JP5572981B2 - フッ素ガス生成装置 - Google Patents
フッ素ガス生成装置 Download PDFInfo
- Publication number
- JP5572981B2 JP5572981B2 JP2009089444A JP2009089444A JP5572981B2 JP 5572981 B2 JP5572981 B2 JP 5572981B2 JP 2009089444 A JP2009089444 A JP 2009089444A JP 2009089444 A JP2009089444 A JP 2009089444A JP 5572981 B2 JP5572981 B2 JP 5572981B2
- Authority
- JP
- Japan
- Prior art keywords
- gas
- fluorine gas
- hydrogen fluoride
- fluorine
- inner tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 title claims description 179
- 239000011737 fluorine Substances 0.000 title claims description 179
- 229910052731 fluorine Inorganic materials 0.000 title claims description 179
- 239000007789 gas Substances 0.000 claims description 230
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 80
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims description 79
- 238000000746 purification Methods 0.000 claims description 49
- 150000003839 salts Chemical class 0.000 claims description 37
- 238000001514 detection method Methods 0.000 claims description 18
- 238000001816 cooling Methods 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 15
- 230000001105 regulatory effect Effects 0.000 claims description 15
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 14
- 238000009825 accumulation Methods 0.000 claims description 10
- 238000009835 boiling Methods 0.000 claims description 10
- 230000001276 controlling effect Effects 0.000 claims description 7
- 238000002844 melting Methods 0.000 claims description 7
- 230000008018 melting Effects 0.000 claims description 7
- 230000000630 rising effect Effects 0.000 claims description 2
- 239000012266 salt solution Substances 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 121
- 239000007788 liquid Substances 0.000 description 62
- 229910052757 nitrogen Inorganic materials 0.000 description 42
- 229910001873 dinitrogen Inorganic materials 0.000 description 37
- 238000007670 refining Methods 0.000 description 20
- 230000008929 regeneration Effects 0.000 description 13
- 238000011069 regeneration method Methods 0.000 description 13
- 239000006227 byproduct Substances 0.000 description 8
- 239000002994 raw material Substances 0.000 description 8
- 238000007599 discharging Methods 0.000 description 7
- 239000012159 carrier gas Substances 0.000 description 6
- 238000005868 electrolysis reaction Methods 0.000 description 5
- 238000005192 partition Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000011144 upstream manufacturing Methods 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 239000011698 potassium fluoride Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 230000009897 systematic effect Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910000792 Monel Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/245—Fluorine; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/02—Process control or regulation
- C25B15/021—Process control or regulation of heating or cooling
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Automation & Control Theory (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009089444A JP5572981B2 (ja) | 2009-04-01 | 2009-04-01 | フッ素ガス生成装置 |
EP10758387A EP2415906A4 (de) | 2009-04-01 | 2010-03-04 | Vorrichtung zur erzeugung von fluorgas |
CN2010800147025A CN102369311A (zh) | 2009-04-01 | 2010-03-04 | 氟气生成装置 |
KR1020117022150A KR20110129914A (ko) | 2009-04-01 | 2010-03-04 | 불소 가스 생성 장치 |
PCT/JP2010/054061 WO2010113611A1 (ja) | 2009-04-01 | 2010-03-04 | フッ素ガス生成装置 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009089444A JP5572981B2 (ja) | 2009-04-01 | 2009-04-01 | フッ素ガス生成装置 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2010242127A JP2010242127A (ja) | 2010-10-28 |
JP5572981B2 true JP5572981B2 (ja) | 2014-08-20 |
Family
ID=42827911
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009089444A Active JP5572981B2 (ja) | 2009-04-01 | 2009-04-01 | フッ素ガス生成装置 |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP2415906A4 (de) |
JP (1) | JP5572981B2 (de) |
KR (1) | KR20110129914A (de) |
CN (1) | CN102369311A (de) |
WO (1) | WO2010113611A1 (de) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101198350B1 (ko) | 2011-04-05 | 2012-11-08 | (주)원익머트리얼즈 | 고순도 헥사플루오르프로필렌 정제용기 |
JP5757168B2 (ja) * | 2011-06-10 | 2015-07-29 | セントラル硝子株式会社 | フッ素ガス生成装置 |
CN117160179B (zh) * | 2023-10-26 | 2024-02-13 | 福建德尔科技股份有限公司 | 一种电子级三氟化氯制备用原材料纯化设备 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2986885B2 (ja) * | 1990-10-03 | 1999-12-06 | 財団法人川村理化学研究所 | 電解フッ素化方法およびその装置 |
US6843258B2 (en) * | 2000-12-19 | 2005-01-18 | Applied Materials, Inc. | On-site cleaning gas generation for process chamber cleaning |
US20040151656A1 (en) * | 2001-11-26 | 2004-08-05 | Siegele Stephen H. | Modular molecular halogen gas generation system |
US20030121796A1 (en) * | 2001-11-26 | 2003-07-03 | Siegele Stephen H | Generation and distribution of molecular fluorine within a fabrication facility |
JP3855081B2 (ja) | 2002-07-01 | 2006-12-06 | 株式会社日立国際電気 | フッ素ガスによるクリーニング機構を備えたcvd装置およびcvd装置のフッ素ガスによるクリーニング方法 |
JP3905433B2 (ja) | 2002-07-11 | 2007-04-18 | レール・リキード−ソシエテ・アノニム・ア・ディレクトワール・エ・コンセイユ・ドゥ・スールベイランス・プール・レテュード・エ・レクスプロワタシオン・デ・プロセデ・ジョルジュ・クロード | フッ素ガス生成装置 |
KR100533411B1 (ko) * | 2002-11-08 | 2005-12-02 | 도요탄소 가부시키가이샤 | 불소가스 발생장치와 그 전해욕 액면 제어방법 |
JP4624699B2 (ja) * | 2004-03-18 | 2011-02-02 | レール・リキード−ソシエテ・アノニム・プール・レテュード・エ・レクスプロワタシオン・デ・プロセデ・ジョルジュ・クロード | フッ素ガス生成装置 |
JP5055484B2 (ja) | 2009-01-28 | 2012-10-24 | 株式会社メガチップス | 撮像システム |
-
2009
- 2009-04-01 JP JP2009089444A patent/JP5572981B2/ja active Active
-
2010
- 2010-03-04 EP EP10758387A patent/EP2415906A4/de not_active Withdrawn
- 2010-03-04 KR KR1020117022150A patent/KR20110129914A/ko not_active Application Discontinuation
- 2010-03-04 WO PCT/JP2010/054061 patent/WO2010113611A1/ja active Application Filing
- 2010-03-04 CN CN2010800147025A patent/CN102369311A/zh active Pending
Also Published As
Publication number | Publication date |
---|---|
EP2415906A4 (de) | 2012-08-29 |
EP2415906A1 (de) | 2012-02-08 |
WO2010113611A1 (ja) | 2010-10-07 |
KR20110129914A (ko) | 2011-12-02 |
CN102369311A (zh) | 2012-03-07 |
JP2010242127A (ja) | 2010-10-28 |
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