JP2016505692A5 - - Google Patents
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- Publication number
- JP2016505692A5 JP2016505692A5 JP2015550693A JP2015550693A JP2016505692A5 JP 2016505692 A5 JP2016505692 A5 JP 2016505692A5 JP 2015550693 A JP2015550693 A JP 2015550693A JP 2015550693 A JP2015550693 A JP 2015550693A JP 2016505692 A5 JP2016505692 A5 JP 2016505692A5
- Authority
- JP
- Japan
- Prior art keywords
- poly
- glucan
- acid
- ester compound
- anhydride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920005640 poly alpha-1,3-glucan Polymers 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 16
- -1 ester compound Chemical class 0.000 claims description 15
- 150000008065 acid anhydrides Chemical class 0.000 claims description 14
- 125000002252 acyl group Chemical group 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 12
- 150000007524 organic acids Chemical class 0.000 claims description 12
- 150000001875 compounds Chemical class 0.000 claims description 7
- 239000003377 acid catalyst Substances 0.000 claims description 6
- 238000006467 substitution reaction Methods 0.000 claims description 6
- 239000000376 reactant Substances 0.000 claims description 5
- 238000010276 construction Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 21
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 12
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 6
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 6
- ILJSQTXMGCGYMG-UHFFFAOYSA-N triacetic acid Chemical compound CC(=O)CC(=O)CC(O)=O ILJSQTXMGCGYMG-UHFFFAOYSA-N 0.000 description 5
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
- 229920001503 Glucan Polymers 0.000 description 3
- YHASWHZGWUONAO-UHFFFAOYSA-N butanoyl butanoate Chemical compound CCCC(=O)OC(=O)CCC YHASWHZGWUONAO-UHFFFAOYSA-N 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 235000019260 propionic acid Nutrition 0.000 description 3
- WYVAMUWZEOHJOQ-UHFFFAOYSA-N propionic anhydride Chemical compound CCC(=O)OC(=O)CC WYVAMUWZEOHJOQ-UHFFFAOYSA-N 0.000 description 3
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- UGZICOVULPINFH-UHFFFAOYSA-N acetic acid;butanoic acid Chemical compound CC(O)=O.CCCC(O)=O UGZICOVULPINFH-UHFFFAOYSA-N 0.000 description 2
- AVMNFQHJOOYCAP-UHFFFAOYSA-N acetic acid;propanoic acid Chemical compound CC(O)=O.CCC(O)=O AVMNFQHJOOYCAP-UHFFFAOYSA-N 0.000 description 2
- 125000004063 butyryl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 150000007522 mineralic acids Chemical group 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 2
- 125000001501 propionyl group Chemical group O=C([*])C([H])([H])C([H])([H])[H] 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 1
- 125000000268 heptanoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000003104 hexanoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 125000002801 octanoyl group Chemical group C(CCCCCCC)(=O)* 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 125000003774 valeryl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
Applications Claiming Priority (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261746335P | 2012-12-27 | 2012-12-27 | |
| US201261746328P | 2012-12-27 | 2012-12-27 | |
| US201261746338P | 2012-12-27 | 2012-12-27 | |
| US61/746,328 | 2012-12-27 | ||
| US61/746,338 | 2012-12-27 | ||
| US61/746,335 | 2012-12-27 | ||
| PCT/US2013/076919 WO2014105698A1 (en) | 2012-12-27 | 2013-12-20 | Preparation of poly alpha-1,3-glucan esters and films therefrom |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016505692A JP2016505692A (ja) | 2016-02-25 |
