JP5850372B2 - 鋳造用結晶粒微細化剤およびその製造方法 - Google Patents
鋳造用結晶粒微細化剤およびその製造方法 Download PDFInfo
- Publication number
- JP5850372B2 JP5850372B2 JP2012554746A JP2012554746A JP5850372B2 JP 5850372 B2 JP5850372 B2 JP 5850372B2 JP 2012554746 A JP2012554746 A JP 2012554746A JP 2012554746 A JP2012554746 A JP 2012554746A JP 5850372 B2 JP5850372 B2 JP 5850372B2
- Authority
- JP
- Japan
- Prior art keywords
- crystal grain
- casting
- intermetallic compound
- grain refiner
- refining agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000005266 casting Methods 0.000 title claims description 29
- 238000004519 manufacturing process Methods 0.000 title claims description 14
- 239000013078 crystal Substances 0.000 claims description 73
- 229910000765 intermetallic Inorganic materials 0.000 claims description 38
- 239000003795 chemical substances by application Substances 0.000 claims description 36
- 239000000463 material Substances 0.000 claims description 34
- 238000007670 refining Methods 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 21
- 239000002245 particle Substances 0.000 claims description 18
- 229910052782 aluminium Inorganic materials 0.000 claims description 17
- 229910000838 Al alloy Inorganic materials 0.000 claims description 12
- 229910052751 metal Inorganic materials 0.000 claims description 11
- 239000002184 metal Substances 0.000 claims description 11
- 239000000843 powder Substances 0.000 claims description 11
- 238000005245 sintering Methods 0.000 claims description 10
- 229910052719 titanium Inorganic materials 0.000 claims description 7
- 229910052727 yttrium Inorganic materials 0.000 claims description 7
- 239000011159 matrix material Substances 0.000 claims description 6
- 229910052725 zinc Inorganic materials 0.000 claims description 4
- 229910052737 gold Inorganic materials 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 229910052804 chromium Inorganic materials 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 229910052735 hafnium Inorganic materials 0.000 claims description 2
- 229910052748 manganese Inorganic materials 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 229910052763 palladium Inorganic materials 0.000 claims description 2
- 229910052697 platinum Inorganic materials 0.000 claims description 2
- 229910052726 zirconium Inorganic materials 0.000 claims description 2
- 239000010936 titanium Substances 0.000 description 43
- 238000010586 diagram Methods 0.000 description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 10
- 229910045601 alloy Inorganic materials 0.000 description 8
- 239000011824 nuclear material Substances 0.000 description 7
- 239000000956 alloy Substances 0.000 description 6
- 238000002474 experimental method Methods 0.000 description 6
- 239000000155 melt Substances 0.000 description 6
- 238000002490 spark plasma sintering Methods 0.000 description 6
- 238000002441 X-ray diffraction Methods 0.000 description 5
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 4
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 238000000265 homogenisation Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 238000001878 scanning electron micrograph Methods 0.000 description 4
- 238000007711 solidification Methods 0.000 description 4
- 230000008023 solidification Effects 0.000 description 4
- 229910018575 Al—Ti Inorganic materials 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 238000011049 filling Methods 0.000 description 3
