of compounds having a carbonphosphorus linkage |
| US2822376A (en) * | 1957-02-27 | 1958-02-04 | American Cyanamid Co | Reaction of phosphine with alpha, beta-unsatu-rated compounds |
| TW303379B (enExample) * | 1994-03-02 | 1997-04-21 | Ciba Sc Holding Ag | |
| RU2141962C1 (ru) * | 1994-07-29 | 1999-11-27 | Пферси Хеми ГмбХ | Способ получения диэфиров производных фосфонкарбоновых кислот |
| SG53043A1 (en) * | 1996-08-28 | 1998-09-28 | Ciba Geigy Ag | Molecular complex compounds as photoinitiators |
| ATE221893T1 (de) | 1998-11-30 | 2002-08-15 | Ciba Sc Holding Ag | Verfahren zur herstellung von acylphosphinen und derivaten |
| JP2001200007A (ja) * | 2000-01-19 | 2001-07-24 | Shin Etsu Chem Co Ltd | 光硬化性樹脂組成物及び光ファイバー用被覆材 |
| GB2360283B (en) * | 2000-02-08 | 2002-08-21 | Ciba Sc Holding Ag | Monoacylarylphosphines and acylphosphine oxides and sulphides |
| AU2002366198A1 (en) | 2001-11-20 | 2003-06-10 | Ciba Specialty Chemicals Holding Inc. | Multimer forms of acylphosphines and their derivatives |
| JP2003228150A (ja) * | 2002-02-04 | 2003-08-15 | Konica Corp | 光熱写真画像形成材料 |
| KR20050009744A (ko) * | 2002-06-11 | 2005-01-25 | 시바 스페셜티 케미칼스 홀딩 인크. | 모노- 및 비스아실포스핀 옥사이드의 다량체 형태 |
| MXPA06000681A (es) | 2003-07-18 | 2006-04-11 | Ciba Sc Holding Ag | Proceso para preparar acilfosfanos y derivados de los mismos. |
| EP1765878B1 (en) | 2004-04-15 | 2010-12-08 | Basf Se | Process for photocuring with light emitting diodes |
| EP1814891B1 (en) | 2004-11-23 | 2011-01-26 | Basf Se | Bisacylphosphanes and their use as photoinitiators; process for preparing acylphosphanes |
| WO2006074983A1 (en) | 2005-01-17 | 2006-07-20 | Ciba Specialty Chemicals Holding Inc. | Process for preparing acylphosphanes and their oxides and sulphides |
| JP2007272106A (ja) * | 2006-03-31 | 2007-10-18 | Fujifilm Corp | ホログラム記録媒体用組成物及びホログラム記録媒体 |
| JP2009541554A (ja) * | 2006-07-04 | 2009-11-26 | チバ ホールディング インコーポレーテッド | 異相重合技術によって作製された光開始剤の水ベースの濃縮されたプロダクト形態 |
| JP5832430B2 (ja) * | 2009-07-06 | 2015-12-16 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | ポリマーに固定されたビスアシルホスフィンオキシド |
| US8633258B2 (en) | 2010-06-30 | 2014-01-21 | Dsm Ip Assets B.V. | D1492 liquid BAPO photoinitiator and its use in radiation curable compositions |
-
2013
- 2013-09-30 EP EP13771462.2A patent/EP2903995B1/en active Active
- 2013-09-30 JP JP2015533630A patent/JP6445438B2/ja active Active
- 2013-09-30 CN CN201810249476.7A patent/CN108383874B/zh active Active
- 2013-09-30 US US14/432,212 patent/US9701700B2/en active Active
- 2013-09-30 EP EP19151535.2A patent/EP3508489B1/en active Active
- 2013-09-30 ES ES19151535T patent/ES2881686T3/es active Active
- 2013-09-30 BR BR112015007295-0A patent/BR112015007295B1/pt active IP Right Grant
- 2013-09-30 KR KR1020157011628A patent/KR102135300B1/ko active Active
- 2013-09-30 WO PCT/EP2013/070378 patent/WO2014053455A1/en not_active Ceased
- 2013-09-30 CN CN201380051352.3A patent/CN104703995B/zh active Active
- 2013-09-30 RU RU2015116292A patent/RU2719592C2/ru active
- 2013-09-30 ES ES13771462T patent/ES2720760T3/es active Active
-
2017
- 2017-05-24 US US15/603,467 patent/US10273258B2/en active Active
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