JP6050372B2 - クロロアルカンの製造方法 - Google Patents
クロロアルカンの製造方法 Download PDFInfo
- Publication number
- JP6050372B2 JP6050372B2 JP2014542375A JP2014542375A JP6050372B2 JP 6050372 B2 JP6050372 B2 JP 6050372B2 JP 2014542375 A JP2014542375 A JP 2014542375A JP 2014542375 A JP2014542375 A JP 2014542375A JP 6050372 B2 JP6050372 B2 JP 6050372B2
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- JP
- Japan
- Prior art keywords
- catalyst
- tetra
- tri
- trichloropropane
- mono
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Description
〈1〉1つ以上のモノ及び/又はジクロロアルカンから、トリ―、テトラ―、及び/又はペンタクロロアルカンを製造する方法であって、1つのイオン性塩素化触媒の存在下、上記モノ及び/又はジクロロアルカンを塩素化することを含んでおり、塩素化剤が塩化スルフリルを含む、方法。
〈2〉上記1つ以上のモノ―及び/又はジクロロアルカンの少なくとも1つが、ビシナルジクロロアルカンを含む、項目1に記載の方法。
〈3〉上記ジクロロアルカンが、1,2―ジクロロプロパンを含む、項目1又は2に記載の方法。
〈4〉上記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,1,2―トリクロロアルカンを含む、項目3に記載の方法。
〈5〉上記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,1,2―トリクロロプロパンを含む、項目4に記載の方法。
〈6〉1,1,2―トリクロロプロパンに対する方法の選択性が、少なくとも20:1である、項目5に記載の方法。
〈7〉1,1,2―トリクロロプロパンに対する方法の選択性が、少なくとも40:1である、項目6に記載の方法。
〈8〉上記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,2,2,3―テトラクロロアルカンを含む、項目3に記載の方法。
〈9〉上記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,2,2,3―テトラクロロプロパンを含む、項目8に記載の方法。
〈10〉上記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,1,2,2,3―ペンタクロロアルカンを含む、項目3に記載の方法。
〈11〉上記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,1,2,2,3―ペンタクロロプロパンを含む、項目10に記載の方法。
〈12〉イオン性塩素化触媒がAlCl 3 を含む、項目1に記載の方法。
〈13〉方法を40℃〜70℃の温度で行う、項目1に記載の方法。
〈14〉方法を周囲圧力で行う、項目1に記載の方法。
〈15〉方法を液相反応器で行い、反応器滞留時間が1時間未満である、項目1に記載の方法。
Claims (2)
- 1つ以上のジクロロアルカンから、トリ―、テトラ―、及び/又はペンタクロロアルカンを製造する方法であって、塩化アルミニウムの存在下、1,2―ジクロロプロパンを含むジクロロアルカンを塩素化することを含んでおり、塩素化剤が塩化スルフリルを含み、前記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,1,2―トリクロロプロパンを含み、1,1,2―トリクロロプロパンに対する方法の選択性が、モル比で少なくとも20:1である、方法。
- 前記トリ―、テトラ―、及び/又はペンタクロロアルカンが、1,1,2,2,3―ペンタクロロプロパンを含む、請求項1に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161562025P | 2011-11-21 | 2011-11-21 | |
US61/562,025 | 2011-11-21 | ||
PCT/US2012/064792 WO2013078035A1 (en) | 2011-11-21 | 2012-11-13 | Process for the production of chlorinated alkanes |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2015501801A JP2015501801A (ja) | 2015-01-19 |
JP6050372B2 true JP6050372B2 (ja) | 2016-12-21 |
Family
ID=47226472
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2014542375A Expired - Fee Related JP6050372B2 (ja) | 2011-11-21 | 2012-11-13 | クロロアルカンの製造方法 |
Country Status (7)
Country | Link |
---|---|
US (1) | US9067855B2 (ja) |
EP (1) | EP2782889B1 (ja) |
JP (1) | JP6050372B2 (ja) |
CN (1) | CN104039744B (ja) |
CA (1) | CA2856271A1 (ja) |
IN (1) | IN2014CN03748A (ja) |
WO (1) | WO2013078035A1 (ja) |
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WO2014100066A1 (en) | 2012-12-18 | 2014-06-26 | Dow Global Technologies, Llc | Process for the production of chlorinated propenes |
WO2014100039A1 (en) | 2012-12-19 | 2014-06-26 | Dow Global Technologies, Llc | Process for the production of chlorinated propenes |
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CN104981449B (zh) | 2013-02-27 | 2016-12-28 | 蓝立方知识产权有限责任公司 | 用于生产氯化丙烯的方法 |
US9403741B2 (en) | 2013-03-09 | 2016-08-02 | Blue Cube Ip Llc | Process for the production of chlorinated alkanes |
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US20150045592A1 (en) | 2015-02-12 |
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EP2782889B1 (en) | 2016-12-21 |
EP2782889A1 (en) | 2014-10-01 |
CA2856271A1 (en) | 2013-05-30 |
CN104039744B (zh) | 2016-04-20 |
US9067855B2 (en) | 2015-06-30 |
JP2015501801A (ja) | 2015-01-19 |
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