JP5415287B2 - Ｅｄｄｎを経由するｔｅｔａの新規製法 - Google Patents

Ｅｄｄｎを経由するｔｅｔａの新規製法 Download PDF

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Publication number
JP5415287B2
JP5415287B2 JP2009551210A JP2009551210A JP5415287B2 JP 5415287 B2 JP5415287 B2 JP 5415287B2 JP 2009551210 A JP2009551210 A JP 2009551210A JP 2009551210 A JP2009551210 A JP 2009551210A JP 5415287 B2 JP5415287 B2 JP 5415287B2
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Prior art keywords
eddn
eda
hydrogenation
fach
process according
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Expired - Fee Related
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Japanese (ja)
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JP2010520170A5 (https=
JP2010520170A (ja
Inventor
ダーメン キルステン
オフトリング アルフレート
バウマン カトリン
フーゴ ランドルフ
ハーン ティロ
メルダー ヨハン−ペーター
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
    • C07D295/125—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
    • C07D295/13—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/20—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic unsaturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2009551210A 2007-03-01 2008-02-28 Ｅｄｄｎを経由するｔｅｔａの新規製法 Expired - Fee Related JP5415287B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP07103295.7 2007-03-01
EP07103295 2007-03-01
PCT/EP2008/052413 WO2008104582A2 (de) 2007-03-01 2008-02-28 Neues verfahren zur herstellung von teta über eddn

Publications (3)

Publication Number Publication Date
JP2010520170A JP2010520170A (ja) 2010-06-10
JP2010520170A5 JP2010520170A5 (https=) 2011-04-14
JP5415287B2 true JP5415287B2 (ja) 2014-02-12

Family

ID=39433821

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2009551210A Expired - Fee Related JP5415287B2 (ja) 2007-03-01 2008-02-28 Ｅｄｄｎを経由するｔｅｔａの新規製法

Country Status (7)

Country Link
US (1) US8299249B2 (https=)
EP (2) EP2537835B1 (https=)
JP (1) JP5415287B2 (https=)
KR (1) KR20090122435A (https=)
CN (1) CN101622224B (https=)
RU (1) RU2472772C2 (https=)
WO (1) WO2008104582A2 (https=)

