CN101622224B - 借助eddn生产teta的新方法 - Google Patents
借助eddn生产teta的新方法 Download PDFInfo
- Publication number
- CN101622224B CN101622224B CN200880006798.3A CN200880006798A CN101622224B CN 101622224 B CN101622224 B CN 101622224B CN 200880006798 A CN200880006798 A CN 200880006798A CN 101622224 B CN101622224 B CN 101622224B
- Authority
- CN
- China
- Prior art keywords
- eddn
- hydrogenation
- fach
- eda
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
- C07D295/125—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/13—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
- C07C211/20—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic unsaturated carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07103295.7 | 2007-03-01 | ||
| EP07103295 | 2007-03-01 | ||
| PCT/EP2008/052413 WO2008104582A2 (de) | 2007-03-01 | 2008-02-28 | Neues verfahren zur herstellung von teta über eddn |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101622224A CN101622224A (zh) | 2010-01-06 |
| CN101622224B true CN101622224B (zh) | 2015-10-07 |
Family
ID=39433821
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200880006798.3A Expired - Fee Related CN101622224B (zh) | 2007-03-01 | 2008-02-28 | 借助eddn生产teta的新方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8299249B2 (https=) |
| EP (2) | EP2129651B1 (https=) |
| JP (1) | JP5415287B2 (https=) |
| KR (1) | KR20090122435A (https=) |
| CN (1) | CN101622224B (https=) |
| RU (1) | RU2472772C2 (https=) |
| WO (1) | WO2008104582A2 (https=) |
Families Citing this family (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2478092C2 (ru) * | 2007-03-01 | 2013-03-27 | Басф Се | Способ получения смесей этиленаминов |
| JP5377335B2 (ja) * | 2007-03-01 | 2013-12-25 | ビーエーエスエフ ソシエタス・ヨーロピア | テトラエチレンペンタアミンの製造方法 |
| ES2390626T3 (es) * | 2007-03-01 | 2012-11-14 | Basf Se | Método de preparación de trietilentetraamina |
| JP5480276B2 (ja) | 2008-10-06 | 2014-04-23 | ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー | 担体として酸性混合金属酸化物を含む低金属(ニッケル及びレニウム)触媒組成物 |
| EP2356095B2 (en) | 2008-10-06 | 2017-09-27 | Union Carbide Chemicals & Plastics Technology LLC | Methods of making cyclic, n-amino functional triamines |
| JP5469173B2 (ja) | 2008-10-06 | 2014-04-09 | ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー | 金属低配合、アルミナ担持触媒組成物及びアミノ化方法 |
| JP2012504610A (ja) | 2008-10-06 | 2012-02-23 | ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー | エチレンアミンの製造方法 |
| WO2010069856A1 (de) | 2008-12-19 | 2010-06-24 | Basf Se | Verfahren zur herstellung von reinem triethanolamin (teoa) |
| US8586795B2 (en) | 2009-06-18 | 2013-11-19 | Basf Se | Methyl-substituted teta compounds |
| WO2011067226A1 (de) | 2009-12-02 | 2011-06-09 | Basf Se | Verfahren zur destillation von gemischen enthaltend ethylendiamin, n-methylethylendiamin und wasser und damit erhältliche gemische aus ethylendiamin und n-methylethylendiamin mit einem geringen n-methylethylendiamingehalt |
| WO2011107512A1 (en) * | 2010-03-02 | 2011-09-09 | Basf Se | The use of linear triethylentetramine as curing agent for epoxy resins |
| EP2557074A1 (en) * | 2011-08-11 | 2013-02-13 | Astellas Pharma Inc. | Process for the preparation of N,N,N',N'-tetrakis(3-aminopropyl)-1,4-butanediamine |
| CN103764614A (zh) * | 2011-08-31 | 2014-04-30 | 巴斯夫欧洲公司 | Eddn或edmn氢化反应出料的后处理方法 |
| WO2013030254A1 (de) * | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von teta und/oder deta |
| IN2014CN00796A (https=) | 2011-08-31 | 2015-04-03 | Basf Se | |
| WO2013030259A1 (de) * | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von teta |
| US20130053536A1 (en) * | 2011-08-31 | 2013-02-28 | Basf Se | Process for preparing eddn and/or edmn and a process for preparing deta and/or teta |
| JP2014525942A (ja) * | 2011-08-31 | 2014-10-02 | ビーエーエスエフ ソシエタス・ヨーロピア | Fachとedaの反応によるeddnおよび/またはedmnの製造方法 |
| CN103764618A (zh) * | 2011-08-31 | 2014-04-30 | 巴斯夫欧洲公司 | 制备edfa和/或edmfa以及deta和/或teta的方法 |
