JP4567465B2 - 表面改質された有機分子を含有するエマルジョン - Google Patents

表面改質された有機分子を含有するエマルジョン Download PDF

Info

Publication number
JP4567465B2
JP4567465B2 JP2004564896A JP2004564896A JP4567465B2 JP 4567465 B2 JP4567465 B2 JP 4567465B2 JP 2004564896 A JP2004564896 A JP 2004564896A JP 2004564896 A JP2004564896 A JP 2004564896A JP 4567465 B2 JP4567465 B2 JP 4567465B2
Authority
JP
Japan
Prior art keywords
phase
emulsion
dispersed
organic molecules
continuous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2004564896A
Other languages
English (en)
Japanese (ja)
Other versions
JP2006512199A (ja
JP2006512199A5 (enExample
Inventor
アール．ジュニア バラン，ジミー
エス． ステフェリー，ジェイムズ
ダブリュ． ステイン，スティーブン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of JP2006512199A publication Critical patent/JP2006512199A/ja
Publication of JP2006512199A5 publication Critical patent/JP2006512199A5/ja
Application granted granted Critical
Publication of JP4567465B2 publication Critical patent/JP4567465B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/09—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids
    • C08J3/11—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in organic liquids from solid polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/003—Organic compounds containing only carbon and hydrogen
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/017—Mixtures of compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/16—Amines or polyamines
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/39—Fullerene, e.g. c60, c70 derivative and related process
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/40—Fullerene composition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Composite Materials (AREA)
  • Colloid Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
  • Cosmetics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Medicinal Preparation (AREA)
JP2004564896A 2002-12-31 2003-11-11 表面改質された有機分子を含有するエマルジョン Expired - Fee Related JP4567465B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/335,495 US7001580B2 (en) 2002-12-31 2002-12-31 Emulsions including surface-modified organic molecules
PCT/US2003/035738 WO2004060543A2 (en) 2002-12-31 2003-11-11 Emulsions including surface-modified organic molecules

Publications (3)

Publication Number Publication Date
JP2006512199A JP2006512199A (ja) 2006-04-13
JP2006512199A5 JP2006512199A5 (enExample) 2006-12-28
JP4567465B2 true JP4567465B2 (ja) 2010-10-20

Family

ID=32655365

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2004564896A Expired - Fee Related JP4567465B2 (ja) 2002-12-31 2003-11-11 表面改質された有機分子を含有するエマルジョン

Country Status (8)

Country Link
US (2) US7001580B2 (enExample)
EP (1) EP1587609B1 (enExample)
JP (1) JP4567465B2 (enExample)
CN (1) CN100377771C (enExample)
AT (1) ATE357967T1 (enExample)
AU (1) AU2003294253A1 (enExample)
DE (1) DE60312895T2 (enExample)
WO (1) WO2004060543A2 (enExample)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7109247B2 (en) * 2003-05-30 2006-09-19 3M Innovative Properties Company Stabilized particle dispersions containing nanoparticles
US7459146B2 (en) * 2003-05-30 2008-12-02 3M Innovative Properties Company Stabilized aerosol dispersions
US20040242729A1 (en) * 2003-05-30 2004-12-02 3M Innovative Properties Company Stabilized particle dispersions containing surface-modified inorganic nanoparticles
EP1667636A2 (fr) * 2003-09-29 2006-06-14 Rhodia Chimie Emulsions comprenant un polymere dendritique et utilisation d'un polymere dendritique comme agent d emulsification
ES2297728T5 (es) * 2004-08-17 2013-11-04 Unilever N.V. Procedimiento de tratamiento del cabello con composiciones que comprenden un polímero dendrítico
ES2360639T5 (es) 2004-08-17 2014-02-26 Unilever N.V. Procedimiento de tratamiento del cabello con una composición que comprende una macromolécula dendrítica
US7976693B2 (en) 2006-07-17 2011-07-12 Westinghouse Electric Company Llc Hydrogen generation process with dual pressure multi stage electrolysis
WO2011068678A1 (en) 2009-12-03 2011-06-09 3M Innovative Properties Company Method of electrostatic deposition of particles, abrasive grain and articles
CN102639650A (zh) 2009-12-03 2012-08-15 3M创新有限公司 通过添加疏水性纳米粒子抑制粉末吸水性的方法
US9085463B2 (en) 2011-01-17 2015-07-21 Marelle, Llc Water-soluble functionalized fullerenes
FR3001592A1 (fr) 2013-01-29 2014-08-01 Schneider Toshiba Inverter Convertisseur de puissance multi-niveaux
CN104941542B (zh) * 2015-06-09 2017-03-22 中国科学院山西煤炭化学研究所 一种无需分散剂的酚醛树脂微球的简易制备方法
CN106362641B (zh) * 2016-12-02 2018-12-04 威海晨源分子新材料有限公司 一种树枝状聚酰胺-胺破乳剂及其制备方法
CN109161293A (zh) * 2018-08-16 2019-01-08 苏州火睿新材料科技有限公司 富勒烯改性水性涂料及其制备方法
CN115155472B (zh) * 2022-07-07 2023-10-13 中科南京绿色制造产业创新研究院 一种采用相转化法制备聚合物微球的方法

