JP2019504840A - ハロゲン置換ジケトン、ピラゾール化合物およびピラゾール化合物の製造方法 - Google Patents

ハロゲン置換ジケトン、ピラゾール化合物およびピラゾール化合物の製造方法 Download PDF

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JP2019504840A
JP2019504840A JP2018539274A JP2018539274A JP2019504840A JP 2019504840 A JP2019504840 A JP 2019504840A JP 2018539274 A JP2018539274 A JP 2018539274A JP 2018539274 A JP2018539274 A JP 2018539274A JP 2019504840 A JP2019504840 A JP 2019504840A
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formula
group
alkyl
vii
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JP2019504840A5 (OSRAM
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スザンネ ヴァスマン，
スザンネ ヴァスマン，
ジャニス ファンゼムス，
ジャニス ファンゼムス，
シュテファン ムロス，
シュテファン ムロス，
ジャン ファーブル，
ジャン ファーブル，
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ソルヴェイ（ソシエテ アノニム）
ソルヴェイ（ソシエテ アノニム）
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Publication of JP2019504840A publication Critical patent/JP2019504840A/ja
Publication of JP2019504840A5 publication Critical patent/JP2019504840A5/ja
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18—One oxygen or sulfur atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C225/00—Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones
    • C07C225/02—Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones having amino groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C225/14—Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones having amino groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being unsaturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/12—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
JP2018539274A 2016-01-28 2017-01-27 ハロゲン置換ジケトン、ピラゾール化合物およびピラゾール化合物の製造方法 Pending JP2019504840A (ja)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
EP16153112.4 2016-01-28
EP16153112 2016-01-28
EP16162487 2016-03-25
EP16162487.9 2016-03-25
EP16196175.0 2016-10-28
EP16196175 2016-10-28
PCT/EP2017/051797 WO2017129759A1 (en) 2016-01-28 2017-01-27 Halogen substituted diketones, pyrazole compounds and processes for the manufacture of pyrazole compounds

Publications (2)

Publication Number Publication Date
JP2019504840A true JP2019504840A (ja) 2019-02-21
JP2019504840A5 JP2019504840A5 (OSRAM) 2020-02-13

Family

ID=57960426

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JP2018539274A Pending JP2019504840A (ja) 2016-01-28 2017-01-27 ハロゲン置換ジケトン、ピラゾール化合物およびピラゾール化合物の製造方法

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US (2) US10829456B2 (OSRAM)
EP (1) EP3408259A1 (OSRAM)
JP (1) JP2019504840A (OSRAM)
KR (1) KR20180108695A (OSRAM)
CN (1) CN108884051A (OSRAM)
WO (1) WO2017129759A1 (OSRAM)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2019524765A (ja) * 2016-08-02 2019-09-05 ソルヴェイ（ソシエテ アノニム） ピラゾールカルボン酸および誘導体の製造に有用なヒドラジニル化合物の製造、ヒドラジニル化合物ならびにその使用

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105541716B (zh) 2015-03-26 2024-02-23 Ａｇｃ株式会社 吡唑衍生物的制造方法
CN110461822A (zh) * 2017-03-27 2019-11-15 Ａｇｃ株式会社 含卤素吡唑羧酸及其中间体的制造方法
US20200407304A1 (en) 2017-09-04 2020-12-31 Solvay Sa Process and intermediate for the manufacture of difluoroacetyl chloride
CN107987021A (zh) * 2017-11-24 2018-05-04 上海应用技术大学 一种3-二氟甲基-1-甲基-1h-吡唑-4-羧酸的制备方法
EP3495351A1 (en) * 2017-12-08 2019-06-12 Solvay Sa Oxidation of a pyrazolyl ketone compound to the corresponding carboxylic acid
WO2019122164A1 (en) 2017-12-22 2019-06-27 Solvay Sa Process for the manufacture of pyrazole carboxylic derivatives and precursors thereof
CN111587241A (zh) * 2017-12-22 2020-08-25 索尔维公司 亚胺鎓化合物的制造方法及其在制造吡唑衍生物中的应用
WO2019122204A1 (en) 2017-12-22 2019-06-27 Solvay Sa Process for the manufacture of pyrazole compounds
CN110526810A (zh) * 2018-05-25 2019-12-03 浙江蓝天环保高科技股份有限公司 一种1,1,1-三氟-4-乙氧基戊-3-烯-2-酮的制备方法
EP3605699A1 (en) 2018-07-31 2020-02-05 Solvay Sa New components for electrolyte compositions

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0632784A (ja) * 1992-05-15 1994-02-08 Hoechst Ag ４−アルキル−置換ピリミジン−５−カルボキシアニリド、それらの製造方法、それらを含有する組成物およびそれらの殺菌剤としての用途
JP2006273844A (ja) * 2005-02-17 2006-10-12 Shionogi & Co Ltd 新規ベンゾジアゼピン類
JP2006525355A (ja) * 2003-05-01 2006-11-09 アボット・ラボラトリーズ ナトリウムチャンネルモジュレーターとしてのピラゾール−アミドおよびスルホンアミド

