JP5203208B2 - チタノケイ酸塩ゼオライトts−1の調製 - Google Patents
チタノケイ酸塩ゼオライトts−1の調製 Download PDFInfo
- Publication number
- JP5203208B2 JP5203208B2 JP2008531225A JP2008531225A JP5203208B2 JP 5203208 B2 JP5203208 B2 JP 5203208B2 JP 2008531225 A JP2008531225 A JP 2008531225A JP 2008531225 A JP2008531225 A JP 2008531225A JP 5203208 B2 JP5203208 B2 JP 5203208B2
- Authority
- JP
- Japan
- Prior art keywords
- reaction mixture
- sio
- zeolite
- water
- titanosilicate zeolite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
- C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2973—Particular cross section
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Catalysts (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/226,609 | 2005-09-13 | ||
| US11/226,609 US7837977B2 (en) | 2005-09-13 | 2005-09-13 | Preparation of titanosilicate zeolite TS-1 |
| PCT/US2006/035358 WO2007033102A2 (en) | 2005-09-13 | 2006-09-12 | Preparation of titanosilicate zeolite ts-1 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009507757A JP2009507757A (ja) | 2009-02-26 |
| JP2009507757A5 JP2009507757A5 (enExample) | 2009-10-08 |
| JP5203208B2 true JP5203208B2 (ja) | 2013-06-05 |
Family
ID=37855392
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008531225A Expired - Fee Related JP5203208B2 (ja) | 2005-09-13 | 2006-09-12 | チタノケイ酸塩ゼオライトts−1の調製 |
Country Status (9)
| Country | Link |
|---|---|
| US (7) | US7837977B2 (enExample) |
| EP (1) | EP1931596A4 (enExample) |
| JP (1) | JP5203208B2 (enExample) |
| KR (1) | KR101310989B1 (enExample) |
| CN (1) | CN101291877B (enExample) |
| AU (1) | AU2006291153B2 (enExample) |
| CA (1) | CA2621400C (enExample) |
| WO (1) | WO2007033102A2 (enExample) |
| ZA (1) | ZA200803019B (enExample) |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009055216A2 (en) | 2007-10-26 | 2009-04-30 | Exxonmobil Chemical Patents Inc. | Method of preparing a molecular sieve composition |
| ITMI20072342A1 (it) * | 2007-12-14 | 2009-06-15 | Polimeri Europa Spa | Processo per preparare zeoliti ts-1 |
| US8609925B2 (en) * | 2008-06-30 | 2013-12-17 | Uop Llc | Adsorbents with improved mass transfer properties and their use in the adsorptive separation of para-xylene |
| US7820869B2 (en) * | 2008-06-30 | 2010-10-26 | Uop Llc | Binderless adsorbents and their use in the adsorptive separation of para-xylene |
| US20090326308A1 (en) * | 2008-06-30 | 2009-12-31 | Uop Llc | Binderless adsorbents comprising nano-size zeolite x and their use in the adsorptive separation of para-xylene |
| US7812208B2 (en) * | 2008-09-22 | 2010-10-12 | Uop Llc | Binderless adsorbents with improved mass transfer properties and their use in the adsorptive separation of para-xylene |
| WO2011062123A1 (ja) * | 2009-11-18 | 2011-05-26 | 日本電産サンキョー株式会社 | レンズ駆動装置 |
| US8992884B2 (en) * | 2009-11-30 | 2015-03-31 | Chevron U.S.A. Inc. | Preparation of X zeolite |
| CZ2010245A3 (cs) * | 2010-04-01 | 2011-05-18 | Výzkumný ústav anorganické chemie, a.s. | Zpusob výroby titanosilikátu Ti-ZSM-5 z polotovaru |
| CN102145300B (zh) * | 2011-03-08 | 2012-11-28 | 华东师范大学 | 一种微球ts-1催化剂及其制备方法 |