| JP2016505692A5 true JP2016505692A5 (https=) | 2017-02-02 |
| JP6261610B2 JP6261610B2 (ja) | 2018-01-17 |
Family
ID=49956448
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015550693A Active JP6261610B2 (ja) | 2012-12-27 | 2013-12-20 | ポリα−１，３−グルカンエステルの調製及びそれからのフィルム |
Country Status (16)
| Country | Link |
|---|---|
| US (3) | US9278988B2 (https=) |
| EP (1) | EP2938639B1 (https=) |
| JP (1) | JP6261610B2 (https=) |
| KR (1) | KR20150100702A (https=) |
| CN (1) | CN105008401A (https=) |
| AU (1) | AU2013370663B2 (https=) |
| BR (1) | BR112015015528A8 (https=) |
| CA (1) | CA2895132A1 (https=) |
| CL (1) | CL2015001853A1 (https=) |
| ES (1) | ES2736042T3 (https=) |
| MX (1) | MX370287B (https=) |
| MY (1) | MY170135A (https=) |
| NZ (1) | NZ708558A (https=) |
| PH (1) | PH12015501541B1 (https=) |
| SG (2) | SG11201504218XA (https=) |
| WO (2) | WO2014105696A1 (https=) |
Families Citing this family (55)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2938639B1 (en) * | 2012-12-27 | 2019-05-01 | E. I. du Pont de Nemours and Company | Preparation of poly alpha-1,3-glucan esters |
| KR20150103678A (ko) * | 2013-12-20 | 2015-09-11 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 폴리 알파-1,3-글루칸 에스테르 필름 및 그 제조 방법 |
| CN106103551A (zh) | 2014-01-06 | 2016-11-09 | 纳幕尔杜邦公司 | 聚α‑1,3‑葡聚糖膜的制备 |
| US10106626B2 (en) | 2014-01-17 | 2018-10-23 | Ei Du Pont De Nemours And Company | Production of poly alpha-1,3-glucan formate films |
| CN106062050A (zh) * | 2014-01-17 | 2016-10-26 | 纳幕尔杜邦公司 | 聚α‑1，3‑葡聚糖甲酸酯的胶凝网络的制备以及由其形成的膜 |
| CN107074984A (zh) * | 2014-06-26 | 2017-08-18 | 纳幕尔杜邦公司 | 聚α‑1,3‑葡聚糖酯膜的制备 |
| BR112017013368B1 (pt) | 2014-12-22 | 2021-11-23 | Nutrition & Biosciences USA 4, Inc. | Composição de mistura polimérica |
| US11351104B2 (en) | 2015-02-06 | 2022-06-07 | Nutrition & Biosciences USA 4, Inc. | Colloidal dispersions of poly alpha-1,3-glucan based polymers |
| US10738266B2 (en) | 2015-06-01 | 2020-08-11 | Dupont Industrial Biosciences Usa, Llc | Structured liquid compositions comprising colloidal dispersions of poly alpha-1,3-glucan |
| JP6817972B2 (ja) * | 2015-06-30 | 2021-01-20 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ | 環状有機無水物を用いるポリα−１，３−グルカンエステルの調製 |
| ES2937288T3 (es) * | 2015-10-26 | 2023-03-27 | Nutrition & Biosciences Usa 4 Inc | Composición de alfa-(1,3->glucano) insoluble en agua |
| CA2997563C (en) | 2015-10-26 | 2022-03-22 | E. I. Du Pont De Nemours And Company | Polysaccharide coatings for paper |
| JP7045313B2 (ja) | 2015-11-13 | 2022-03-31 | ニュートリション・アンド・バイオサイエンシーズ・ユーエスエー・フォー，インコーポレイテッド | 洗濯ケアおよび織物ケアにおいて使用するためのグルカン繊維組成物 |
| WO2017083226A1 (en) | 2015-11-13 | 2017-05-18 | E. I. Du Pont De Nemours And Company | Glucan fiber compositions for use in laundry care and fabric care |
| EP3374401B1 (en) | 2015-11-13 | 2022-04-06 | Nutrition & Biosciences USA 4, Inc. | Glucan fiber compositions for use in laundry care and fabric care |
| US10895028B2 (en) | 2015-12-14 | 2021-01-19 | Dupont Industrial Biosciences Usa, Llc | Nonwoven glucan webs |
| BR112019001171B1 (pt) | 2016-07-22 | 2022-08-16 | Nutrition & Biosciences Usa 4, Inc | Polímero de poliuretano, composição de poliuretano, espuma de poliuretano e substrato fibroso revestido |
| KR102542217B1 (ko) * | 2016-10-28 | 2023-06-12 | 뉴트리션 앤드 바이오사이언시스 유에스에이 4, 인크. | 다당류를 포함하는 고무 조성물 |
| EP3545038A1 (en) | 2016-11-22 | 2019-10-02 | E. I. du Pont de Nemours and Company | Process for making polyacrylonitrile fibers |
