JP6102044B2 - 消色プライマー組成物、ならびに消色プライマー組成物を用いたシーリング材の施工方法、防水材の施工方法および上塗り塗料の施工方法 - Google Patents
消色プライマー組成物、ならびに消色プライマー組成物を用いたシーリング材の施工方法、防水材の施工方法および上塗り塗料の施工方法 Download PDFInfo
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- JP6102044B2 JP6102044B2 JP2012244538A JP2012244538A JP6102044B2 JP 6102044 B2 JP6102044 B2 JP 6102044B2 JP 2012244538 A JP2012244538 A JP 2012244538A JP 2012244538 A JP2012244538 A JP 2012244538A JP 6102044 B2 JP6102044 B2 JP 6102044B2
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- UUIQMZJEGPQKFD-UHFFFAOYSA-N n-butyric acid methyl ester Natural products CCCC(=O)OC UUIQMZJEGPQKFD-UHFFFAOYSA-N 0.000 description 1
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- KYTZHLUVELPASH-UHFFFAOYSA-N naphthalene-1,2-dicarboxylic acid Chemical compound C1=CC=CC2=C(C(O)=O)C(C(=O)O)=CC=C21 KYTZHLUVELPASH-UHFFFAOYSA-N 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- FLESAADTDNKLFJ-UHFFFAOYSA-N nickel;pentane-2,4-dione Chemical compound [Ni].CC(=O)CC(C)=O FLESAADTDNKLFJ-UHFFFAOYSA-N 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- SSDSCDGVMJFTEQ-UHFFFAOYSA-N octadecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 SSDSCDGVMJFTEQ-UHFFFAOYSA-N 0.000 description 1
- IOQPZZOEVPZRBK-UHFFFAOYSA-N octan-1-amine Chemical compound CCCCCCCCN IOQPZZOEVPZRBK-UHFFFAOYSA-N 0.000 description 1
- OEIJHBUUFURJLI-UHFFFAOYSA-N octane-1,8-diol Chemical compound OCCCCCCCCO OEIJHBUUFURJLI-UHFFFAOYSA-N 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 150000002902 organometallic compounds Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
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- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- WATYAKBWIQTPDE-UHFFFAOYSA-N pentane-2,4-dione;zinc Chemical compound [Zn].CC(=O)CC(C)=O WATYAKBWIQTPDE-UHFFFAOYSA-N 0.000 description 1
- 125000005010 perfluoroalkyl group Chemical group 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002530 phenolic antioxidant Substances 0.000 description 1
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 150000003014 phosphoric acid esters Chemical class 0.000 description 1
- 238000001782 photodegradation Methods 0.000 description 1
