KR102135300B1 - 아실포스판의 제조 방법 - Google Patents

아실포스판의 제조 방법 Download PDF

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KR102135300B1
KR102135300B1 KR1020157011628A KR20157011628A KR102135300B1 KR 102135300 B1 KR102135300 B1 KR 102135300B1 KR 1020157011628 A KR1020157011628 A KR 1020157011628A KR 20157011628 A KR20157011628 A KR 20157011628A KR 102135300 B1 KR102135300 B1 KR 102135300B1
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KR20150064747A (ko
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한스욕 거츠마허
조지나 뮐러
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에테하 취리히
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/53Organo-phosphine oxides; Organo-phosphine thioxides
    • C07F9/5337Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/5036Phosphines containing the structure -C(=X)-P or NC-P
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/505Preparation; Separation; Purification; Stabilisation
    • C07F9/5063Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds
    • C07F9/5072Preparation; Separation; Purification; Stabilisation from compounds having the structure P-H or P-Heteroatom, in which one or more of such bonds are converted into P-C bonds from starting materials having the structure P-H
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/28Phosphorus compounds with one or more P—C bonds
    • C07F9/50Organo-phosphines
    • C07F9/53Organo-phosphine oxides; Organo-phosphine thioxides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/572Five-membered rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/553Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
    • C07F9/576Six-membered rings
    • C07F9/58Pyridine rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/655Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
    • C07F9/65515Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a five-membered ring
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/46Polymerisation initiated by wave energy or particle radiation
    • C08F2/48Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C08F2/50Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light with sensitising agents
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F218/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid or of a haloformic acid
    • C08F218/02Esters of monocarboxylic acids
    • C08F218/04Vinyl esters
    • C08F218/08Vinyl acetate

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Polymerisation Methods In General (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
KR1020157011628A 2012-10-01 2013-09-30 아실포스판의 제조 방법 Active KR102135300B1 (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
EP12006822.6 2012-10-01
EP12006822 2012-10-01
EP13003616.3 2013-07-18
EP13003616 2013-07-18
PCT/EP2013/070378 WO2014053455A1 (en) 2012-10-01 2013-09-30 A process for the preparation of acylphosphanes

Publications (2)

Publication Number Publication Date
KR20150064747A KR20150064747A (ko) 2015-06-11
KR102135300B1 true KR102135300B1 (ko) 2020-08-27

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KR1020157011628A Active KR102135300B1 (ko) 2012-10-01 2013-09-30 아실포스판의 제조 방법

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US (2) US9701700B2 (enExample)
EP (2) EP2903995B1 (enExample)
JP (1) JP6445438B2 (enExample)
KR (1) KR102135300B1 (enExample)
CN (2) CN104703995B (enExample)
BR (1) BR112015007295B1 (enExample)
ES (2) ES2720760T3 (enExample)
RU (1) RU2719592C2 (enExample)
WO (1) WO2014053455A1 (enExample)

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EP3031798B1 (en) 2014-12-10 2017-09-27 Belenos Clean Power Holding AG A novel cross-linker for the preparation of a new family of single ion conduction polymers for electrochemical devices and such polymers
EP3296301A1 (en) 2016-09-19 2018-03-21 ETH Zürich A versatile process for the preparation of acylphosphines
CA3043849A1 (en) 2016-11-16 2018-05-24 Ecole Polytechnique Federale De Lausanne (Epfl) Photopolymerizable bone filler material
EP3409680B1 (en) * 2017-05-30 2021-01-06 IGM Group B.V. Synthesis of bis(acyl)phosphines by activation of unreactive metal phosphides
CN107400144B (zh) * 2017-08-03 2020-04-14 深圳有为技术控股集团有限公司 酰基膦(氧)化合物及其制备方法和应用
EP3539924A1 (en) 2018-03-14 2019-09-18 ETH Zurich Novel vinyl phosphines and photo-initiators obtainable therefrom
EP3539969A1 (en) 2018-03-14 2019-09-18 ETH Zurich Novel photo-initiators and their application
CN112673012B (zh) * 2018-09-07 2024-05-24 意大利艾坚蒙树脂有限公司 多官能双酰基氧化膦光引发剂
EP3747942A1 (en) 2019-06-05 2020-12-09 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Bridged phosphorus based flame retardants
EP4059719A4 (en) * 2019-11-11 2022-12-14 FUJIFILM Corporation ACTIVE ENERGY RAYS CURING INK AND IMAGE RECORDING METHOD
JP7570714B2 (ja) 2020-05-29 2024-10-22 オドネ エージー 化学的に安定したポリマーゲルのための架橋性プレポリマー
CN112547122A (zh) * 2020-12-18 2021-03-26 商河知济新材料技术中心 叔丁醇盐和吡啶盐在制备一种光引发剂中的用途
WO2024056948A1 (fr) 2022-09-15 2024-03-21 Elkem Silicones France Sas Méthode de fabrication additive pour produire un article en élastomère silicone
CN120365331B (zh) * 2025-06-26 2025-11-04 北京大学深圳研究生院 一种光引发剂及其制备方法

Citations (1)

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KR100769838B1 (ko) * 2000-02-08 2007-10-24 시바 스페셜티 케미칼스 홀딩 인크. 유기 금속 모노아실아릴포스핀

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US2957931A (en) * 1949-07-28 1960-10-25 Socony Mobil Oil Co Inc Synthesis of compounds having a carbonphosphorus linkage
US2822376A (en) * 1957-02-27 1958-02-04 American Cyanamid Co Reaction of phosphine with alpha, beta-unsatu-rated compounds
TW303379B (enExample) * 1994-03-02 1997-04-21 Ciba Sc Holding Ag
DK0694556T3 (da) * 1994-07-29 1999-11-15 Ciba Spezialitotenchemie Pfers Fremgangsmåde til fremstilling af diestere af phosphonocarbocylsyrederivater
SG53043A1 (en) 1996-08-28 1998-09-28 Ciba Geigy Ag Molecular complex compounds as photoinitiators
SK286152B6 (sk) 1998-11-30 2008-04-07 Ciba Specialty Chemicals Holding Inc. Spôsob prípravy acylfosfínov, acylfosfínoxidov a acylfosfínsulfidov
JP2001200007A (ja) * 2000-01-19 2001-07-24 Shin Etsu Chem Co Ltd 光硬化性樹脂組成物及び光ファイバー用被覆材
BR0214324A (pt) * 2001-11-20 2004-11-03 Ciba Sc Holding Ag Formas diméricas e multiméricas de acilfosfinas, óxidos de acilfosfina e sulfetos de acilfosfina
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Publication number Publication date
EP3508489A1 (en) 2019-07-10
EP3508489B1 (en) 2021-04-14
US10273258B2 (en) 2019-04-30
BR112015007295B1 (pt) 2021-12-14
KR20150064747A (ko) 2015-06-11
BR112015007295A2 (pt) 2017-07-04
EP2903995B1 (en) 2019-01-16
RU2719592C2 (ru) 2020-04-21
US20180002357A1 (en) 2018-01-04
WO2014053455A1 (en) 2014-04-10
US9701700B2 (en) 2017-07-11
CN104703995A (zh) 2015-06-10
CN108383874B (zh) 2021-10-08
CN108383874A (zh) 2018-08-10
US20150299231A1 (en) 2015-10-22
RU2015116292A (ru) 2016-11-27
ES2720760T3 (es) 2019-07-24
ES2881686T3 (es) 2021-11-30
EP2903995A1 (en) 2015-08-12
CN104703995B (zh) 2018-04-20
JP6445438B2 (ja) 2018-12-26
JP2015532275A (ja) 2015-11-09

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