JP4150252B2 - 吸水性樹脂の製造方法 - Google Patents
吸水性樹脂の製造方法 Download PDFInfo
- Publication number
- JP4150252B2 JP4150252B2 JP2002366968A JP2002366968A JP4150252B2 JP 4150252 B2 JP4150252 B2 JP 4150252B2 JP 2002366968 A JP2002366968 A JP 2002366968A JP 2002366968 A JP2002366968 A JP 2002366968A JP 4150252 B2 JP4150252 B2 JP 4150252B2
- Authority
- JP
- Japan
- Prior art keywords
- water
- polymerization
- mass
- aqueous solution
- unsaturated monomer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/04—Polymerisation in solution
- C08F2/10—Aqueous solvent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
- C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
- C08F20/04—Acids, Metal salts or ammonium salts thereof
- C08F20/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/60—Liquid-swellable gel-forming materials, e.g. super-absorbents
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Polymers & Plastics (AREA)
- Medicinal Chemistry (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hematology (AREA)
- Dispersion Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Absorbent Articles And Supports Therefor (AREA)
- Orthopedics, Nursing, And Contraception (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002366968A JP4150252B2 (ja) | 2001-12-19 | 2002-12-18 | 吸水性樹脂の製造方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001-385730 | 2001-12-19 | ||
| JP2001385730 | 2001-12-19 | ||
| JP2002366968A JP4150252B2 (ja) | 2001-12-19 | 2002-12-18 | 吸水性樹脂の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2003246812A JP2003246812A (ja) | 2003-09-05 |
| JP2003246812A5 JP2003246812A5 (OSRAM) | 2005-10-27 |
| JP4150252B2 true JP4150252B2 (ja) | 2008-09-17 |
Family
ID=19187867
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2002366968A Expired - Fee Related JP4150252B2 (ja) | 2001-12-19 | 2002-12-18 | 吸水性樹脂の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US7009010B2 (OSRAM) |
| EP (1) | EP1456258B1 (OSRAM) |
| JP (1) | JP4150252B2 (OSRAM) |
| KR (1) | KR100504592B1 (OSRAM) |
| CN (1) | CN1235922C (OSRAM) |
| DE (1) | DE60231834D1 (OSRAM) |
| SA (1) | SA03230502B1 (OSRAM) |
| WO (1) | WO2003051939A1 (OSRAM) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6927268B2 (en) * | 2000-06-21 | 2005-08-09 | Nippon Shokubai Co., Ltd. | Production process for water-absorbent resin |
| WO2005097313A1 (en) | 2004-03-31 | 2005-10-20 | Nippon Shokubai Co., Ltd. | An aqueous-liquid-absorbing agent and its production process |
| DE102004019264B4 (de) | 2004-04-21 | 2008-04-10 | Stockhausen Gmbh | Verfahren zur Herstellung eines absorbierenden Polymers mittels Spreittrocknung |
| DE102004028002A1 (de) * | 2004-06-09 | 2006-01-05 | Stockhausen Gmbh | Verfahren zur Herstellung von hydrophilen Polymeren unter Verwendung eines rechnererzeugten Modells |
| DE102004057874A1 (de) | 2004-11-30 | 2006-06-01 | Basf Ag | Verfahren zur Nachvernetzung wasserabsorbierender Polymerpartikel |