- 230000014759 maintenance of location Effects 0.000 description 3
- 238000010128 melt processing Methods 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 229910002056 binary alloy Inorganic materials 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000009694 cold isostatic pressing Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000001513 hot isostatic pressing Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000006911 nucleation Effects 0.000 description 2
- 238000010899 nucleation Methods 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 229910000881 Cu alloy Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 229910001651 emery Inorganic materials 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 238000007731 hot pressing Methods 0.000 description 1
- 230000002706 hydrostatic effect Effects 0.000 description 1
- 238000010191 image analysis Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/10—Sintering only
- B22F3/105—Sintering only by using electric current other than for infrared radiant energy, laser radiation or plasma ; by ultrasonic bonding
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/02—Making non-ferrous alloys by melting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/02—Making non-ferrous alloys by melting
- C22C1/026—Alloys based on aluminium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/0408—Light metal alloys
- C22C1/0416—Aluminium-based alloys
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/047—Making non-ferrous alloys by powder metallurgy comprising intermetallic compounds
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/06—Making non-ferrous alloys with the use of special agents for refining or deoxidising
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C21/00—Alloys based on aluminium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
- B22F2998/10—Processes characterised by the sequence of their steps
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Manufacturing & Machinery (AREA)
- Powder Metallurgy (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Manufacture Of Alloys Or Alloy Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012554746A JP5850372B2 (ja) | 2011-01-25 | 2012-01-19 | 鋳造用結晶粒微細化剤およびその製造方法 |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2011013269 | 2011-01-25 | ||
| JP2011013269 | 2011-01-25 | ||
| JP2012554746A JP5850372B2 (ja) | 2011-01-25 | 2012-01-19 | 鋳造用結晶粒微細化剤およびその製造方法 |
| PCT/JP2012/051050 WO2012102162A1 (fr) | 2011-01-25 | 2012-01-19 | Agent d'affinage de grain cristallin pour coulage et son procédé de production |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPWO2012102162A1 JPWO2012102162A1 (ja) | 2014-06-30 |
| JP5850372B2 true JP5850372B2 (ja) | 2016-02-03 |
Family
ID=46580734
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012554746A Expired - Fee Related JP5850372B2 (ja) | 2011-01-25 | 2012-01-19 | 鋳造用結晶粒微細化剤およびその製造方法 |
Country Status (3)
| Country | Link |
|---|---|
| EP (1) | EP2669028B1 (fr) |
| JP (1) | JP5850372B2 (fr) |
| WO (1) | WO2012102162A1 (fr) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6238403B2 (ja) * | 2013-11-07 | 2017-11-29 | 国立大学法人 名古屋工業大学 | 結晶粒微細化剤およびその製造方法 |
| WO2016013637A1 (fr) * | 2014-07-25 | 2016-01-28 | 国立大学法人名古屋工業大学 | Agent d'affinage de structure de matériau de coulage d'alliage d'aluminium |