- 125000005498 phthalate group Chemical class 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 1
- 239000011120 plywood Substances 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 229920006149 polyester-amide block copolymer Polymers 0.000 description 1
- 229920000921 polyethylene adipate Polymers 0.000 description 1
- 229920006389 polyphenyl polymer Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- 229920005749 polyurethane resin Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- HKJYVRJHDIPMQB-UHFFFAOYSA-N propan-1-olate;titanium(4+) Chemical compound CCCO[Ti](OCCC)(OCCC)OCCC HKJYVRJHDIPMQB-UHFFFAOYSA-N 0.000 description 1
- KCXFHTAICRTXLI-UHFFFAOYSA-N propane-1-sulfonic acid Chemical compound CCCS(O)(=O)=O KCXFHTAICRTXLI-UHFFFAOYSA-N 0.000 description 1
- 229940090181 propyl acetate Drugs 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 description 1
- 150000003856 quaternary ammonium compounds Chemical class 0.000 description 1
- 239000007870 radical polymerization initiator Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- IYMSIPPWHNIMGE-UHFFFAOYSA-N silylurea Chemical compound NC(=O)N[SiH3] IYMSIPPWHNIMGE-UHFFFAOYSA-N 0.000 description 1
- 239000010454 slate Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 125000003396 thiol group Chemical group [H]S* 0.000 description 1
- RUELTTOHQODFPA-UHFFFAOYSA-N toluene 2,6-diisocyanate Chemical compound CC1=C(N=C=O)C=CC=C1N=C=O RUELTTOHQODFPA-UHFFFAOYSA-N 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- FRGPKMWIYVTFIQ-UHFFFAOYSA-N triethoxy(3-isocyanatopropyl)silane Chemical compound CCO[Si](OCC)(OCC)CCCN=C=O FRGPKMWIYVTFIQ-UHFFFAOYSA-N 0.000 description 1
- UDUKMRHNZZLJRB-UHFFFAOYSA-N triethoxy-[2-(7-oxabicyclo[4.1.0]heptan-4-yl)ethyl]silane Chemical compound C1C(CC[Si](OCC)(OCC)OCC)CCC2OC21 UDUKMRHNZZLJRB-UHFFFAOYSA-N 0.000 description 1
- JXUKBNICSRJFAP-UHFFFAOYSA-N triethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CCO[Si](OCC)(OCC)CCCOCC1CO1 JXUKBNICSRJFAP-UHFFFAOYSA-N 0.000 description 1
- ROWWCTUMLAVVQB-UHFFFAOYSA-N triethoxysilylmethanamine Chemical compound CCO[Si](CN)(OCC)OCC ROWWCTUMLAVVQB-UHFFFAOYSA-N 0.000 description 1