| US8431764B2 (en) * | 2011-04-13 | 2013-04-30 | Uop Llc | Para-xylene-separation with aluminosilicate X-type zeolite compositions with low LTA-type zeolite |
| JP2014522357A (ja) * | 2011-04-13 | 2014-09-04 | ユーオーピー エルエルシー | 少量のlta型ゼオライトを含む結合剤転化アルミノケイ酸塩x型ゼオライト組成物 |
| JP5813859B2 (ja) | 2011-04-15 | 2015-11-17 | エクソンモービル ケミカル パテンツ インコーポレイテッド | M41s族モレキュラーシーブの合成およびその使用 |
| SG194087A1 (en) | 2011-04-15 | 2013-11-29 | Exxonmobil Chem Patents Inc | Process for producing molecular sieve materials |
| WO2012146146A1 (zh) * | 2011-04-29 | 2012-11-01 | 岳阳昌德化工实业有限公司 | 一种氧化环己烷的设备及一种环己烷氧化的方法 |
| CN102766032B (zh) * | 2011-05-05 | 2014-10-01 | 中国石油化工股份有限公司 | 一种环己烷氧化的方法 |
| CN102502690A (zh) | 2011-10-31 | 2012-06-20 | 大连理工大学 | 一种基于季铵盐和无机碱混合液的ts-1改性方法 |
| WO2014053483A1 (en) | 2012-10-05 | 2014-04-10 | Basf Se | Process for the production of a zeolitic material employing elemental precursors |
| CN104418343B (zh) * | 2013-08-20 | 2016-06-08 | 中触媒新材料股份有限公司 | 一种ts-1钛硅分子筛及其制备方法和应用 |
| CN104418354B (zh) * | 2013-09-09 | 2016-07-20 | 中国石油化工股份有限公司 | 一种钛硅微孔材料及其合成方法 |
| CN104556104B (zh) * | 2013-10-29 | 2017-05-24 | 中国石油化工股份有限公司 | 一种使用有机季铵盐模板剂合成钛硅分子筛的方法 |
| DE102013021750A1 (de) * | 2013-12-20 | 2015-06-25 | Clariant International Ltd. | Titanhaltige Zeolithkatalysatoren zur Oxidation von Methan in Abgasströmen |
| CN103864093B (zh) * | 2014-02-18 | 2015-08-12 | 太原大成环能化工技术有限公司 | 一种含钛分子筛的阶梯式晶化制备方法 |
| CN104229820B (zh) * | 2014-09-11 | 2016-02-24 | 黎明化工研究设计院有限责任公司 | 一种制备ts-1钛硅分子筛的方法 |
| CN107032365B (zh) * | 2015-07-29 | 2019-01-29 | 武汉理工大学 | 一种钛硅分子筛ts-1的固相合成方法 |
| CN106829996B (zh) * | 2015-12-03 | 2019-03-15 | 中国石油大学(华东) | 一种钛硅分子筛及其制备方法 |
| CN105728034B (zh) * | 2016-03-23 | 2018-09-28 | 华东师范大学 | 一种Ti-ECNU-5钛硅分子筛催化剂及其制备方法和应用 |
| CN106379912B (zh) * | 2016-08-29 | 2018-06-29 | 上海交通大学 | 一种多级孔道钛硅分子筛的制备方法 |
| CN109721065B (zh) * | 2017-10-31 | 2020-10-27 | 中国石油化工股份有限公司 | 钛硅分子筛的生产方法以及由该方法生产的钛硅分子筛和氨肟化反应方法 |
| CN108554444B (zh) * | 2018-05-08 | 2019-07-30 | 哈尔滨工业大学 | 一种多级孔Ti-ZSM-5分子筛汽车尾气催化剂的制备方法 |
| US12478959B2 (en) | 2019-12-19 | 2025-11-25 | Basf Se | Continuous synthesis of a titanosilicate zeolitic material, said zeolitic material, molding prepared thereof, and their use |
| CN111569938A (zh) * | 2020-06-04 | 2020-08-25 | 深圳市汇德丰控股集团有限公司 | 一种加氢精制催化剂及其制备方法与应用 |
| CN111732483B (zh) * | 2020-08-25 | 2020-11-17 | 烟台水禾土生物科技有限公司 | 浒苔生物肥的发酵方法 |
| CN113845126B (zh) * | 2021-05-31 | 2023-04-07 | 大连理工大学 | 一种钛硅分子筛及其制备方法和应用 |
| CN114835137B (zh) * | 2022-05-25 | 2023-05-09 | 中国矿业大学(北京) | 一种ddr分子筛的制备方法 |
| CN114853029A (zh) * | 2022-06-08 | 2022-08-05 | 青岛科技大学 | 一种钛硅分子筛的制备方法、一种过渡金属负载型钛硅分子筛的制备方法 |
| CN115920958B (zh) * | 2022-12-21 | 2024-06-25 | 中触媒新材料股份有限公司 | 一种钛硅分子筛的改性方法及其应用 |
Family Cites Families (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3119656A (en) | 1960-06-06 | 1964-01-28 | Nat Distillers Chem Corp | Preparation of trivalent titanium salts |
| US3094383A (en) | 1960-12-16 | 1963-06-18 | Minerals & Chem Philipp Corp | Method for making synthetic zeolitic material |