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4342601A1 (de) 1993-08-13 1995-02-16 Solvay Fluor & Derivate Verfahren zur Herstellung von Poly- und Perfluorcarbonsäurechloriden
ES2119952T3 (es) 1993-12-23 1998-10-16 Solvay Fluor & Derivate Procedimiento para la preparacion de cloruros de acidos polifluoroclorocarboxilicos y perfluorocarboxilicos bajo adicion de cloro.
JP3632243B2 (ja) 1994-07-28 2005-03-23 旭硝子株式会社 ジフルオロ酢酸フルオリドおよびジフルオロ酢酸エステルの製造方法
US5905169A (en) 1995-03-20 1999-05-18 E. I. Du Pont De Nemours And Company Process for producing polyfluoroacyl compositions
US6248923B1 (en) 1999-09-03 2001-06-19 Eastman Chemical Company Process for the production of fluorocarboxylic acid anhydrides
DE10215292A1 (de) 2002-02-19 2003-08-28 Bayer Cropscience Ag Disubstitutierte Pyrazolylcarbocanilide
GB0224316D0 (en) 2002-10-18 2002-11-27 Syngenta Participations Ag Chemical compounds
US20040220170A1 (en) * 2003-05-01 2004-11-04 Atkinson Robert N. Pyrazole-amides and sulfonamides as sodium channel modulators
DE10325715A1 (de) 2003-06-06 2004-12-23 Solvay Fluor Und Derivate Gmbh Vereinfachte Herstellung von Alkenonen
GB0418048D0 (en) 2004-08-12 2004-09-15 Syngenta Participations Ag Method for protecting useful plants or plant propagation material
DE102005007160A1 (de) 2005-02-16 2006-08-24 Basf Ag Pyrazolcarbonsäureanilide, Verfahren zu ihrer Herstellung und sie enthaltende Mittel zur Bekämpfung von Schadpilzen
CN101223144A (zh) 2005-07-18 2008-07-16 先正达参股股份有限公司 作为杀微生物剂的吡唑-4-羧酰胺衍生物
EP2253622A1 (en) 2005-09-16 2010-11-24 Syngenta Participations AG. Process for the production of amides
BRPI0617739B1 (pt) 2005-10-25 2017-11-21 Syngenta Participations Ag Heterocyclic amide derivatives useful as microbiocides, composition comprising them and method of controlling or preventing infestation of useful plants by phytopathogenic microorganisms
CA2690460A1 (en) 2007-06-15 2008-12-18 Markus Nett Method for producing difluoromethyl-substituted pyrazole compounds
CN101801906A (zh) 2007-08-16 2010-08-11 索尔维公司 制备4-氟取代的3-氧代-烷酸酯的方法
BRPI0911897A2 (pt) 2008-05-02 2015-07-28 Basf Se Processo para a preparação de compostos, e, composto
KR101652539B1 (ko) 2008-07-04 2016-08-30 솔베이(소시에떼아노님) 알케논의 제조 방법
JP2010030970A (ja) 2008-07-31 2010-02-12 Bayer Cropscience Ag 殺虫性ベンゼンジカルボキサミド誘導体
EP2184273A1 (de) 2008-11-05 2010-05-12 Bayer CropScience AG Halogen-substituierte Verbindungen als Pestizide
EP2595962B1 (en) 2010-07-23 2018-07-11 Solvay Sa Process for the preparation of esters of 1-substituted-3-fluoroalkyl-pyrazole-4-carboxylic acids
WO2012055864A1 (en) 2010-10-27 2012-05-03 Solvay Sa Process for the preparation of pyrazole-4-carboxamides
PL2810931T3 (pl) 2013-06-06 2018-09-28 Solvay Sa Sposób otrzymywania halogenowanych bezwodników kwasów karboksylowych
ITMI20132201A1 (it) 2013-12-23 2015-06-24 Isagro Spa Processo per la sintesi regioselettiva di pirazoli

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0632784A (ja) * 1992-05-15 1994-02-08 Hoechst Ag ４−アルキル−置換ピリミジン−５−カルボキシアニリド、それらの製造方法、それらを含有する組成物およびそれらの殺菌剤としての用途
JP2006525355A (ja) * 2003-05-01 2006-11-09 アボット・ラボラトリーズ ナトリウムチャンネルモジュレーターとしてのピラゾール−アミドおよびスルホンアミド
JP2006273844A (ja) * 2005-02-17 2006-10-12 Shionogi & Co Ltd 新規ベンゾジアゼピン類

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
ETSUJI OKADA: "FACILE SYNTHETIC METHODS FOR 3- AND 5-TRIFLUOROMETHYL- 4-TRIFLUOROACETYL-PYRAZOLES 以下備考", HETEROCYCLES, vol. VOL:34, NR:4, JPN5019001050, 1992, JP, pages 791 - 798, ISSN: 0004563923 *
FERNANDA A ROSA: "N- AND C-ACYLATION IN β-ENAMINO KETONES: STRUCTURAL EFFECTS ON REGIOCONTROL", SYNLETT, vol. NR:20, JPN5019001055, 4 September 2007 (2007-09-04), pages 3165 - 3171, ISSN: 0004563922 *
MUSTAPHA SOUFYANE: "SYNTHESIS OF SOME FLUORINATED NITROGEN HETEROCYCLES FROM 以下備考", TETRAHEDRON LETTERS, vol. VOL:34, NR:48, JPN5019001052, 10 January 1993 (1993-01-10), pages 7737 - 7740, ISSN: 0004563924 *
OTA NORIO: "A CONVENIENT SYNTHESIS OF FLUORINE-CONTAINING DIHYDROBENZO(B)(1,4) DIAZEPINOLS AND ITS 以下備考", HETEROCYCLES, vol. VOL:76, NR:2, JPN5019001054, 2008, pages 1205 - 1217, ISSN: 0004563921 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2019524765A (ja) * 2016-08-02 2019-09-05 ソルヴェイ（ソシエテ アノニム） ピラゾールカルボン酸および誘導体の製造に有用なヒドラジニル化合物の製造、ヒドラジニル化合物ならびにその使用

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Publication number Publication date
US10829456B2 (en) 2020-11-10
EP3408259A1 (en) 2018-12-05
CN108884051A (zh) 2018-11-23
US20210040043A1 (en) 2021-02-11
WO2017129759A1 (en) 2017-08-03
US20190031616A1 (en) 2019-01-31
KR20180108695A (ko) 2018-10-04

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