- HUZZQXYTKNNCOU-UHFFFAOYSA-N triethyl(methoxy)silane Chemical compound CC[Si](CC)(CC)OC HUZZQXYTKNNCOU-UHFFFAOYSA-N 0.000 description 1
- 239000013638 trimer Substances 0.000 description 1
- NMEPHPOFYLLFTK-UHFFFAOYSA-N trimethoxy(octyl)silane Chemical compound CCCCCCCC[Si](OC)(OC)OC NMEPHPOFYLLFTK-UHFFFAOYSA-N 0.000 description 1
- ZNOCGWVLWPVKAO-UHFFFAOYSA-N trimethoxy(phenyl)silane Chemical compound CO[Si](OC)(OC)C1=CC=CC=C1 ZNOCGWVLWPVKAO-UHFFFAOYSA-N 0.000 description 1
- DQZNLOXENNXVAD-UHFFFAOYSA-N trimethoxy-[2-(7-oxabicyclo[4.1.0]heptan-4-yl)ethyl]silane Chemical compound C1C(CC[Si](OC)(OC)OC)CCC2OC21 DQZNLOXENNXVAD-UHFFFAOYSA-N 0.000 description 1
- BPSIOYPQMFLKFR-UHFFFAOYSA-N trimethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CO[Si](OC)(OC)CCCOCC1CO1 BPSIOYPQMFLKFR-UHFFFAOYSA-N 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- 229920006305 unsaturated polyester Chemical class 0.000 description 1
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Building Environments (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
Description
着色剤を配合したプライマーが塗布時のはみ出し等で下地材の被着面以外の所に付着し、無色化するまでに多くの日数を要すると着色した所が目立つため意匠上の不具合要因となる。このため、太陽光が当たらない所でも早期に無色化する消色性(退色性)の高いプライマーが求められる。
そこで本発明は、プライマーの塗布状態を容易に視認し、プライマー塗布部が太陽光の当たらない所でも早期に無色化する消色プライマー組成物の提供、ならびに消色プライマー組成物を用いたシーリング材の施工方法、防水材の施工方法および上塗り塗料の施工方法の提供を課題とする。
(1)バインダー樹脂(A)と、湿気により消色性を示す金属錯体化合物(B)と、を含有する、シーリング材若しくは防水材の下地処理用または上塗り塗料の施工時のバリア用の消色プライマー組成物。
(2)前記バインダー樹脂(A)が、イソシアネート基含有化合物(A−1)、ならびに/または、イソシアネート基および加水分解性シリル基含有化合物、および/もしくは、加水分解性シリル基含有化合物(A−2)である、(1)に記載の消色プライマー組成物。
(3)前記湿気により消色性を示す金属錯体化合物(B)が、チオシアン酸の金属錯イオンおよび/またはその塩である、(1)に記載の消色プライマー組成物。
(4)前記湿気により消色性を示す金属錯体化合物(B)が、チオシアン酸鉄(III)の錯イオンおよび/またはその塩である、(1)または(3)に記載の消色プライマー組成物。
(5)(1)〜(4)のいずれか一項に記載の消色プライマー組成物によるプライマー層を下地材に直接または他の層を介して形成した後、シーリング材を打設することを特徴とする、シーリング材の施工方法。
(6)(1)〜(4)のいずれか一項に記載の消色プライマー組成物によるプライマー層を下地材に直接または他の層を介して形成した後、防水材を塗布することを特徴とする、防水材の施工方法。
(7)(1)〜(4)のいずれか一項に記載の消色プライマー組成物によるプライマー層をシーリング材の表面または防水材の表面に形成した後、上塗り塗料を塗布することを特徴とする、上塗り塗料の施工方法。
本発明の消色プライマー組成物は、バインダー樹脂(A)と、水により消色性を示す金属錯体化合物(B)と、を含有することを特徴とする。以下、各成分について、詳細に説明する。