| US8952156B2 (en) | 2011-08-31 | 2015-02-10 | Basf Se | Process for working up reaction outputs from the hydrogenation of EDDN or EDMN |
| WO2013030144A1 (de) * | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von eddn, edmn, teta und deta |
| WO2013030249A1 (de) * | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von aminen durch hydrierung von nitrilen |
| WO2013030255A1 (de) * | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von eddn und/oder edmn sowie verfahren zur herstellung von deta und/oder teta |
| US9012638B2 (en) | 2011-08-31 | 2015-04-21 | Basf Se | Process for preparing EDDN and/or EDMN by conversion of FACH and EDA |
| WO2013030023A1 (de) * | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von eddn und/oder edmn sowie ein verfahren zur herstellung von deta und/oder teta |
| US8946459B2 (en) | 2011-08-31 | 2015-02-03 | Basf Se | Process for preparing EDDN and/or EDMN by reacting EDFA and/or EDMFA with HCN |
| US9096497B2 (en) | 2011-08-31 | 2015-08-04 | Basf Se | Process for preparing EDDN and EDMN |
| WO2013030143A1 (de) | 2011-08-31 | 2013-03-07 | Basf Se | Verfahren zur herstellung von eddn und/edmn |
| JP2017500386A (ja) | 2013-12-02 | 2017-01-05 | ダウ グローバル テクノロジーズ エルエルシー | 高分子量の分岐鎖非環式ポリアルキレンアミン及びその混合物の調製 |
| US9888584B2 (en) | 2014-12-31 | 2018-02-06 | Invensas Corporation | Contact structures with porous networks for solder connections, and methods of fabricating same |
| BR112018014272B1 (pt) | 2016-02-12 | 2021-12-28 | Akzo Nobel Chemicals International B.V. | Processo de preparação de etilenoaminas |
| MX390660B (es) * | 2016-02-12 | 2025-03-21 | Akzo Nobel Chemicals Int Bv | Proceso para preparar etilenaminas superiores y derivados de etilenamina. |
| BR112018014270B1 (pt) | 2016-02-12 | 2022-10-11 | Akzo Nobel Chemicals International B.V. | Processo de preparação de etilenoaminas |
| TWI762669B (zh) | 2017-07-10 | 2022-05-01 | 荷蘭商安科智諾貝爾化學國際公司 | 製造較高分子量伸乙基胺之方法 |
| TWI762670B (zh) * | 2017-07-10 | 2022-05-01 | 荷蘭商安科智諾貝爾化學國際公司 | 製備較高分子量伸乙基胺或其脲衍生物之方法 |
| US11339117B2 (en) | 2017-10-27 | 2022-05-24 | Basf Se | Method for the production of ethyleneamines |
| CN111278802A (zh) | 2017-10-27 | 2020-06-12 | 巴斯夫欧洲公司 | 制备亚乙基胺的方法 |
| JP7277455B2 (ja) | 2017-10-27 | 2023-05-19 | ビーエーエスエフ ソシエタス・ヨーロピア | Eda含有混合物からのn-メチルエチレンジアミンの分離除去 |
| JP7268016B2 (ja) | 2017-10-27 | 2023-05-02 | ビーエーエスエフ ソシエタス・ヨーロピア | エチレンアミンの製造方法 |
| CN109490453A (zh) * | 2018-11-06 | 2019-03-19 | 广东省安全生产技术中心有限公司 | 一种三乙烯四胺的分离鉴定方法 |
| CN113924286A (zh) * | 2019-06-13 | 2022-01-11 | 陶氏环球技术有限责任公司 | 制备乙二胺四乙酸 |
| JP2023510492A (ja) | 2019-12-13 | 2023-03-14 | ビーエーエスエフ ソシエタス・ヨーロピア | Eda含有混合物からのn-メチルエチレンジアミンの分離 |
| CA3201514A1 (en) * | 2020-12-16 | 2022-06-23 | Nouryon Chemicals International B.V. | Manufacture of nitrile compounds |
| CN119451938A (zh) | 2022-06-29 | 2025-02-14 | 巴斯夫欧洲公司 | 用于制造亚乙基胺的方法 |
| WO2024002740A1 (en) | 2022-06-29 | 2024-01-04 | Basf Se | Method for manufacture of ethyleneamines |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3462493A (en) | 1967-01-16 | 1969-08-19 | Dow Chemical Co | Process for making triethylenetetramine |
| DE2439275B2 (de) * | 1974-08-16 | 1978-09-21 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Diäthylentriamin und Triäthylentetramin aus Äthylendiamin |
| GB1579599A (en) | 1977-01-28 | 1980-11-19 | Texaco Development Corp | Catalyst pellet stabilization in the preparation of polyamines from polynitriles |
| JPS5459228A (en) * | 1977-10-17 | 1979-05-12 | Showa Denko Kk | Preparation of ethylenediamine diacetonitrile |
| US4235821A (en) | 1979-02-01 | 1980-11-25 | Suntech, Inc. | Hydrogenation of aliphatic nitriles to primary amines |
| US4404167A (en) | 1979-05-14 | 1983-09-13 | Rozenfeld Iosif L | Protecting steel and ferrous metals against H2 S corrosion |
| US4721811A (en) | 1985-08-26 | 1988-01-26 | W. R. Grace & Co. | Synthesis of aliphatic polyamines |