| JP5084513B2 (ja) * | 2004-12-10 | 2012-11-28 | 株式会社日本触媒 | 改質された吸水性樹脂の製造方法 |
| TWI353360B (en) * | 2005-04-07 | 2011-12-01 | Nippon Catalytic Chem Ind | Production process of polyacrylic acid (salt) wate |
| CN101155840B (zh) * | 2005-04-07 | 2011-06-15 | 株式会社日本触媒 | 聚丙烯酸(盐)吸水树脂的生产方法 |
| DE602006012640D1 (de) * | 2005-04-12 | 2010-04-15 | Nippon Catalytic Chem Ind | Altend wasserabsorbierendes harz auf basis von polyacrylsäure (polyacrylat) als hauptkomponente, herstellungsverfahren dafür, wasserabsorbierender kerige wasserabsorbierende mittel verwendet wird |
| US20060266941A1 (en) * | 2005-05-26 | 2006-11-30 | Vestal Marvin L | Method and apparatus for interfacing separations techniques to MALDI-TOF mass spectrometry |
| DE102005042608A1 (de) † | 2005-09-07 | 2007-03-08 | Basf Ag | Polymerisationsverfahren |
| US20070066716A1 (en) * | 2005-09-19 | 2007-03-22 | Craig Daniel H | Nonpolar thermoplastic compositions including inorganic particulates |
| US20070066715A1 (en) * | 2005-09-19 | 2007-03-22 | Craig Daniel H | Process for manufacturing nonpolar thermoplastic materials containing inorganic particulates |
| TWI394789B (zh) | 2005-12-22 | 2013-05-01 | Nippon Catalytic Chem Ind | 吸水性樹脂組成物及其製造方法、吸收性物品 |
| EP1837348B9 (en) | 2006-03-24 | 2020-01-08 | Nippon Shokubai Co.,Ltd. | Water-absorbing resin and method for manufacturing the same |
| US8383746B2 (en) * | 2006-03-27 | 2013-02-26 | Nippon Shokubai Co., Ltd | Water absorbing resin with improved internal structure and manufacturing method therefor |
| JP5378790B2 (ja) | 2006-04-27 | 2013-12-25 | 住友精化株式会社 | 吸水性樹脂の製造方法 |
| BRPI0815730B1 (pt) * | 2007-08-23 | 2020-10-20 | Sumitomo Seika Chemicals Co., Ltd. | método para a produção de uma resina absorvente de água |
| JP5502762B2 (ja) * | 2008-03-05 | 2014-05-28 | ビーエーエスエフ ソシエタス・ヨーロピア | 超吸収材の製造方法 |
| US7916989B2 (en) | 2008-07-31 | 2011-03-29 | Corning Cable Systems Llc | Optical fiber assemblies having a powder or powder blend at least partially mechanically attached |
| EP2318872B1 (en) | 2008-08-15 | 2013-03-20 | Corning Cable Systems LLC | Optical fiber assemblies, and methods and apparatus for the manufacture thereof |
| EP2471846B1 (en) * | 2009-08-27 | 2016-12-21 | Nippon Shokubai Co., Ltd. | Polyacrylic acid (salt) water absorbent resin and method for producing same |
| CN102548654A (zh) | 2009-09-29 | 2012-07-04 | 株式会社日本触媒 | 颗粒状吸水剂及其制造方法 |
| US10294315B2 (en) | 2009-09-30 | 2019-05-21 | Nippon Shokubai Co., Ltd. | Polyacrylic acid (salt)-based water absorbent resin and method for producing same |
| US8507620B2 (en) * | 2010-06-08 | 2013-08-13 | Lg Display Co., Ltd. | Process for preparing water absorbent resin with high performance |
| US8883944B2 (en) | 2010-07-28 | 2014-11-11 | Sumitomo Seika Chemicals Co., Ltd. | Method for producing a water-absorbent resin |
| WO2012014749A1 (ja) | 2010-07-28 | 2012-02-02 | 住友精化株式会社 | 吸水性樹脂の製造方法 |