| CN104439206B (zh) * | 2014-11-29 | 2017-02-22 | 山东大学 | 一种硅晶粒异质形核强化剂在促进铝硅合金熔体中硅晶粒形核中的应用 |
| CN105648251A (zh) * | 2016-02-01 | 2016-06-08 | 东南大学 | 一种铸造铝合金用铝镧硼晶粒细化剂的制备方法 |
| CN107419135B (zh) * | 2017-07-27 | 2018-09-25 | 济南大学 | 锌-铝-钇中间合金细化剂及其制备方法和应用 |
| JP6955254B2 (ja) * | 2017-08-23 | 2021-10-27 | 国立大学法人 名古屋工業大学 | 高濃度に異質核粒子を含有した鋳造用結晶粒微細化剤およびその製造方法 |
| US20190062871A1 (en) * | 2017-08-25 | 2019-02-28 | The Boeing Company | Tailoring high strength aluminum alloys for additive manufacturing through the use of grain refiners |
| CN109136599B (zh) * | 2018-10-08 | 2021-01-29 | 兰州理工大学 | 高熵合金孕育亚共晶铝硅合金制备工艺 |
| JP7430514B2 (ja) * | 2019-11-05 | 2024-02-13 | 東邦チタニウム株式会社 | 鋳造合金、母合金粉末の製造方法及び、鋳造合金の製造方法 |
| CN110951985B (zh) * | 2019-11-25 | 2021-05-11 | 河南科技大学 | 一种铜或铜合金材料的制备方法及精炼用精炼剂 |
| CN111020248B (zh) * | 2019-12-02 | 2020-12-18 | 上海航天精密机械研究所 | 一种Ag-Zr-Zn中间合金及其制备方法和应用 |
| CN112301245A (zh) * | 2020-10-09 | 2021-02-02 | 济南大学 | 一种锌-铜合金中ε相的变质处理方法 |
| CN112981162A (zh) * | 2021-02-10 | 2021-06-18 | 大连交通大学 | 6xxx系铝合金熔体纯化剂及其使用方法 |
| CN113005311A (zh) * | 2021-02-10 | 2021-06-22 | 大连交通大学 | 5xxx系铝合金熔体净化剂及其制备方法 |
| CN112981161A (zh) * | 2021-02-10 | 2021-06-18 | 大连交通大学 | 铝硅系合金真空熔炼用碘酸铯熔体净化剂及其加工方法 |
| CN113005321A (zh) * | 2021-02-10 | 2021-06-22 | 大连交通大学 | 铝锌系合金真空熔炼纯化剂及其制备和使用方法 |
| TWI801846B (zh) * | 2021-04-21 | 2023-05-11 | 台灣雨虹有限公司 | 單方向晶粒金屬材料及其製造方法 |
| CN115627391B (zh) * | 2022-09-29 | 2024-01-30 | 河北科技大学 | 一种铝及其合金用晶粒细化剂及其制备方法与应用 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10204555A (ja) * | 1997-01-17 | 1998-08-04 | Toyota Motor Corp | アルミニウム鋳造合金の結晶粒微細化剤の製造方法 |
| JP2005329459A (ja) * | 2004-05-20 | 2005-12-02 | Ueda Seni Kagaku Shinkokai | 鋳造用結晶粒微細化剤及びその製造方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4865666A (en) * | 1987-10-14 | 1989-09-12 | Martin Marietta Corporation | Multicomponent, low density cubic L12 aluminides |
| JPH07188701A (ja) * | 1993-12-27 | 1995-07-25 | Suzuki Motor Corp | Ａｌ３ Ｔｉ分散強化アルミニウム合金と、その粉末並びにそれらの製造方法 |
| JPH10317083A (ja) | 1997-05-13 | 1998-12-02 | Kobe Steel Ltd | アルミニウム合金用結晶粒微細化剤 |
| JP2001152263A (ja) * | 1999-11-18 | 2001-06-05 | Ueda Seni Kagaku Shinkokai | ハイブリッド傾斜機能材料及びその製造方法 |
| JP2004346368A (ja) * | 2003-05-21 | 2004-12-09 | Ngk Insulators Ltd | 複合材料の製造方法、及び複合材料 |
| TR200504376A2 (tr) * | 2005-11-02 | 2008-05-21 | T�B�Tak-T�Rk�Ye B�L�Msel Ve Tekn�K Ara�Tirma Kurumu | Tane küçültücü ön alaşım üretmek için bir proses |
-
2012
- 2012-01-19 EP EP12738824.7A patent/EP2669028B1/fr active Active
- 2012-01-19 WO PCT/JP2012/051050 patent/WO2012102162A1/fr active Application Filing
- 2012-01-19 JP JP2012554746A patent/JP5850372B2/ja not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10204555A (ja) * | 1997-01-17 | 1998-08-04 | Toyota Motor Corp | アルミニウム鋳造合金の結晶粒微細化剤の製造方法 |
| JP2005329459A (ja) * | 2004-05-20 | 2005-12-02 | Ueda Seni Kagaku Shinkokai | 鋳造用結晶粒微細化剤及びその製造方法 |
Non-Patent Citations (1)
| Title |
|---|
| JPN6012017421; ＪＯＨＮＳＯＮ，Ｍ．， ＢＡＥＣＫＥＲＵＤ，Ｌ．: 'Ｎｕｃｌｅａｎｔｓ ｉｎ Ｇｒａｉｎ Ｒｅｆｉｎｅｄ Ａｌｕｍｉｎｉｕｍ ａｆｔｅｒ Ａｄｄｉｔｉｏｎ ｏｆ Ｔｉ- ａｎｄ Ｂ-ｃｏｎｔａｉｎｉｎｇ Ｍａｓｔｅｒ Ａｌｌｏｙｓ' Ｚｅｉｔｓｃｈｒｉｆｔ ｆｕｅｒ Ｍｅｔａｌｌｋｕｎｄｅ ｖｏｌ．８３，Ｎｏ．１１, 1992, ｐ７７４-７８０, Ｃａｒｌ Ｈａｎｓｅｒ Ｖｅｒｌａｇ * |
Also Published As
| Publication number | Publication date |
|---|---|
| JPWO2012102162A1 (ja) | 2014-06-30 |
| EP2669028A1 (fr) | 2013-12-04 |
| EP2669028A4 (fr) | 2016-08-24 |
| WO2012102162A1 (fr) | 2012-08-02 |
| EP2669028B1 (fr) | 2019-07-17 |
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