本発明におけるバインダー樹脂(A)は、プライマー層を形成することが可能なものであれば特に制限されないが、溶媒の揮散および/または硬化反応によりプライマー層を形成する(塗膜を形成する)化合物が好ましい。なお、本発明においてプライマー層とは、シーリング材、防水材の施工前に予め下地材表面または他の層表面に形成されるプライマー層や、シーリング材の表面または防水材の表面に設けられる上塗り塗料との間に形成されるプライマー層(バリアプライマー)である。
イソシアネート基含有化合物と加水分解性シリル基含有化合物とを反応して得られる化合物としては、具体的には、前述したイソシアネート基含有化合物(A−1)と同様のイソシアネート基含有化合物と、分子内にイソシアネート基との反応性を有する有機官能基および加水分解性(架橋性)シリル基を有する化合物とを反応して得られる化合物である。前記有機官能基はイソシアネート基含有化合物との反応のし易さから活性水素を有する有機官能基が好ましい。
本発明における水により消色性を示す金属錯体化合物(B)は、その金属錯体化合物が有色であり、水の作用によって消色性を示す(無色となる)金属錯体化合物であれば、特に制限することなく使用することができる。
水により消色性を示す金属錯体化合物(B)としては、特に制限はないが、具体的には、チオシアン酸の金属錯体化合物(錯イオンを含む)を挙げることができる。金属錯体化合物に含まれる金属としては、特に制限はないが、銅、鉄、チタン、ニッケル、クロム、コバルト、銀等種々の金属が挙げられる。この中でも、入手のしやすさおよび経済性を考慮すると、銅および鉄が好ましい。特に、チオシアン酸鉄(III)の錯イオンおよび/またはその塩は、プライマー組成物に少量添加した場合でも着色性が良くプライマー塗布部の視認性が良好で、また、水による消色性も高いため早期に無色となるから好適に使用することができる。
2Fe3+ + 6KSCN → 6K++ Fe[Fe(SCN)6] (II)
Fe3+ + nKSCN + mH2O →
nK+ + [Fe(SCN)n(H2O)m]3−n (III)
(式中、nは1〜6の整数、mは1〜5の整数を示す)
なお、本発明においては、バインダー樹脂(A)が水との反応性を有しており、バインダー樹脂(A)を有機溶媒との混合物として調製する方法が好ましい。
チオシアン酸鉄(III)の錯イオンおよび/またはその塩を着色剤として用いたプライマー組成物は、プライマー組成物の塗布部が良好な視認性を示すとともに、主に空気中の水分(湿分)によって消色(無色化)する。このため、プライマー組成物を被着面以外の所に塗布した場合でも塗布部が経時的に消色し、意匠上の問題を生じることはない。
本発明の消色プライマー組成物は本発明の目的を損なわない範囲で上記成分の他に、必要に応じて有機溶剤や添加剤を使用することができる。
本発明の消色プライマー組成物を用いたシーリング材の施工方法、防水材の施工方法および上塗り塗料の施工方法について説明する。
シーリング材の施工方法および防水材の施工方法の手順としては、最初に被着面となる下地材の表面に水、切りくずや埃等が付着していないことを目視や指触により確認する。下地材の表面に水、切りくずや埃等が付着している場合は、刷毛やウエス等を用いてそれらを取り除く。次いで消色プライマー組成物が下地材の被着面以外の箇所に付着することを防止するため、必要に応じてマスキングテープや養生シート等を下地材に貼付し、消色プライマー組成物を後述する下地材の表面または他の層の表面に刷毛、ローラー、スプレー等で所定量塗布する。消色プライマー組成物を塗布後、所定の時間(オープンタイム:通常は5℃〜35℃で30分〜60分程度)放置乾燥し、消色プライマー組成物を硬化させプライマー層(塗膜)を形成させる。
上塗り塗料の施工方法の手順としては、最初に被着面となるシーリング材または防水材の硬化状態を指触等により確認する。それらの表面が硬化していれば上塗り塗料の施工は可能であるが、消色プライマー組成物の塗布のし易さから、それらの内部も完全に硬化していることが望ましい。
攪拌機、温度計、冷却管及び乾燥窒素導入管付きの反応容器に、窒素気流下で、酢酸エチルを572.8g、数平均分子量300のポリオキシプロピレントリオールを122.1g仕込み、攪拌しながらイソホロンジイソシアネートを257.4g仕込んだ。次いで、ジブチル錫ジラウレートを0.4g仕込み、発熱に注意しながら70℃まで徐々に加熱し、イソシアネート基含有量が4.6質量%になるまでウレタン化反応を行ない、理論不揮発分40質量%のイソシアネート基含有ウレタンプレポリマー(P−1)を得た。
攪拌機、温度計、冷却管及び乾燥窒素導入管付きの反応容器に、窒素気流下で、酢酸エチルを550g、HDIとTDIとの混合イソシアヌレート三量体であるデスモジュールHL(住化バイエルウレタン社製、イソシアネート基濃度10.5%、固形分60質量%、酢酸ブチル溶液)を350g、N−フェニル−γ−アミノプロピルトリメトキシシラン(信越化学工業社製、KBM−573)を31.2g仕込み、70℃で1時間混合・攪拌し、イソシアネート基含有量が3.9質量%、理論不揮発分26質量%のイソシアネート基含有ウレタンプレポリマー(P−2)を得た。
