JP5576040B2 - 樹脂物品の剥離方法およびマイクロチップの剥離方法 - Google Patents
樹脂物品の剥離方法およびマイクロチップの剥離方法 Download PDFInfo
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- JP5576040B2 JP5576040B2 JP2008325346A JP2008325346A JP5576040B2 JP 5576040 B2 JP5576040 B2 JP 5576040B2 JP 2008325346 A JP2008325346 A JP 2008325346A JP 2008325346 A JP2008325346 A JP 2008325346A JP 5576040 B2 JP5576040 B2 JP 5576040B2
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- resin
- ultraviolet light
- bonded
- irradiation
- vacuum ultraviolet
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/001—Joining in special atmospheres
- B29C66/0012—Joining in special atmospheres characterised by the type of environment
- B29C66/0014—Gaseous environments
- B29C66/00143—Active gases
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/1403—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation characterised by the type of electromagnetic or particle radiation
- B29C65/1406—Ultraviolet [UV] radiation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/02—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure
- B29C65/14—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation
- B29C65/1429—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation characterised by the way of heating the interface
- B29C65/1432—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor by heating, with or without pressure using wave energy, i.e. electromagnetic radiation, or particle radiation characterised by the way of heating the interface direct heating of the surfaces to be joined
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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- B29C65/00—Joining or sealing of preformed parts, e.g. welding of plastics materials; Apparatus therefor
- B29C65/76—Making non-permanent or releasable joints
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/50—General aspects of joining tubular articles; General aspects of joining long products, i.e. bars or profiled elements; General aspects of joining single elements to tubular articles, hollow articles or bars; General aspects of joining several hollow-preforms to form hollow or tubular articles
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- B29C66/53—Joining single elements to tubular articles, hollow articles or bars
- B29C66/534—Joining single elements to open ends of tubular or hollow articles or to the ends of bars
- B29C66/5346—Joining single elements to open ends of tubular or hollow articles or to the ends of bars said single elements being substantially flat
- B29C66/53461—Joining single elements to open ends of tubular or hollow articles or to the ends of bars said single elements being substantially flat joining substantially flat covers and/or substantially flat bottoms to open ends of container bodies
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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- B29C66/80—General aspects of machine operations or constructions and parts thereof
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- B29C66/826—Pressure application arrangements, e.g. transmission or actuating mechanisms for joining tools or clamps without using a separate pressure application tool, e.g. the own weight of the parts to be joined
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B29C66/90—Measuring or controlling the joining process
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
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- B29C66/91641—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the heat or the thermal flux, i.e. the heat flux the heat or the thermal flux being non-constant over time
- B29C66/91643—Measuring or controlling the joining process by measuring or controlling the temperature, the heat or the thermal flux by controlling or regulating the temperature, the heat or the thermal flux by controlling or regulating the heat or the thermal flux, i.e. the heat flux the heat or the thermal flux being non-constant over time following a heat-time profile
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- C—CHEMISTRY; METALLURGY