| US8859700B2 (en) | 2010-07-28 | 2014-10-14 | Sumitomo Seika Chemicals Co., Ltd. | Method for producing a water-absorbent resin |
| JP5777620B2 (ja) * | 2010-07-28 | 2015-09-09 | 住友精化株式会社 | 吸水性樹脂の製造方法 |
| JP5784286B2 (ja) * | 2010-07-30 | 2015-09-24 | 株式会社日本触媒 | ポリアクリル酸(塩)系吸水性樹脂およびその製造方法 |
| KR101290740B1 (ko) | 2010-11-22 | 2013-07-29 | 주식회사 엘지화학 | 고흡수성 수지의 제조 방법 |
| BR112013032972A2 (pt) | 2011-06-24 | 2017-01-31 | Sumitomo Seika Chemicals | método para a produção de uma resina absorvente de água |
| WO2013073614A1 (ja) * | 2011-11-15 | 2013-05-23 | 株式会社日本触媒 | 吸水剤組成物及びその製造方法、並びにその保管及び在庫方法 |
| CN103450388B (zh) * | 2013-09-12 | 2016-04-20 | 浙江卫星石化股份有限公司 | 一种吸收快的高吸水性树脂的制备方法 |
| JP5719079B1 (ja) * | 2014-07-11 | 2015-05-13 | 住友精化株式会社 | 吸水性樹脂及び吸収性物品 |
| EP3412710B1 (en) | 2016-12-23 | 2021-11-10 | LG Chem, Ltd. | Method for producing porous superabsorbent polymer |
| KR102112833B1 (ko) | 2016-12-26 | 2020-05-19 | 주식회사 엘지화학 | 다공성 고흡수성 수지의 제조 방법 |
| CN114096606A (zh) | 2019-07-05 | 2022-02-25 | 住友精化株式会社 | 交联聚合物凝胶及其制造方法、单体组合物以及交联聚合物颗粒的制造方法 |
| CN114805662B (zh) * | 2022-04-20 | 2023-07-14 | 山东昊月新材料股份有限公司 | 一种具有原位抗菌性能的高吸收树脂及其合成方法 |
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|---|---|---|---|---|
| JPS5346389A (en) | 1976-10-07 | 1978-04-25 | Kao Corp | Preparation of self-crosslinking polymer of acrylic alkali metal salt |
| GB2088392B (en) | 1980-12-03 | 1984-05-02 | Sumitomo Chemical Co | Production of hydrogels |
| JPS57158209A (en) | 1981-03-25 | 1982-09-30 | Kao Corp | Production of bead-form highly water-absorbing polymer |
| US4625001A (en) | 1984-09-25 | 1986-11-25 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Method for continuous production of cross-linked polymer |
| JPS6187702A (ja) | 1984-10-05 | 1986-05-06 | Seitetsu Kagaku Co Ltd | 吸水性樹脂の製造方法 |
| DE3537276A1 (de) | 1985-10-19 | 1987-04-23 | Basf Ag | Verfahren zur kontinuierlichen herstellung von vernetzten feinteiligen gelfoermigen polymerisaten |
| DE3544770A1 (de) | 1985-12-18 | 1987-06-19 | Stockhausen Chem Fab Gmbh | Verfahren und vorrichtung zum kontinuierlichen herstellen von polymerisaten und copolymerisaten der acrylsaeure und/oder methacrylsaeure |
| DE3609545A1 (de) | 1986-03-21 | 1987-09-24 | Basf Ag | Verfahren zur diskontinuierlichen herstellung von vernetzten, feinteiligen polymerisaten |
| DE3872978T2 (de) | 1987-08-10 | 1993-06-09 | Nippon Catalytic Chem Ind | Verfahren zur herstellung eines wasserabsorbierenden harzes. |
| CA1333439C (en) | 1988-05-23 | 1994-12-06 | Akito Yano | Method for production of hydrophilic polymer |
| US5244735A (en) | 1988-06-28 | 1993-09-14 | Nippon Shokubai Kagaku Kabushiki Kaisha | Water-absorbent resin and production process |
| TW201758B (OSRAM) | 1988-06-28 | 1993-03-11 | Catalyst co ltd | |
| DE3843780A1 (de) | 1988-12-24 | 1990-07-05 | Basf Ag | Verfahren zur herstellung von feinteiligen, gelfoermigen, wasserquellbaren copolymerisaten |
| JPH07119246B2 (ja) | 1989-06-29 | 1995-12-20 | 東亞合成株式会社 | 吸水性樹脂の製造方法 |