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CN101675026A (zh) * 2007-03-01 2010-03-17 巴斯夫欧洲公司 制备亚乙基胺混合物的方法
JP5377335B2 (ja) * 2007-03-01 2013-12-25 ビーエーエスエフ ソシエタス・ヨーロピア テトラエチレンペンタアミンの製造方法
WO2008104553A1 (de) * 2007-03-01 2008-09-04 Basf Se Verfahren zur herstellung von triethylentetraamin
CN102227413B (zh) 2008-10-06 2014-11-05 联合碳化化学品及塑料技术公司 制备环状n-氨基官能化三胺的方法
WO2010042161A1 (en) 2008-10-06 2010-04-15 Union Carbide Chemicals & Plastics Technology Llc Low metal (nickel and rhenium) catalyst compositions including acidic mixed metal oxide as support
JP2012504610A (ja) 2008-10-06 2012-02-23 ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー エチレンアミンの製造方法
CN102239002B (zh) 2008-10-06 2013-10-30 联合碳化化学品及塑料技术公司 低金属负载的氧化铝载体的催化剂组合物和氨基化方法
BRPI0922984B1 (pt) 2008-12-19 2017-10-24 Basf Se Process for preparing pure triethanolamine
JP5431582B2 (ja) 2009-06-18 2014-03-05 ビーエーエスエフ ソシエタス・ヨーロピア メチル置換ｔｅｔａ化合物
US8766010B2 (en) 2009-12-02 2014-07-01 Basf Se Method for distilling mixtures comprising ethylenediamine, N-methylethylenediamine, and water, and mixtures of ethylenediamine and N-methylethylenediamine having a low content of N-methylethylenediamine obtainable thereby
EP2542609A1 (en) * 2010-03-02 2013-01-09 Basf Se The use of linear triethylentetramine as curing agent for epoxy resins
EP2557074A1 (en) * 2011-08-11 2013-02-13 Astellas Pharma Inc. Process for the preparation of N,N,N',N'-tetrakis(3-aminopropyl)-1,4-butanediamine
CN103764614A (zh) * 2011-08-31 2014-04-30 巴斯夫欧洲公司 Eddn或edmn氢化反应出料的后处理方法
WO2013030287A1 (de) 2011-08-31 2013-03-07 Basf Se Verfahren zur herstellung von eddn und/oder edmn durch umsetzung von fach und eda
US20130053536A1 (en) * 2011-08-31 2013-02-28 Basf Se Process for preparing eddn and/or edmn and a process for preparing deta and/or teta
US8952156B2 (en) 2011-08-31 2015-02-10 Basf Se Process for working up reaction outputs from the hydrogenation of EDDN or EDMN
WO2013030259A1 (de) * 2011-08-31 2013-03-07 Basf Se Verfahren zur herstellung von teta
WO2013030144A1 (de) * 2011-08-31 2013-03-07 Basf Se Verfahren zur herstellung von eddn, edmn, teta und deta
US9012638B2 (en) 2011-08-31 2015-04-21 Basf Se Process for preparing EDDN and/or EDMN by conversion of FACH and EDA
WO2013030249A1 (de) * 2011-08-31 2013-03-07 Basf Se Verfahren zur herstellung von aminen durch hydrierung von nitrilen
WO2013030023A1 (de) * 2011-08-31 2013-03-07 Basf Se Verfahren zur herstellung von eddn und/oder edmn sowie ein verfahren zur herstellung von deta und/oder teta
WO2013030254A1 (de) * 2011-08-31 2013-03-07 Basf Se Verfahren zur herstellung von teta und/oder deta
IN2014CN00791A (https=) * 2011-08-31 2015-04-03 Basf Se
US9096497B2 (en) 2011-08-31 2015-08-04 Basf Se Process for preparing EDDN and EDMN
EP2751066A1 (de) * 2011-08-31 2014-07-09 Basf Se Verfahren zur herstellung von edfa und/oder edmfa und deta und/oder teta
WO2013030255A1 (de) * 2011-08-31 2013-03-07 Basf Se Verfahren zur herstellung von eddn und/oder edmn sowie verfahren zur herstellung von deta und/oder teta
JP2014525941A (ja) * 2011-08-31 2014-10-02 ビーエーエスエフ ソシエタス・ヨーロピア Ｅｄｆａおよび／またはｅｄｍｆａとｈｃｎとの反応によりｅｄｄｎおよび／またはｅｄｍｎを製造する方法
US8946459B2 (en) 2011-08-31 2015-02-03 Basf Se Process for preparing EDDN and/or EDMN by reacting EDFA and/or EDMFA with HCN
EP3077444B1 (en) 2013-12-02 2018-04-25 Dow Global Technologies LLC Preparation of high molecular weight, branched, acyclic polyalkyleneamines and mixtures thereof
US9888584B2 (en) 2014-12-31 2018-02-06 Invensas Corporation Contact structures with porous networks for solder connections, and methods of fabricating same
JP6671490B2 (ja) 2016-02-12 2020-03-25 ヌーリオン ケミカルズ インターナショナル ベスローテン フェノーツハップＮｏｕｒｙｏｎ Ｃｈｅｍｉｃａｌｓ Ｉｎｔｅｒｎａｔｉｏｎａｌ Ｂ．Ｖ． 高級エチレンアミンおよびエチレンアミン誘導体を調製する方法
US10844001B2 (en) 2016-02-12 2020-11-24 Nouryon Chemicals International B.V. Process to prepare higher ethylene amines and ethylene amine derivatives
MX378938B (es) 2016-02-12 2025-03-10 Akzo Nobel Chemicals Int Bv Proceso para preparar etilenaminas y derivados de etilenaminas superiores.
KR102585829B1 (ko) * 2017-07-10 2023-10-05 누리온 케미칼즈 인터내셔널 비.브이. 고급 에틸렌아민 또는 이의 우레아 유도체의 제조 방법
BR112020000020B1 (pt) 2017-07-10 2023-10-17 Nouryon Chemicals International B.V Processo para preparar etileno aminas, derivado de ureia de tetraetileno pentamina, derivado de ureia de pentaetileno-hexamina e uso do derivado de ureia
CN111278801B (zh) 2017-10-27 2023-05-26 巴斯夫欧洲公司 从含eda的混合物中分离n-甲基乙二胺
JP7268016B2 (ja) 2017-10-27 2023-05-02 ビーエーエスエフ ソシエタス・ヨーロピア エチレンアミンの製造方法
JP7277454B2 (ja) 2017-10-27 2023-05-19 ビーエーエスエフ ソシエタス・ヨーロピア エチレンアミンの製造方法
CN111263746B (zh) 2017-10-27 2024-01-19 巴斯夫欧洲公司 制备亚乙基胺的方法
CN109490453A (zh) * 2018-11-06 2019-03-19 广东省安全生产技术中心有限公司 一种三乙烯四胺的分离鉴定方法
CN113924286A (zh) * 2019-06-13 2022-01-11 陶氏环球技术有限责任公司 制备乙二胺四乙酸
EP4073026B1 (en) 2019-12-13 2024-06-05 Basf Se Separation of n-methylethylenediamine from eda-containing mixtures
KR20230091141A (ko) * 2020-12-16 2023-06-22 누리온 케미칼즈 인터내셔널 비.브이. 니트릴 화합물의 제조
WO2024002740A1 (en) 2022-06-29 2024-01-04 Basf Se Method for manufacture of ethyleneamines
JP2025520810A (ja) 2022-06-29 2025-07-03 ビーエーエスエフ ソシエタス・ヨーロピア エチレンアミンの製造方法

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Also Published As

Publication number Publication date
EP2537835B1 (de) 2014-04-30
CN101622224A (zh) 2010-01-06
WO2008104582A2 (de) 2008-09-04
RU2472772C2 (ru) 2013-01-20
WO2008104582A3 (de) 2009-02-12
KR20090122435A (ko) 2009-11-30
EP2129651A2 (de) 2009-12-09
JP2010520170A (ja) 2010-06-10
CN101622224B (zh) 2015-10-07
US20100121064A1 (en) 2010-05-13
EP2537835A1 (de) 2012-12-26
RU2009136185A (ru) 2011-04-10
EP2129651B1 (de) 2013-04-10
US8299249B2 (en) 2012-10-30

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