Family Cites Families (50)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2801185A (en) 1952-05-16 1957-07-30 Du Pont Silica hydrosol powder
US4478876A (en) 1980-12-18 1984-10-23 General Electric Company Process of coating a substrate with an abrasion resistant ultraviolet curable composition
US4379201A (en) 1981-03-30 1983-04-05 Minnesota Mining And Manufacturing Company Multiacrylate cross-linking agents in pressure-sensitive photoadhesives
US4455205A (en) 1981-06-01 1984-06-19 General Electric Company UV Curable polysiloxane from colloidal silica, methacryloyl silane, diacrylate, resorcinol monobenzoate and photoinitiator
US4491508A (en) 1981-06-01 1985-01-01 General Electric Company Method of preparing curable coating composition from alcohol, colloidal silica, silylacrylate and multiacrylate monomer
US4486504A (en) 1982-03-19 1984-12-04 General Electric Company Solventless, ultraviolet radiation-curable silicone coating compositions
US4507466A (en) 1983-01-07 1985-03-26 The Dow Chemical Corporation Dense star polymers having core, core branches, terminal groups
US4522958A (en) 1983-09-06 1985-06-11 Ppg Industries, Inc. High-solids coating composition for improved rheology control containing chemically modified inorganic microparticles
US4609689A (en) * 1984-04-27 1986-09-02 Becton, Dickinson And Company Method of preparing fluorescently labeled microbeads
US4737559A (en) 1986-05-19 1988-04-12 Minnesota Mining And Manufacturing Co. Pressure-sensitive adhesive crosslinked by copolymerizable aromatic ketone monomers
JPS6328443A (ja) * 1986-07-21 1988-02-06 Shiseido Co Ltd 水中油型メーキャップ化粧料
US6312679B1 (en) 1986-08-18 2001-11-06 The Dow Chemical Company Dense star polymer conjugates as dyes
US5560929A (en) * 1986-08-18 1996-10-01 The Dow Chemical Company Structured copolymers and their use as absorbents, gels and carriers of metal ions
US5037579A (en) 1990-02-12 1991-08-06 Nalco Chemical Company Hydrothermal process for producing zirconia sol
US5258225A (en) 1990-02-16 1993-11-02 General Electric Company Acrylic coated thermoplastic substrate
GB2244714B (en) * 1990-05-31 1993-10-06 Sanyo Chemical Ind Ltd Foamed polyurethane-forming composition,foamed polyurethane and process for making the same
JPH04161500A (ja) * 1990-10-25 1992-06-04 Lion Corp 乳濁光沢性液体洗浄剤
FR2698002B1 (fr) * 1992-11-13 1995-01-13 Oreal Composition cosmétique de maquillage contenant un fullerène ou un mélange de fullerènes comme agent pigmentant.
US5387617A (en) * 1993-01-22 1995-02-07 The Dow Chemical Company Small cell foams and blends and a process for their preparation
JPH06242543A (ja) 1993-02-18 1994-09-02 Fuji Photo Film Co Ltd ハロゲン化銀感光材料
JP3432892B2 (ja) * 1994-06-08 2003-08-04 日本碍子株式会社 改質ガスのｃｏ除去方法
AUPM623994A0 (en) * 1994-06-15 1994-07-07 Biomolecular Research Institute Limited Antiviral dendrimers
US5449519C1 (en) * 1994-08-09 2001-05-01 Revlon Consumer Prod Corp Cosmetic compositions having keratolytic and anti-acne activity
US5648407A (en) 1995-05-16 1997-07-15 Minnesota Mining And Manufacturing Company Curable resin sols and fiber-reinforced composites derived therefrom
FR2746302B1 (fr) * 1996-03-20 1998-12-24 Oreal Compositions cosmetiques comprenant des nanopigments