| US5140076A (en) | 1990-04-02 | 1992-08-18 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Method of treating the surface of an absorbent resin |
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| JP2966539B2 (ja) | 1991-02-07 | 1999-10-25 | 株式会社日本触媒 | 含水ゲル状重合体の製造方法 |
| US5250640A (en) | 1991-04-10 | 1993-10-05 | Nippon Shokubai Co., Ltd. | Method for production of particulate hydrogel polymer and absorbent resin |
| GB9107952D0 (en) | 1991-04-15 | 1991-05-29 | Dow Rheinmuenster | Surface crosslinked and surfactant coated absorbent resin particles and method of preparation |
| DE69323652T2 (de) | 1992-06-10 | 1999-09-09 | Nippon Shokubai Co. Ltd. | Verfahren zur Herstellung eines hydrophilen Harzes |
| JPH06107800A (ja) | 1992-10-01 | 1994-04-19 | Nippon Shokubai Co Ltd | 粒子状含水ゲル状重合体および吸水性樹脂の製造方法 |
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| JP2675729B2 (ja) | 1992-12-16 | 1997-11-12 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| DE4244548C2 (de) | 1992-12-30 | 1997-10-02 | Stockhausen Chem Fab Gmbh | Pulverförmige, unter Belastung wäßrige Flüssigkeiten sowie Blut absorbierende Polymere, Verfahren zu ihrer Herstellung und ihre Verwendung in textilen Konstruktionen für die Körperhygiene |
| JP2995276B2 (ja) | 1993-01-18 | 1999-12-27 | 三洋化成工業株式会社 | 吸水性樹脂の製造法 |
| JP3659507B2 (ja) * | 1993-09-13 | 2005-06-15 | 月島機械株式会社 | アクリル酸の精製方法 |
| US5451613A (en) | 1993-09-17 | 1995-09-19 | Nalco Chemical Company | Superabsorbent polymer having improved absorption rate and absorption under pressure |
| DE4333056C2 (de) | 1993-09-29 | 1998-07-02 | Stockhausen Chem Fab Gmbh | Pulverförmige, wäßrige Flüssigkeiten absorbierende Polymere, Verfahren zu ihrer Herstellung und ihre Verwendung als Absorptionsmittel |
| JPH07224204A (ja) | 1994-02-10 | 1995-08-22 | Toagosei Co Ltd | 吸水性樹脂の製造方法 |
| US5610208A (en) | 1994-02-17 | 1997-03-11 | Nippon Shokubai Co., Ltd. | Water-absorbent agent, method for production thereof, and water-absorbent composition |
| JPH09509591A (ja) | 1994-02-17 | 1997-09-30 | ザ、プロクター、エンド、ギャンブル、カンパニー | 改良された吸収特性を有する吸収性材料およびその製造方法 |
| JPH07242709A (ja) | 1994-03-03 | 1995-09-19 | Toagosei Co Ltd | 吸水性樹脂の製造方法 |
| EP0755413A4 (en) | 1994-04-11 | 1999-11-17 | Hoechst Celanese Corp | SUPER ABSORBENT POLYMERS AND PRODUCTS MANUFACTURED WITH THEM |
| US5759358A (en) * | 1994-05-31 | 1998-06-02 | Rohm And Haas Company | Process for pure grade acrylic acid |
| WO1997024394A1 (fr) | 1995-12-27 | 1997-07-10 | Nippon Shokubai Co., Ltd. | Produit absorbant l'eau, procede et appareil de fabrication |
| US6139742A (en) * | 1996-10-31 | 2000-10-31 | University Of Kentucky Research Foundation | Membrane-based sorbent for heavy metal sequestration |
| US6174975B1 (en) * | 1998-01-13 | 2001-01-16 | E.I. Du Pont De Nemours And Company | Polymerization of olefins |
| US6228930B1 (en) | 1997-06-18 | 2001-05-08 | Nippon Shokubai Co., Ltd. | Water-absorbent resin granule-containing composition and production process for water-absorbent resin granule |