| EP0222934A1 (en) | 1985-09-11 | 1987-05-27 | The Dow Chemical Company | Process for preparation of polyalkylenepolyamines |
| JPH07107025B2 (ja) * | 1986-06-04 | 1995-11-15 | 三井東圧化学株式会社 | ポリエチレンポリアミンの製造方法 |
| SU1541204A1 (ru) * | 1988-01-25 | 1990-02-07 | Предприятие П/Я В-8469 | Способ совместного получени триэтилентетрамина и 1-[(2-аминоэтил)-аминоэтил]-пиперазина |
| US5030740A (en) * | 1988-10-14 | 1991-07-09 | The Dow Chemical Company | Process for preparing linearly-extended polyalkylenepolyamines |
| AU620205B2 (en) | 1989-02-07 | 1992-02-13 | W.R. Grace & Co.-Conn. | Preparation of tris(2-aminoethyl)amine |
| JPH04202163A (ja) * | 1990-11-30 | 1992-07-22 | Mitsui Toatsu Chem Inc | エチレンアミン類の製造法 |
| DE4428004A1 (de) | 1994-08-08 | 1996-02-15 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE59608407D1 (de) | 1995-05-09 | 2002-01-24 | Basf Ag | Kobaltkatalysatoren |
| JPH1045682A (ja) * | 1996-08-05 | 1998-02-17 | Tosoh Corp | 高品位ポリエチレンポリアミン類の製造方法 |
| CN1211487C (zh) * | 1996-12-06 | 2005-07-20 | 明尼苏达大学董事会 | 链球菌毒素a突变体及其使用方法 |
| US5869653A (en) | 1997-10-30 | 1999-02-09 | Air Products And Chemicals, Inc. | Hydrogenation of nitriles to produce amines |
| FR2773086B1 (fr) | 1997-12-29 | 2000-02-11 | Rhone Poulenc Fibres | Procede de regeneration d'un catalyseur d'hydrogenation procede d'hydrogenation de composes comprenant des fonctions nitriles |
| DE19809687A1 (de) | 1998-03-06 | 1999-09-09 | Basf Ag | Hydrierkatalysator |
| DE19826396A1 (de) | 1998-06-12 | 1999-12-16 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE10056840A1 (de) | 2000-11-16 | 2002-05-23 | Basf Ag | Verfahren zur Hydrierung von Nitrilen an Raney-Katalysatoren |
| DE10335991A1 (de) * | 2003-08-01 | 2005-02-24 | Basf Ag | Verfahren zur Herstellung von Ethylenaminen |
| EP3115777B1 (en) | 2004-04-19 | 2020-01-08 | PHC Holdings Corporation | Method for measuring blood components |
| PT1778618E (pt) * | 2004-07-19 | 2014-03-04 | Philera New Zealand Ltd | Síntese de trietilenotetraminas |
| RU2478092C2 (ru) * | 2007-03-01 | 2013-03-27 | Басф Се | Способ получения смесей этиленаминов |
| ES2390626T3 (es) * | 2007-03-01 | 2012-11-14 | Basf Se | Método de preparación de trietilentetraamina |
-
2008
- 2008-02-28 US US12/529,072 patent/US8299249B2/en not_active Expired - Fee Related
- 2008-02-28 JP JP2009551210A patent/JP5415287B2/ja not_active Expired - Fee Related
- 2008-02-28 KR KR1020097018164A patent/KR20090122435A/ko not_active Withdrawn
- 2008-02-28 EP EP08717210.2A patent/EP2129651B1/de not_active Not-in-force
- 2008-02-28 RU RU2009136185/04A patent/RU2472772C2/ru not_active IP Right Cessation
- 2008-02-28 WO PCT/EP2008/052413 patent/WO2008104582A2/de not_active Ceased
- 2008-02-28 EP EP12183433.7A patent/EP2537835B1/de not_active Not-in-force
- 2008-02-28 CN CN200880006798.3A patent/CN101622224B/zh not_active Expired - Fee Related
Non-Patent Citations (2)
| Title |
|---|
| Kuniyoshi MASUZAWA et al..Syntheses and Reactions of Nitrogen- and Sulfur-Analogs of 2-Piperazinone.《BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN》.1968,第41卷(第3期),第702-707页. * |
| Yi Li et al..The Syntheses of Cyclic Spermine Alkaloids: Analogues of Buchnerine and Budmunchiamine C.《HELVETICA CHIMICA ACTA》.2003,第86卷第310-323页. * |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2129651A2 (de) | 2009-12-09 |
| JP5415287B2 (ja) | 2014-02-12 |
| US8299249B2 (en) | 2012-10-30 |
| EP2537835B1 (de) | 2014-04-30 |
| RU2472772C2 (ru) | 2013-01-20 |
| KR20090122435A (ko) | 2009-11-30 |
| EP2537835A1 (de) | 2012-12-26 |
| US20100121064A1 (en) | 2010-05-13 |
| WO2008104582A3 (de) | 2009-02-12 |
| JP2010520170A (ja) | 2010-06-10 |
| WO2008104582A2 (de) | 2008-09-04 |
| EP2129651B1 (de) | 2013-04-10 |
| CN101622224A (zh) | 2010-01-06 |
| RU2009136185A (ru) | 2011-04-10 |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151007 |
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| CF01 | Termination of patent right due to non-payment of annual fee |