| US4058586A (en) | 1976-02-25 | 1977-11-15 | W. R. Grace & Co. | Forming and crystallization process for molecular sieve manufacture |
| IT1127311B (it) | 1979-12-21 | 1986-05-21 | Anic Spa | Materiale sintetico,cristallino,poroso costituito da ossidi di silicio e titanio,metodo per la sua preparazione e suoi usi |
| US4381255A (en) | 1981-01-14 | 1983-04-26 | W. R. Grace & Co. | Binderless zeolite extrudates and method of producing |
| IT1152299B (it) * | 1982-07-28 | 1986-12-31 | Anic Spa | Procedimento per l'espossidazione di composti olefinici |
| JPS60127217A (ja) * | 1983-12-09 | 1985-07-06 | Japan Synthetic Rubber Co Ltd | チタノシリケ−トゼオライトの製造方法 |
| FR2565847B1 (fr) | 1984-06-18 | 1986-08-29 | Inst Francais Du Petrole | Synthese et utilisation de zeolithes preformees |
| US4822899A (en) * | 1985-04-12 | 1989-04-18 | The University Of Michigan | Metallic porphyrin complexes as catalysts in epoxidation reactions |
| GB9101456D0 (en) | 1991-01-23 | 1991-03-06 | Exxon Chemical Patents Inc | Process for producing substantially binder-free zeolite |
| KR950704191A (ko) | 1992-12-16 | 1995-11-17 | 더블유. 케이스 터너 | 알루미노실리케이트 제올라이트의 제조방법(preparation of aluminosilicate zeolites) |
| US5474754A (en) * | 1994-08-15 | 1995-12-12 | Arco Chemical Technology, L.P. | Preparation of an aluminosilicotitanate isomorphous with zeolite beta |
| DE19608493A1 (de) * | 1996-03-05 | 1997-09-11 | Basf Ag | Edelmetallfreie Katalysatorzusammensetzung zur Erzeugung von Wasserstoffperoxid |
| CN1050584C (zh) | 1996-06-05 | 2000-03-22 | 中国石油化工总公司 | 一种钛硅分子筛(ts-1)的制备方法 |
| CN1050370C (zh) | 1996-06-07 | 2000-03-15 | 田树霖 | 长效快速抗菌聚乙烯产品的制备方法 |
| US5919430A (en) * | 1996-06-19 | 1999-07-06 | Degussa Aktiengesellschaft | Preparation of crystalline microporous and mesoporous metal silicates, products produced thereby and use thereof |
| US5688484A (en) * | 1996-07-29 | 1997-11-18 | Arco Chemical Technology, L.P. | Non-hydrothermal method of making a titanium-containing zeolite |
| US5939044A (en) | 1996-12-31 | 1999-08-17 | Chevron U.S.A. Inc. | Zeolite SSZ-36 |
| DE19723950A1 (de) * | 1997-06-06 | 1998-12-10 | Basf Ag | Verfahren zur Oxidation einer mindestens eine C-C-Doppelbindung aufweisenden organischen Verbindung |
| BE1011581A3 (fr) * | 1997-12-01 | 1999-11-09 | Solvay | Catalyseur a base de zeolite, son utilisation et procede d'epoxydation en presence de ce catalyseur. |
| JP2000185912A (ja) * | 1998-12-22 | 2000-07-04 | Tosoh Corp | 結晶性チタノシリケートゼオライトおよびその製造方法 |
| JP4646409B2 (ja) * | 1999-04-08 | 2011-03-09 | ダウ グローバル テクノロジーズ インコーポレイティド | 酸化された金触媒を使用してオレフィンをオレフィンオキシドにハイドロ酸化するための方法 |
| EP1061046B1 (en) | 1999-06-18 | 2007-09-26 | Nippon Shokubai Co., Ltd. | Molding of binderless zeolite, method for its production and its use |
| EP1129991A1 (de) * | 2000-03-02 | 2001-09-05 | Degussa AG | Verfahren zur Herstellung eines titanhaltigen Zeolithen |
| KR100392408B1 (ko) | 2000-10-05 | 2003-07-22 | 학교법인 서강대학교 | 미세다공성 제올라이트 또는 유사 물질로 된 거대다공성발포체 및 스폰지 구조의 고분자 주형을 이용하는 이의제조 방법 |
| US6534661B1 (en) * | 2000-12-28 | 2003-03-18 | Hydrocarbon Technologies, Inc. | Integrated process and dual-function catalyst for olefin epoxidation |