| JPH1171529A (ja) | 1997-07-03 | 1999-03-16 | Nippon Shokubai Co Ltd | 吸水性樹脂及びそれを用いた吸水性物品 |
| TW473485B (en) | 1997-12-10 | 2002-01-21 | Nippon Catalytic Chem Ind | The production process of a water-absorbent resin |
| US6254990B1 (en) | 1998-02-18 | 2001-07-03 | Nippon Shokubai Co., Ltd. | Surface-crosslinking process for water-absorbent resin |
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| US6503979B1 (en) | 1998-02-26 | 2003-01-07 | Basf Aktiengesellschaft | Method for cross-linking hydrogels with bis- and poly-2-oxazolidinones |
| US6444744B1 (en) | 1998-03-11 | 2002-09-03 | Nippon Shokubai Co., Ltd. | Hydrophilic resin, absorbent article, and acrylic acid for polymerization |
| JP4141526B2 (ja) | 1998-04-07 | 2008-08-27 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| US6241928B1 (en) | 1998-04-28 | 2001-06-05 | Nippon Shokubai Co., Ltd. | Method for production of shaped hydrogel of absorbent resin |
| DE19849499A1 (de) | 1998-10-27 | 2000-05-04 | Basf Ag | Verfahren zur vollständigen Trocknung von Hydrogelen |
| DE19955861A1 (de) | 1999-11-20 | 2001-05-23 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von vernetzten feinteiligen gelförmigen Polymerisaten |
| US6927268B2 (en) | 2000-06-21 | 2005-08-09 | Nippon Shokubai Co., Ltd. | Production process for water-absorbent resin |
| US6906159B2 (en) | 2000-08-03 | 2005-06-14 | Nippon Shokubai Co., Ltd. | Water-absorbent resin, hydropolymer, process for producing them, and uses of them |
| JP4805490B2 (ja) | 2000-08-03 | 2011-11-02 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| US6794473B2 (en) | 2001-05-01 | 2004-09-21 | Nippon Shokubai Co., Ltd. | Acrylic acid (salt) polymer, its production process and uses |
-
2002
- 2002-12-17 KR KR10-2003-7010825A patent/KR100504592B1/ko not_active Expired - Fee Related
- 2002-12-17 US US10/472,038 patent/US7009010B2/en not_active Expired - Fee Related
- 2002-12-17 DE DE60231834T patent/DE60231834D1/de not_active Expired - Lifetime
- 2002-12-17 WO PCT/JP2002/013160 patent/WO2003051939A1/en not_active Ceased
- 2002-12-17 CN CNB028055144A patent/CN1235922C/zh not_active Expired - Fee Related
- 2002-12-17 EP EP02786104A patent/EP1456258B1/en not_active Expired - Lifetime
- 2002-12-18 JP JP2002366968A patent/JP4150252B2/ja not_active Expired - Fee Related
-
2003
- 2003-01-06 SA SA03230502A patent/SA03230502B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| KR100504592B1 (ko) | 2005-08-03 |
| JP2003246812A (ja) | 2003-09-05 |
| CN1492884A (zh) | 2004-04-28 |
| KR20030078925A (ko) | 2003-10-08 |
| SA03230502B1 (ar) | 2007-02-27 |
| DE60231834D1 (de) | 2009-05-14 |
| CN1235922C (zh) | 2006-01-11 |
| EP1456258B1 (en) | 2009-04-01 |
| US7009010B2 (en) | 2006-03-07 |
| EP1456258A1 (en) | 2004-09-15 |
| US20040110913A1 (en) | 2004-06-10 |
| WO2003051939A1 (en) | 2003-06-26 |
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