攪拌機、乾燥窒素導入管付きの混合容器に、窒素気流下で、メチルエチルケトンを99.8g、無水塩化鉄(III)(和光純薬工業社製)を0.2g仕込み、攪拌・混合し、0.2%塩化鉄(III)溶液を得た。
また、攪拌機、乾燥窒素導入管付きの混合容器に、窒素気流下で、メチルエチルケトンを99.8g、チオシアン酸カリウム(和光純薬工業社製)を0.2g仕込み、攪拌・混合し、0.2%チオシアン酸カリウム溶液を得た。
次いで、攪拌機、乾燥窒素導入管付きの混合容器に、窒素気流下で、0.2%塩化鉄(III)溶液を100g、0.2%チオシアン酸カリウム溶液を300g仕込み、攪拌・混合し、赤色のチオシアン酸鉄(III)の錯イオン溶液を得た。
攪拌機、乾燥窒素導入管付きの混合容器に、窒素気流下で、調製例1で得たイソシアネート基含有ウレタンプレポリマー(P−1)を100g、調製例3で得た赤色のチオシアン酸鉄(III)の錯イオン溶液を75.1g仕込み、攪拌・混合し、消色プライマー組成物を得た。
攪拌機、乾燥窒素導入管付きの混合容器に、窒素気流下で、調製例2で得たイソシアネート基含有ウレタンプレポリマー(P−2)を100g、調製例3で得た赤色のチオシアン酸鉄(III)の錯イオン溶液を75.1g仕込み、攪拌・混合し、消色プライマー組成物を得た。
調製例1で得たイソシアネート基含有ウレタンプレポリマー(P−1)を使用した。
調製例2で得たイソシアネート基含有ウレタンプレポリマー(P−2)を使用した。
攪拌機、乾燥窒素導入管付きの混合容器に、窒素気流下で、調製例1で得たイソシアネート基含有ウレタンプレポリマー(P−1)を100g、リボフラビン酪酸エステル(三菱化学フーズ社製)を0.03gそれぞれ仕込み、攪拌・混合し、プライマー組成物を得た。
攪拌機、乾燥窒素導入管付きの混合容器に、窒素気流下で、調製例2で得たイソシアネート基含有ウレタンプレポリマー(P−2)を100g、リボフラビン酪酸エステル(三菱化学フーズ社製)を0.03gそれぞれ仕込み、攪拌・混合し、プライマー組成物を得た。
実施例1〜2および比較例1〜4で得たプライマー組成物を用いて、下記に示す評価を行った。
50mm×50mm×15mmのサイディング(ケイミュー社製、塗装面:ホワイト色)の小口面(切出し面)に実施例1〜2および比較例1〜4のプライマー組成物をそれぞれ140g/m2の塗布量で刷毛塗りし、プライマー組成物の塗布面の着色状態を目視で評価した。
[太陽光の当たる所]
50mm×50mm×15mmのサイディング(ケイミュー社製、塗装面:ホワイト色)の塗装面に実施例1〜2および比較例1〜4のプライマー組成物をそれぞれ140g/m2の塗布量で刷毛塗りした。次いで、プライマー組成物の塗布面が鉛直方向(水平面から90°)となるように、サイディングを屋外の太陽光が当たる所(日向)に静置し、合計3日間暴露した。
[太陽光の当たらない所]
50mm×50mm×15mmのサイディング(ケイミュー社製、塗装面:ホワイト色)の塗装面に実施例1〜2および比較例1〜4のプライマー組成物をそれぞれ140g/m2の塗布量で刷毛塗りした。次いで、プライマー組成物の塗布面が鉛直方向(水平面から90°)となるように、サイディングを屋外の太陽光が当たらない所(日陰)に静置し、合計16週間暴露した。
屋外への暴露後、プライマー組成物の塗布面の状態をそれぞれ目視で評価した。
Claims (7)
- バインダー樹脂(A)と、湿気により消色性を示す金属錯体化合物(B)と、を含有する、シーリング材若しくは防水材の下地処理用または上塗り塗料の施工時のバリア用の消色プライマー組成物。
- 前記バインダー樹脂(A)が、イソシアネート基含有化合物(A−1)、ならびに/または、イソシアネート基および加水分解性シリル基含有化合物、および/もしくは、加水分解性シリル基含有化合物(A−2)である、請求項1に記載の消色プライマー組成物。
- 前記湿気により消色性を示す金属錯体化合物(B)が、チオシアン酸の金属錯イオンおよび/またはその塩である、請求項1に記載の消色プライマー組成物。
- 前記湿気により消色性を示す金属錯体化合物(B)が、チオシアン酸鉄(III)の錯イオンおよび/またはその塩である、請求項1または請求項3に記載の消色プライマー組成物。
- 請求項1〜4のいずれか一項に記載の消色プライマー組成物によるプライマー層を下地材に直接または他の層を介して形成した後、シーリング材を打設することを特徴とする、シーリング材の施工方法。
- 請求項1〜4のいずれか一項に記載の消色プライマー組成物によるプライマー層を下地材に直接または他の層を介して形成した後、防水材を塗布することを特徴とする、防水材の施工方法。
- 請求項1〜4のいずれか一項に記載の消色プライマー組成物によるプライマー層をシーリング材の表面または防水材の表面に形成した後、上塗り塗料を塗布することを特徴とする、上塗り塗料の施工方法。
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