DE19625982A1 (de) * 1996-06-28 1998-01-02 Wella Ag Kosmetisches Mittel zur Haarbehandlung mit Dendrimeren
FR2759582A1 (fr) * 1997-02-14 1998-08-21 Oreal Composition deodorante
FR2760641B1 (fr) 1997-03-13 2000-08-18 Oreal Emulsion huile-dans-eau stable, son procede de fabrication et son utilisation dans les domaines cosmetique et dermatologique
US6440399B1 (en) * 1997-03-25 2002-08-27 Beiersdorf Ag Emulsifier-free finely dispersed systems of the water-in-oil type
US6245318B1 (en) * 1997-05-27 2001-06-12 Mallinckrodt Inc. Selectively binding ultrasound contrast agents
US5879715A (en) * 1997-09-02 1999-03-09 Ceramem Corporation Process and system for production of inorganic nanoparticles
DE19742761A1 (de) 1997-09-27 1999-04-01 Gerd Dr Rossmy An ihrer Oberfläche anisotrop verteilte überwiegend hydrophile und überwiegend hydrophobe Domänen aufweisende amphiphile Teilchen oder Moleküle
DE69919794T2 (de) * 1998-03-17 2005-09-01 Hutchinson Stabile emulsionen, verfahren zu deren herstellung und ihre anwendungen
DE19811790A1 (de) * 1998-03-18 1999-09-23 Bayer Ag Nanopartikel enthaltende transparente Lackbindemittel mit verbesserter Verkratzungsbeständigkeit, ein Verfahren zur Herstellung sowie deren Verwendung
US6280748B1 (en) * 1998-06-12 2001-08-28 Dow Corning Toray Silicone, Ltd. Cosmetic raw material cosmetic product and method for manufacturing cosmetic products
KR100547959B1 (ko) 1998-07-30 2006-02-02 미네소타 마이닝 앤드 매뉴팩춰링 캄파니 투명한 금속 산화물 콜로이드 및 세라머를 제조하기 위한 나노크기 금속 산화물 입자
DE19834819A1 (de) * 1998-08-01 2000-02-03 Beiersdorf Ag Emulgatorfreie feindisperse Systeme vom Typ Öl-in-Wasser und Wasser-in-Öl
DE19842786A1 (de) * 1998-09-18 2000-03-23 Beiersdorf Ag Emulgatorfreie feindisperse Systeme vom Typ Öl-in-Wasser und Wasser-in-Öl
DE19842732A1 (de) * 1998-09-18 2000-03-23 Beiersdorf Ag Emulgatorfreie feindisperse Systeme vom Typ Öl-in-Wasser und Wasser-in-Öl
US6258896B1 (en) * 1998-12-18 2001-07-10 3M Innovative Properties Company Dendritic polymer dispersants for hydrophobic particles in water-based systems
TWI228522B (en) 1999-06-04 2005-03-01 Fuji Spinning Co Ltd Urethane molded products for polishing pad and method for making same
US6436424B1 (en) * 2000-03-20 2002-08-20 Biosphere Medical, Inc. Injectable and swellable microspheres for dermal augmentation
FR2808704B1 (fr) 2000-05-10 2002-08-16 Rhodia Chimie Sa Agents tensioactifs formes par des particules minerales de dimension nanometrique de surface modifiee
JP3423922B2 (ja) * 2000-06-01 2003-07-07 海洋科学技術センター フラーレン水分散液の製造法
WO2002041987A2 (en) * 2000-10-25 2002-05-30 Tufts University Polymeric microspheres
US6586483B2 (en) 2001-01-08 2003-07-01 3M Innovative Properties Company Foam including surface-modified nanoparticles
FR2819406B1 (fr) * 2001-01-15 2003-02-21 Oreal Composition cosmetique contenant des filtres mineraux
WO2003082232A1 (en) * 2002-03-28 2003-10-09 The Procter & Gamble Company Particle stabilizing compositions
US7141612B2 (en) * 2002-12-31 2006-11-28 3M Innovative Properties Company Stabilized foams including surface-modified organic molecules
US7129277B2 (en) * 2002-12-31 2006-10-31 3M Innovative Properties Company Emulsions including surface-modified inorganic nanoparticles