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Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
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- Organic Chemistry (AREA)
- Electromagnetism (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Thermal Sciences (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Fluid Mechanics (AREA)
- General Chemical & Material Sciences (AREA)
- Lining Or Joining Of Plastics Or The Like (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
Description
(II)前記照射後の前記表面を互いに接触させた状態で昇温することにより、前記表面を接着面として前記第1の樹脂と前記第2の樹脂とを接着する工程と、を含む。
シクロオレフィンポリマー(日本ゼオン社製ZEONEX(登録商標)330R、ガラス転移点123℃)からなる一対の樹脂基板(70mm×20mm、厚さ2mm)の各々の表面に、Xeエキシマランプ(ウシオ電機製、UER20−172A)により真空紫外光(波長172nm)を照射した。紫外光の照射は大気中で行い、ランプと基板表面との距離を5mmまたは30mmとし、照射強度を10mW/cm2とした。照射距離が5mmの場合については、照射時間を5分または10分とした。照射距離が30mmの場合については、照射時間を10分または40分とした。真空紫外光は、各々の基板の一方の主面全体に照射した。
シクロオレフィンポリマー(日本ゼオン社製ZEONEX(登録商標)330R、ガラス転移点123℃)からなる一対の樹脂基板(70mm×20mm、厚さ2mm)の各々の表面に、Xeエキシマランプ(ウシオ電機製、UER20−172A)により真空紫外光(波長172nm)を照射した。真空紫外光の照射は大気中で行い、ランプと基板表面との距離を5mm、照射強度を10mW/cm2、照射時間を5分または10分とした。真空紫外光の照射面は、各々の基板の一方の主面全体とした。なお、ランプと基板表面との距離を5mmとしたときに、1秒当たりに基板表面に到達する真空紫外光の光量は3mJ/cm2・sであるため、照射時間5分の場合の到達光量は0.9J/cm2であり、照射時間10分の場合の到達光量は1.8J/cm2であった。
シクロオレフィンポリマー(日本ゼオン社製ZEONEX(登録商標)330R、ガラス転移点123℃)からなる一対の樹脂基板(70mm×20mm、厚さ2mm)の各々の表面に、Xeエキシマランプ(ウシオ電機製、UER20−172A)により真空紫外光(波長172nm)を照射した。紫外光の照射は大気中で行い、ランプと基板表面との距離を5mm、照射強度を10mW/cm2、照射時間を5分とした。真空紫外光の照射面は、各々の基板の一方の主面全体とした。
シクロオレフィンポリマー(日本ゼオン社製ZEONEX(登録商標)330R、ガラス転移点123℃)からなる一対の樹脂基板(70mm×26mm、厚さ1mm)の各々の表面に、Xeエキシマランプ(ウシオ電機製、UER20−172A)により真空紫外光(波長172nm)を照射した。紫外光の照射は大気中で行い、ランプと基板表面との距離を5mm、照射強度を10mW/cm2、照射時間を5分とした。真空紫外光の照射面は、各々の基板の一方の主面全体とした。
実施例5では、本発明の樹脂の接着方法において、真空紫外光照射の雰囲気における湿度が樹脂の接着に及ぼす影響について検討した。
比較例1として、酸素分子が存在しない雰囲気で樹脂基板に真空紫外光を照射して、樹脂表面の状態を確認した例を示す。
比較例2として、酸素分子が存在しない雰囲気中で樹脂基板に真空紫外光を照射して、樹脂の接着を試みた例を示す。
2 第2の樹脂
3a、3b 表面
4 真空紫外光
5 力
10 空間
11 第1の樹脂基板
12 第2の樹脂基板
13 流路
14 表面
15 表面
16 マイクロチップ
Claims (4)
- 樹脂部を有する2以上の部品を含み、前記2以上の部品が前記樹脂部において互いに接着されている樹脂物品について、接着されている前記樹脂部同士を互いに剥離する剥離方法であって、
前記樹脂部同士は、一方の樹脂部を第1の樹脂とし、他方の樹脂部を第2の樹脂として、
(I)第1および第2の樹脂の表面に、波長175nm以下の真空紫外光を照射する工程と、
(II)前記照射後の前記表面を互いに接触させた状態で昇温することにより、前記表面を接着面として前記第1の樹脂と前記第2の樹脂とを接着する工程と、
を含む樹脂の接着方法により接着されており、
前記剥離方法は、40℃以上の水およびアルコールから選ばれる少なくとも何れかの1つの液体を前記樹脂部同士の接着部分に供給することによって、前記樹脂部同士を互いに剥離する工程を含む、
樹脂物品の剥離方法。 - 樹脂部を有する2以上の部品を含み、前記2以上の部品が前記樹脂部において互いに接着されている樹脂物品について、接着されている前記樹脂部同士を互いに剥離する剥離方法であって、
前記樹脂部同士は、一方の樹脂部を第1の樹脂とし、他方の樹脂部を第2の樹脂として、
(I)第1および第2の樹脂の表面に、波長175nm以下の真空紫外光を照射する工程と、
(II)前記照射後の前記表面を互いに接触させた状態で昇温することにより、前記表面を接着面として前記第1の樹脂と前記第2の樹脂とを接着する工程と、
を含む樹脂の接着方法により接着されており、
前記剥離方法は、40℃未満の水およびアルコールから選ばれる少なくとも何れかの1つの液体を前記樹脂部同士の接着部分に供給し、かつ前記樹脂部を超音波で加振することによって、前記樹脂部同士を互いに剥離する工程を含む、
樹脂物品の剥離方法。 - 対向するように互いに接着された一対の樹脂基板を含み、前記樹脂基板の少なくとも一方の接着面に微細な流路が形成されているマイクロチップについて、接着されている前記樹脂基板同士を互いに剥離する剥離方法であって、
前記樹脂基板同士は、一方の樹脂基板を第1の樹脂とし、他方の樹脂基板を第2の樹脂として、
(I)第1および第2の樹脂の表面に、波長175nm以下の真空紫外光を照射する工程と、
(II)前記照射後の前記表面を互いに接触させた状態で昇温することにより、前記表面を接着面として前記第1の樹脂と前記第2の樹脂とを接着する工程と、
を含む樹脂の接着方法により接着されており、
前記剥離方法は、40℃以上の水およびアルコールから選ばれる少なくとも何れかの1つの液体を、前記樹脂基板同士の接着部分に供給することによって、前記樹脂基板同士を互いに剥離する工程を含む、
マイクロチップの剥離方法。 - 対向するように互いに接着された一対の樹脂基板を含み、前記樹脂基板の少なくとも一方の接着面に微細な流路が形成されているマイクロチップについて、接着されている前記樹脂基板同士を互いに剥離する剥離方法であって、
前記樹脂基板同士は、一方の樹脂基板を第1の樹脂とし、他方の樹脂基板を第2の樹脂として、
(I)第1および第2の樹脂の表面に、波長175nm以下の真空紫外光を照射する工程と、
(II)前記照射後の前記表面を互いに接触させた状態で昇温することにより、前記表面を接着面として前記第1の樹脂と前記第2の樹脂とを接着する工程と、
を含む樹脂の接着方法により接着されており、
前記剥離方法は、40℃未満の水およびアルコールから選ばれる少なくとも何れかの1つの液体を前記樹脂基板同士の接着部分に供給し、かつ前記樹脂基板を超音波で加振することによって、前記樹脂基板同士を互いに剥離する工程を含む、
マイクロチップの剥離方法。
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EP08867644A EP2236575A4 (en) | 2007-12-27 | 2008-12-26 | METHOD FOR BONDING A RESIN BY IRRADIATION OF EXTREME ULTRAVIOLET RADIATION, METHOD FOR MANUFACTURING RESIN ARTICLE OR RESIN MICROCHIP USING THE METHOD, AND RESIN ARTICLE OR MICROCHIP OBTAINED BY THE METHOD |
PCT/JP2008/073703 WO2009084622A1 (ja) | 2007-12-27 | 2008-12-26 | 真空紫外光照射による樹脂の接着方法、該方法を用いる樹脂物品又はマイクロチップの製造方法、該方法で製造される樹脂物品又はマイクロチップ |
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WO2013042377A1 (ja) * | 2011-09-22 | 2013-03-28 | 国立大学法人東京工業大学 | 合成樹脂の接着方法 |
JP2013103456A (ja) * | 2011-11-16 | 2013-05-30 | Kyoto Univ | 複合材料およびその製造方法 |
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