| DE10232406A1 (de) | 2002-07-17 | 2004-01-29 | Basf Ag | Verfahren zur Herstellung eines zeolithhaltigen Feststoffes |
| CN1401569A (zh) | 2002-08-26 | 2003-03-12 | 大连理工大学 | 一种纳米级钛硅分子筛催化剂的快速合成方法及应用 |
| US6960671B2 (en) | 2002-09-20 | 2005-11-01 | Arco Chemical Technology, L.P. | Process for direct oxidation of propylene to propylene oxide and large particle size titanium silicalite catalysts for use therein |
| US20050129952A1 (en) | 2003-09-29 | 2005-06-16 | Questair Technologies Inc. | High density adsorbent structures |
| US6984606B2 (en) | 2004-02-19 | 2006-01-10 | Lyondell Chemical Technology, L.P. | Epoxidation catalyst |
| US7276464B2 (en) * | 2004-06-17 | 2007-10-02 | Lyondell Chemical Technology, L.P. | Titanium zeolite catalysts |
| US7211239B2 (en) | 2005-04-22 | 2007-05-01 | Basf Aktiengesellschaft | Process for preparing a nanosized zeolitic material |
-
2005
- 2005-09-13 US US11/226,609 patent/US7837977B2/en not_active Expired - Fee Related
-
2006
- 2006-09-12 ZA ZA200803019A patent/ZA200803019B/xx unknown
- 2006-09-12 JP JP2008531225A patent/JP5203208B2/ja not_active Expired - Fee Related
- 2006-09-12 CN CN2006800386956A patent/CN101291877B/zh not_active Expired - Fee Related
- 2006-09-12 KR KR1020087008775A patent/KR101310989B1/ko not_active Expired - Fee Related
- 2006-09-12 CA CA2621400A patent/CA2621400C/en not_active Expired - Fee Related
- 2006-09-12 EP EP06803362.0A patent/EP1931596A4/en not_active Withdrawn
- 2006-09-12 AU AU2006291153A patent/AU2006291153B2/en not_active Ceased
- 2006-09-12 WO PCT/US2006/035358 patent/WO2007033102A2/en not_active Ceased
-
2008
- 2008-02-18 US US12/032,949 patent/US20080292542A1/en not_active Abandoned
- 2008-02-19 US US12/033,695 patent/US7956204B2/en not_active Expired - Lifetime
- 2008-02-19 US US12/033,687 patent/US20080138619A1/en not_active Abandoned
-
2009
- 2009-10-28 US US12/607,901 patent/US20100048385A1/en not_active Abandoned
-
2010
- 2010-08-26 US US12/868,860 patent/US20100324316A1/en not_active Abandoned
-
2012
- 2012-05-30 US US13/483,596 patent/US20120316352A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| WO2007033102A3 (en) | 2007-11-08 |
| WO2007033102A2 (en) | 2007-03-22 |
| JP2009507757A (ja) | 2009-02-26 |
| US7837977B2 (en) | 2010-11-23 |
| US7956204B2 (en) | 2011-06-07 |
| ZA200803019B (en) | 2009-07-29 |
| CA2621400C (en) | 2014-03-18 |
| EP1931596A4 (en) | 2015-06-03 |
| AU2006291153B2 (en) | 2012-08-23 |
| CA2621400A1 (en) | 2007-03-22 |
| CN101291877A (zh) | 2008-10-22 |
| EP1931596A2 (en) | 2008-06-18 |
| AU2006291153A1 (en) | 2007-03-22 |
| US20100324316A1 (en) | 2010-12-23 |
| US20070059237A1 (en) | 2007-03-15 |
| US20080146827A1 (en) | 2008-06-19 |
| KR20080044348A (ko) | 2008-05-20 |
| US20120316352A1 (en) | 2012-12-13 |
| US20080138619A1 (en) | 2008-06-12 |
| CN101291877B (zh) | 2012-04-18 |
| US20080292542A1 (en) | 2008-11-27 |
| US20100048385A1 (en) | 2010-02-25 |
| KR101310989B1 (ko) | 2013-09-24 |
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