JP2019025842A - 樹脂金属複合体、樹脂金属複合体の製造方法、及び、樹脂金属複合体の解体方法 - Google Patents
樹脂金属複合体、樹脂金属複合体の製造方法、及び、樹脂金属複合体の解体方法 Download PDFInfo
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- JP2019025842A JP2019025842A JP2017149424A JP2017149424A JP2019025842A JP 2019025842 A JP2019025842 A JP 2019025842A JP 2017149424 A JP2017149424 A JP 2017149424A JP 2017149424 A JP2017149424 A JP 2017149424A JP 2019025842 A JP2019025842 A JP 2019025842A
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- B29C66/7392—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of at least one of the parts being a thermoplastic
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B29C66/73—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset
- B29C66/739—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset
- B29C66/7394—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material characterised by the intensive physical properties of the material of the parts to be joined, by the optical properties of the material of the parts to be joined, by the extensive physical properties of the parts to be joined, by the state of the material of the parts to be joined or by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of the parts to be joined being a thermoplastic or a thermoset characterised by the material of at least one of the parts being a thermoset
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/74—Joining plastics material to non-plastics material
- B29C66/742—Joining plastics material to non-plastics material to metals or their alloys
- B29C66/7422—Aluminium or alloys of aluminium
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/70—General aspects of processes or apparatus for joining preformed parts characterised by the composition, physical properties or the structure of the material of the parts to be joined; Joining with non-plastics material
- B29C66/74—Joining plastics material to non-plastics material
- B29C66/742—Joining plastics material to non-plastics material to metals or their alloys
- B29C66/7428—Transition metals or their alloys
- B29C66/74283—Iron or alloys of iron, e.g. steel
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/12—Bonding of a preformed macromolecular material to the same or other solid material such as metal, glass, leather, e.g. using adhesives
- C08J5/121—Bonding of a preformed macromolecular material to the same or other solid material such as metal, glass, leather, e.g. using adhesives by heating
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- C09J5/00—Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers
- C09J5/06—Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers involving heating of the applied adhesive
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- C09J2301/50—Additional features of adhesives in the form of films or foils characterized by process specific features
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Abstract
Description
特許第5749354号公報の実施例1に記載の方法に沿って樹脂組成物(樹脂部材)を作製した。具体的には、まず、10.7gのDER332エポキシ樹脂(ダウケミカル社製)と、0.81gの亜鉛(II)アセチルアセトネートとをビーカに入れた。さらに、3.5gの無水グルタル酸を加え、ビーカを恒温槽に入れ加熱し、これらが完全に溶解するまで混合した。次いで、均一になった溶液をテトラフルオロエチレン製の型に流し込み、140℃で8時間加熱プレスし、樹脂部材として、平板状の樹脂組成物を作製した。そして、作製した樹脂部材をアルミ板(金属部材)と重ね合わせ、200℃で3時間加熱しながらプレスを行い、室温まで自然冷却することで、前記の図1に示す形状の樹脂金属複合体を得た。
まず、国際公開第2016/178345号の実施例1に記載の液状ワニスを作製した。具体的には、スチレン(東京化成社製、重合によりポリスチレンが得られる)3.0gと、ビスフェノールAグリセロラートジメタクリラート(アルドリッチ社製)3.0gと、2−ヒドロキシメタクリレート0.77gと、過酸化物重合開始剤CT50(日立化成社製)0.11gと、ナフテン酸亜鉛(II)(東京化成社製)0.32gとをガラス製のスクリュー瓶に入れた。そして、ミックスロータを用いてスクリュー瓶中の試薬を攪拌し、均一な液状ワニスを作製した。
前記の実施例2と同様の方法により、液状ワニスを作製した。作製した液状ワニスをテトラフルオロエチレン製のビーカに入れ、120℃の恒温槽中で4時間加熱することで硬化物を得た。硬化物をビーカから取り出し、乳鉢で十分に粉砕することで、粉体状の硬化物を得た。この硬化物は、前記の図6を参照しながら説明した接着層3に相当するものである。
エポキシ基を有するシランカップリング剤(3−グリシドキシプロピルトリメトキシラン)の0.5%水溶液にアルミニウム板を浸漬させ、空気中で乾燥させた。この操作により、アルミニウム板(金属部材)の表面に、前記の図7を参照しながら説明したカップリング剤4が配置されたことになる。次いで、このアルミニウム板と、前記の実施例2で作製した繊維強化樹脂(樹脂部材)とを重ね合わせ、前記の実施例2と同様にして樹脂金属複合体を得た。
前記の実施例2に記載の方法と同様の方法により、樹脂金属複合体を作製した。なお、この方法で作製された樹脂金属複合体の接合強度が強固であることは、前記の実施例2において確認されている。
Science、356、62−65ページの記載に従って、ポリメタクリル酸をジオキサボラン誘導体で架橋した樹脂部材を作製した。作製した樹脂部材とステンレス板(SUS304、金属部材)とを重ね合わせ、190℃で1時間加熱プレスし、樹脂金属複合体を得た。
比較例として、特許第5749354号公報の比較例1に記載の方法を一部変更した方法により樹脂組成物(樹脂部材)を作製した。ここで作製した樹脂組成物は、動的共有結合を有しないものである。まず、10.7gのDER332エポキシ樹脂(ダウケミカル社製)をビーカに入れた。さらに、3.5gの無水グルタル酸を加え、ビーカを恒温槽に入れ加熱し、これらが完全に溶解するまで混合した。次いで、均一になった溶液を使用して、前記の実施例1と同様にすることで、平板状の樹脂組成物(樹脂部材)、及び、前記の図1に示す形状の樹脂金属複合体を得た。
2 金属部材
3 接着層
4 カップリング剤
10 樹脂金属複合体
20 樹脂金属複合体
30 樹脂金属複合体
Claims (6)
- 金属部材と、
当該金属部材と接合しているとともに、前記金属部材の表面に存在する官能基に対し可逆的に解離及び結合可能な動的共有結合を有する樹脂部材と、を備えることを特徴とする、樹脂金属複合体。 - 前記樹脂部材は繊維を含むことを特徴とする、請求項1に記載の樹脂金属複合体。
- 前記金属部材と前記樹脂部材とは、接着層を介して接合していることを特徴とする、請求項1又は2に記載の樹脂金属複合体。
- 前記金属部材の表面には、前記樹脂部材が有する前記動的共有結合と結合可能なカップリング剤が配置され、
前記金属部材と前記樹脂部材とは、当該カップリング剤を介して接合していることを特徴とする、請求項1又は2に記載の樹脂金属複合体。 - 金属部材と、当該金属部材と接合しているとともに、当該金属部材の表面に存在する官能基に対し可逆的に解離及び結合可能な動的共有結合を有する樹脂部材と、を備える樹脂金属複合体を製造する方法であって、
前記金属部材と前記樹脂部材とを接触させた後、当該接触をしている部分を加熱することで、前記金属部材と前記樹脂部材とを接合させることを特徴とする、樹脂金属複合体の製造方法。 - 金属部材と、当該金属部材と接合しているとともに、当該金属部材の表面に存在する官能基に対し可逆的に解離及び結合可能な動的共有結合を有する樹脂部材と、を備える樹脂金属複合体を解体する方法であって、
前記金属部材と前記樹脂部材との接合部分を加熱し、前記金属部材と前記樹脂部材との接合を解くことで、前記金属部材と前記樹脂部材とを分離して前記樹脂金属複合体を解体することを特徴とする、樹脂金属複合体の解体方法。
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JP2017149424A JP6912316B2 (ja) | 2017-08-01 | 2017-08-01 | 樹脂金属複合体の解体方法 |
EP18841432.0A EP3663075A4 (en) | 2017-08-01 | 2018-03-20 | RESIN-METAL COMPOSITE, PROCESS FOR PREPARING A RESIN-METAL COMPOSITE AND PROCESS FOR DISMANTLING A RESIN-METAL COMPOSITE |
CN201880046040.6A CN110914043B (zh) | 2017-08-01 | 2018-03-20 | 树脂金属复合体、树脂金属复合体的制造方法以及树脂金属复合体的解体方法 |
PCT/JP2018/011226 WO2019026331A1 (ja) | 2017-08-01 | 2018-03-20 | 樹脂金属複合体、樹脂金属複合体の製造方法、及び、樹脂金属複合体の解体方法 |
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WO2022239463A1 (ja) * | 2021-05-11 | 2022-11-17 | 株式会社日立製作所 | 樹脂複合体、樹脂複合体の製造方法、及び樹脂複合体の解体方法 |
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WO2020183747A1 (ja) * | 2019-03-08 | 2020-09-17 | 睦月電機株式会社 | 合成樹脂成形体の製造方法及び金属樹脂接合体の製造方法 |
US11890788B2 (en) * | 2020-05-20 | 2024-02-06 | The Regents Of The University Of Michigan | Methods and process for producing polymer-metal hybrid components bonded by C—O-M bonds |
GB2606574A (en) * | 2021-05-14 | 2022-11-16 | Avalon Consultancy Services Ltd | Joining process and system |
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CN110914043B (zh) | 2022-03-15 |
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CN110914043A (zh) | 2020-03-24 |
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