Also Published As

Publication number Publication date
WO2004060543A2 (en) 2004-07-22
CN1732038A (zh) 2006-02-08
EP1587609B1 (en) 2007-03-28
EP1587609A2 (en) 2005-10-26
WO2004060543A3 (en) 2004-09-23
US20060002843A1 (en) 2006-01-05
DE60312895T2 (de) 2008-01-17
DE60312895D1 (de) 2007-05-10
AU2003294253A8 (en) 2004-07-29
JP2006512199A (ja) 2006-04-13
US7001580B2 (en) 2006-02-21
AU2003294253A1 (en) 2004-07-29
ATE357967T1 (de) 2007-04-15
US20040127612A1 (en) 2004-07-01
CN100377771C (zh) 2008-04-02

Similar Documents

Publication Publication Date Title
JP4567465B2 (ja) 表面改質された有機分子を含有するエマルジョン
CA1305818C (en) Cross-linked organopolysiloxanes and emulsions based thereon
JP2632532B2 (ja) ペルフルオルポリエーテルを含む３種の不混和性液体を基とするミクロエマルション
US5136068A (en) Cross-linked organopolysiloxanes and emulsions based thereon
JP5750233B2 (ja) グリセリン変性有機ポリシロキサンを含む乳化剤
CN101716475B (zh) 一种反相破乳剂及其制备方法
RU2141996C1 (ru) Многофазная эмульсия и способ ее приготовления
JPS58500066A (ja) ポリジオルガノシロキサンを含むさく井用逆相エマルシヨンとその製法
CN1610717A (zh) 包含水包硅油乳液、盐、醇和溶剂的组合物
JPH0284B2 (enExample)
CN105536640A (zh) 一种以温度为触发机制的开关性表面活性颗粒
CN108070368B (zh) 一种自乳化乳状液及其制备方法
RU2126082C1 (ru) Состав и способ приготовления обратных эмульсий для добычи нефти
Schwab et al. Triglyceride/aqueous ethanol/1-butanol microemulsions
CN109575280A (zh) 利用双亲性超支化聚酰胺胺对水包油型乳状液进行破乳的方法
Liu et al. The emulsions stabilized by Dodecylbenzenesulfonic acid/asphaltene/hydrolyzed polyacrylamide: Emulsion morphology, stability, and rheology
JP4178397B2 (ja) 混合ベシクル、これを用いたエマルション、及びこれらの調製方法
Ma et al. Dual CO2 responsiveness of an oil-in-water emulsion by using sodium oleate and water-soluble tertiary amines
US20040171699A1 (en) Aqueous suspension of cross-linked silicone particles and aqueous emulsion of oil containing cross-linked silicone particles
JP5881042B2 (ja) 乳化物製造用親水性ナノ粒子の製造方法
Liu et al. Impact of nanoparticle movement on oil mobilization: Particles adsorbed at the oil–water interface versus particles dispersed in bulk fluid
JP4194270B2 (ja) 架橋シリコーン粒子の水系サスペンジョンおよび架橋シリコーン粒子を含有するシリコーンオイルの水系エマルジョン
JP3024957B2 (ja) ゲル化した化粧用スティックのための有用な組成物
Ezzat et al. Facile preparation of multi-functionalized zwitterionic surfactants for the separation of water in Arabian heavy crude oil emulsions
JP3100246B2 (ja) 泡抑制剤組成物

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20061113

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20061113

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20091201

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20100301

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20100308

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20100601

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20100706

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20100805

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130813

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees