JP2017110181A5 - - Google Patents
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- Publication number
- JP2017110181A5 JP2017110181A5 JP2016199310A JP2016199310A JP2017110181A5 JP 2017110181 A5 JP2017110181 A5 JP 2017110181A5 JP 2016199310 A JP2016199310 A JP 2016199310A JP 2016199310 A JP2016199310 A JP 2016199310A JP 2017110181 A5 JP2017110181 A5 JP 2017110181A5
- Authority
- JP
- Japan
- Prior art keywords
- tube
- acid
- flow reactor
- tubing
- monomer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 11
- 239000000178 monomer Substances 0.000 claims 9
- 239000002253 acid Substances 0.000 claims 7
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N N-phenyl amine Natural products NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 claims 5
- 239000000839 emulsion Substances 0.000 claims 5
- 150000003839 salts Chemical class 0.000 claims 5
- 238000006116 polymerization reaction Methods 0.000 claims 4
- YTPLMLYBLZKORZ-UHFFFAOYSA-N Thiophene Chemical compound C=1C=CSC=1 YTPLMLYBLZKORZ-UHFFFAOYSA-N 0.000 claims 2
- 239000003960 organic solvent Substances 0.000 claims 2
- 230000000379 polymerizing effect Effects 0.000 claims 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims 1
- 125000002490 anilino group Chemical group [H]N(*)C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 238000009792 diffusion process Methods 0.000 claims 1
- CJMZLCRLBNZJQR-UHFFFAOYSA-N ethyl 2-amino-4-(4-fluorophenyl)thiophene-3-carboxylate Chemical compound CCOC(=O)C1=C(N)SC=C1C1=CC=C(F)C=C1 CJMZLCRLBNZJQR-UHFFFAOYSA-N 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 229920002313 fluoropolymer Polymers 0.000 claims 1
- 239000004811 fluoropolymer Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 150000007524 organic acids Chemical class 0.000 claims 1
- 239000007800 oxidant agent Substances 0.000 claims 1
- 229920000172 poly(styrenesulfonic acid) Polymers 0.000 claims 1
- 229920000642 polymer Polymers 0.000 claims 1
- 229940005642 polystyrene sulfonic acid Drugs 0.000 claims 1
- 239000000376 reactant Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 229930192474 thiophene Natural products 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2021108462A JP7411608B2 (ja) | 2015-10-13 | 2021-06-30 | 重合体のフローリアクター合成 |
| JP2023023428A JP7627713B2 (ja) | 2015-10-13 | 2023-02-17 | 重合体のフローリアクター合成 |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/882,073 US9481764B1 (en) | 2015-10-13 | 2015-10-13 | Flow reactor synthesis of polymers |
| US14/882,073 | 2015-10-13 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2021108462A Division JP7411608B2 (ja) | 2015-10-13 | 2021-06-30 | 重合体のフローリアクター合成 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017110181A JP2017110181A (ja) | 2017-06-22 |
| JP2017110181A5 true JP2017110181A5 (https=) | 2019-11-14 |
| JP6953123B2 JP6953123B2 (ja) | 2021-10-27 |
Family
ID=57136683
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016199310A Active JP6953123B2 (ja) | 2015-10-13 | 2016-10-07 | 重合体のフローリアクター合成 |
| JP2021108462A Active JP7411608B2 (ja) | 2015-10-13 | 2021-06-30 | 重合体のフローリアクター合成 |
| JP2023023428A Active JP7627713B2 (ja) | 2015-10-13 | 2023-02-17 | 重合体のフローリアクター合成 |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2021108462A Active JP7411608B2 (ja) | 2015-10-13 | 2021-06-30 | 重合体のフローリアクター合成 |
| JP2023023428A Active JP7627713B2 (ja) | 2015-10-13 | 2023-02-17 | 重合体のフローリアクター合成 |
Country Status (7)
| Country | Link |
|---|---|
| US (7) | US9481764B1 (https=) |
| EP (3) | EP4039364A1 (https=) |
| JP (3) | JP6953123B2 (https=) |
| KR (1) | KR102666306B1 (https=) |
| CN (2) | CN106563400A (https=) |
| AU (2) | AU2016244187B2 (https=) |
| CA (1) | CA2944762C (https=) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9481764B1 (en) | 2015-10-13 | 2016-11-01 | The Boeing Company | Flow reactor synthesis of polymers |
| US10923723B1 (en) | 2017-05-11 | 2021-02-16 | Richard Carl Auchterlonie | Electro-conductive polymers of halogenated para-aminophenol, and electrochemical cells employing same |
| EP3662994A4 (en) * | 2017-07-31 | 2021-03-17 | Kaneka Corporation | FLOW REACTOR |
| CN112020529A (zh) * | 2017-12-12 | 2020-12-01 | 波音公司 | 制备传导聚合物的连续流动法 |
| CN108822250A (zh) * | 2018-09-03 | 2018-11-16 | 安徽联合辐化有限公司 | 水性高分子乳液的合成方法及设备 |
| CN109942733A (zh) * | 2018-10-26 | 2019-06-28 | 复旦大学 | 一种连续流动合成聚合物的方法 |
| EP4011290A1 (en) | 2018-12-10 | 2022-06-15 | Anastasia Rigas | Breath analyzer devices and breath test methods |
| US12150752B2 (en) | 2018-12-10 | 2024-11-26 | Anastasia Rigas | Hydrogen breath analyzer and breath test method |
| CN111434377B (zh) * | 2019-01-11 | 2022-07-15 | 中国石油化工股份有限公司 | 一种盘管微反应器和一种微反应器系统 |
| US11248089B2 (en) | 2019-04-10 | 2022-02-15 | The Boeing Company | Polyanilines and methods thereof |
| EP4335544A3 (en) | 2019-05-29 | 2024-06-12 | Saudi Arabian Oil Company | Flow synthesis of polymer nanoparticles |
| US11566165B2 (en) | 2019-05-30 | 2023-01-31 | Saudi Arabian Oil Company | Polymers and nanoparticles for flooding |
| JP7577657B2 (ja) * | 2019-07-03 | 2024-11-05 | 富士フイルム株式会社 | 最適化支援装置、方法およびプログラム |
| WO2021011755A1 (en) | 2019-07-16 | 2021-01-21 | Saudi Arabian Oil Company | Multipurpose microfluidics devices for rapid on-site optical chemical analysis |
| CN110918021A (zh) * | 2019-11-21 | 2020-03-27 | 南京先进生物材料与过程装备研究院有限公司 | 一种微反应装置及用其制备二甲苯甲醛树脂的方法 |
| CN110898774A (zh) * | 2019-11-27 | 2020-03-24 | 迪亚莱博（张家港）生物科技有限公司 | 胶乳颗粒的连续生产方法 |
| AU2021236038B2 (en) * | 2020-03-09 | 2026-01-22 | Kemira Oyj | Performic acid production systems and methods |
| US11773715B2 (en) | 2020-09-03 | 2023-10-03 | Saudi Arabian Oil Company | Injecting multiple tracer tag fluids into a wellbore |
| KR102376167B1 (ko) * | 2020-09-04 | 2022-03-17 | 인하대학교 산학협력단 | 연속흐름반응공정을 이용한 전도성 고분자의 제조방법 |
| US11987669B2 (en) | 2020-10-08 | 2024-05-21 | The Boeing Company | Polyaniline compositions, articles thereof, and methods thereof |
| US12043762B2 (en) | 2020-12-21 | 2024-07-23 | The Boeing Company | Compositions and methods thereof |
| US11660595B2 (en) | 2021-01-04 | 2023-05-30 | Saudi Arabian Oil Company | Microfluidic chip with multiple porosity regions for reservoir modeling |
| US11534759B2 (en) | 2021-01-22 | 2022-12-27 | Saudi Arabian Oil Company | Microfluidic chip with mixed porosities for reservoir modeling |
| CN113929881A (zh) * | 2021-11-08 | 2022-01-14 | 上海交通大学 | 一种基于连续流微反应器合成共轭光电高分子的制备方法 |
| US12253467B2 (en) | 2021-12-13 | 2025-03-18 | Saudi Arabian Oil Company | Determining partition coefficients of tracer analytes |
| US12000278B2 (en) | 2021-12-16 | 2024-06-04 | Saudi Arabian Oil Company | Determining oil and water production rates in multiple production zones from a single production well |
| CN115656159A (zh) * | 2022-10-12 | 2023-01-31 | 国家海洋局南海环境监测中心（中国海监南海区检验鉴定中心） | 一种酸可挥发性硫化物的在线流动反应非在线检测分析方法 |
| EP4735158A2 (en) * | 2023-06-29 | 2026-05-06 | Evonik Operations GmbH | Reactor, plant and process for synthesis of products by strongly exothermic reactions |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4877587A (en) * | 1984-08-24 | 1989-10-31 | Union Carbide Chemicals And Plastics Company Inc. | Fluidized bed polymerization reactors |
| US5324453A (en) | 1992-08-07 | 1994-06-28 | Neste Oy | Electrically conducting polyaniline: method for emulsion polymerization |
| US5567356A (en) | 1994-11-07 | 1996-10-22 | Monsanto Company | Emulsion-polymerization process and electrically-conductive polyaniline salts |
| EP1272546B1 (en) * | 2000-04-04 | 2006-08-02 | Panipol OY | A method and an apparatus for preparing polyaniline |
| FI113053B (fi) * | 2000-04-04 | 2004-02-27 | Panipol Oy | Menetelmä polyaniliinin valmistamiseksi |
| JP4177103B2 (ja) * | 2000-12-07 | 2008-11-05 | イーストマン ケミカル カンパニー | 管型反応器を使用する低コストポリエステルの製造方法 |
| DE10301874A1 (de) * | 2003-01-17 | 2004-07-29 | Celanese Emulsions Gmbh | Verfahren und Vorrichtung zur Herstellung von Emulsionspolymerisaten |
| EP1789178A1 (en) * | 2004-08-12 | 2007-05-30 | E.I.Du pont de nemours and company | Device and method of producing low molecular polymers |
| US7795359B2 (en) * | 2005-03-04 | 2010-09-14 | Novartis Ag | Continuous process for production of polymeric materials |
| DE102005055866A1 (de) * | 2005-11-23 | 2007-05-24 | Hte Ag The High Throughput Experimentation Company | Verfahren zur Herstellung von Aryl-Aryl gekoppelter Verbindungen |
| DE102006061967A1 (de) * | 2006-12-21 | 2008-06-26 | Bayer Technology Services Gmbh | Verfahren zur Darstellung von oligomeren Thiophenen |
| US7819967B2 (en) | 2007-11-08 | 2010-10-26 | Fujifilm Corporation | Method of producing an organic fine particle dispersion, organic fine particle dispersion obtained by the same, and ink-jet recording ink and paint using the dispersion |
| FR2928646B1 (fr) | 2008-03-13 | 2012-04-27 | Centre Nat Rech Scient | Procede de preparation de polyaniline et films hautement auto-orientes obtenus. |
| EP2133141A1 (en) * | 2008-06-10 | 2009-12-16 | Nederlandse Organisatie voor Toegepast-Natuuurwetenschappelijk Onderzoek TNO | Process for carrying out multi-phase reactions |
| WO2010059000A2 (ko) * | 2008-11-21 | 2010-05-27 | (주)Lg화학 | 고분자 입자의 제조 장치 및 제조 방법 |
| US9058916B2 (en) | 2009-02-17 | 2015-06-16 | Soken Chemical & Engineering Co., Ltd. | Composite conductive polymer composition, method of manufacturing the same, solution containing the composition, use of the composition |
| CN102834419B (zh) * | 2010-04-01 | 2015-10-21 | 帝斯曼知识产权资产管理有限公司 | 连续乳液聚合的方法 |
| US8946360B2 (en) * | 2010-09-22 | 2015-02-03 | Commonwealth Scientific And Industrial Research Organisation | Continuous flow polymerisation process |
| JP2012092249A (ja) * | 2010-10-28 | 2012-05-17 | Osaka Prefecture Univ | 粒子状重合体及びその製造方法 |
| CN103408754B (zh) | 2013-07-11 | 2015-10-28 | 东华大学 | 一种聚苯胺纳米纤维的制备方法 |
| US20170166690A1 (en) | 2013-11-27 | 2017-06-15 | Corning Incorporated | Advanced flow reactor synthesis of semiconducting polymers |
| US9481764B1 (en) * | 2015-10-13 | 2016-11-01 | The Boeing Company | Flow reactor synthesis of polymers |
-
2015
- 2015-10-13 US US14/882,073 patent/US9481764B1/en active Active
-
2016
- 2016-09-09 US US15/261,441 patent/US9751983B2/en not_active Ceased
- 2016-10-05 CA CA2944762A patent/CA2944762C/en active Active
- 2016-10-07 EP EP22158615.9A patent/EP4039364A1/en not_active Withdrawn
- 2016-10-07 JP JP2016199310A patent/JP6953123B2/ja active Active
- 2016-10-07 EP EP16192931.0A patent/EP3156122B1/en active Active
- 2016-10-07 EP EP16204785.6A patent/EP3170854B1/en active Active
- 2016-10-11 AU AU2016244187A patent/AU2016244187B2/en active Active
- 2016-10-11 KR KR1020160131064A patent/KR102666306B1/ko active Active
- 2016-10-13 CN CN201610892755.6A patent/CN106563400A/zh active Pending
- 2016-10-13 CN CN202210816658.4A patent/CN115178204A/zh active Pending
-
2017
- 2017-07-28 US US15/662,503 patent/US10118992B2/en active Active
-
2018
- 2018-08-08 US US16/058,680 patent/USRE48166E1/en active Active
- 2018-10-02 US US16/149,867 patent/US10584208B2/en active Active
-
2020
- 2020-01-14 US US16/742,282 patent/US11104765B2/en active Active
-
2021
- 2021-05-25 AU AU2021203395A patent/AU2021203395B2/en active Active
- 2021-06-30 JP JP2021108462A patent/JP7411608B2/ja active Active
- 2021-08-02 US US17/391,806 patent/US12104016B2/en active Active
-
2023
- 2023-02-17 JP JP2023023428A patent/JP7627713B2/ja active Active
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