| EP3545005A1 (en) | 2016-11-22 | 2019-10-02 | E. I. du Pont de Nemours and Company | In situ functionalization of polysaccharides and compositions thereof |
| JP2019536873A (ja) * | 2016-11-22 | 2019-12-19 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ | ポリα−１，３−グルカンエステル及びこれより作製された物品 |
| US20230192905A1 (en) * | 2016-11-22 | 2023-06-22 | E I Du Pont De Nemours And Company | Polyalpha-1,3-glucan esters and articles made therefrom |
| MX2019006868A (es) | 2016-12-16 | 2019-09-23 | Du Pont | Derivados de polisacáridos anfifílicos y composiciones que los comprenden. |
| EP3577142B1 (en) | 2017-04-25 | 2023-11-22 | Nutrition & Biosciences USA 4, Inc. | Polysaccharide coatings with oxygen barrier properties |
| US11608417B2 (en) | 2017-06-30 | 2023-03-21 | Nutrition & Biosciences USA 4, Inc. | Polysaccharide-elastomer masterbatch compositions |
| AU2018324496B2 (en) | 2017-09-01 | 2024-05-02 | Nutrition & Biosciences USA 4, Inc. | Latex compositions comprising polysaccharides |
| EP4467599A3 (en) | 2017-12-14 | 2025-04-23 | Nutrition & Biosciences USA 4, Inc. | Alpha-1,3-glucan graft copolymers |
| WO2019164669A1 (en) * | 2018-02-26 | 2019-08-29 | E. I. Du Pont De Nemours And Company | Blends of polyesters and polysaccharides |
| EP3870616B1 (en) | 2018-10-25 | 2023-10-11 | DuPont Industrial Biosciences USA, LLC | Alpha-1,3-glucan graft copolymers |
| BR112022024705A2 (pt) * | 2020-06-04 | 2023-02-28 | Nutrition & Biosciences Usa 4 Inc | Composição, método para produzir um composto de éter ou éster de copolímero de enxerto, método de floculação e método de absorção |
| EP4165091A1 (en) | 2020-06-10 | 2023-04-19 | Nutrition & Biosciences USA 4, Inc. | Poly alpha-1,6-glucan esters and compositions comprising same |
| ES2992779T3 (en) * | 2020-06-10 | 2024-12-18 | Procter & Gamble | A product comprising poly alpha 1,3-glucan esters |
| ES3033620T3 (en) | 2020-06-10 | 2025-08-06 | Procter & Gamble | A laundry care or dish care composition comprising a poly alpha-1,6-glucan derivative |
| HUE071383T2 (hu) | 2020-06-10 | 2025-08-28 | Procter & Gamble | Poli-alfa-1,6-glükánésztert tartalmazó mosószer vagy mosogatószer |
| PL4165154T3 (pl) | 2020-06-10 | 2024-07-08 | The Procter & Gamble Company | Kompozycja do prania lub pielęgnacji naczyń zawierająca pochodną poli(alfa-1,6-glukanu) |
| EP4284906A1 (en) | 2021-01-29 | 2023-12-06 | Danisco US Inc. | Compositions for cleaning and methods related thereto |
| WO2022178073A1 (en) | 2021-02-19 | 2022-08-25 | Nutrition & Biosciences USA 4, Inc. | Polysaccharide derivatives for detergent compositions |
| WO2022235655A1 (en) | 2021-05-04 | 2022-11-10 | Nutrition & Biosciences USA 4, Inc. | Compositions comprising insoluble alpha-glucan |
| US20240307288A1 (en) | 2021-07-13 | 2024-09-19 | Nutrition & Biosciences USA 4, Inc. | Cationic glucan ester derivatives |
| EP4426362A1 (en) | 2021-11-05 | 2024-09-11 | Nutrition & Biosciences USA 4, Inc. | Glucan derivatives for microbial control |
| US20250032390A1 (en) | 2021-12-16 | 2025-01-30 | Nutrition & Biosciences USA 4, Inc. | Compositions comprising cationic alpha-glucan ethers in aqueous polar organic solvents |
| KR20240167661A (ko) | 2022-03-21 | 2024-11-27 | 뉴트리션 앤드 바이오사이언시스 유에스에이 4, 인크. | 불용성 알파-글루칸을 포함하는 조성물 |
| JP2025523007A (ja) | 2022-07-11 | 2025-07-17 | ニュートリション・アンド・バイオサイエンシーズ・ユーエスエー・フォー，インコーポレイテッド | 両親媒性グルカンエステル誘導体 |
| WO2024081773A1 (en) | 2022-10-14 | 2024-04-18 | Nutrition & Biosciences USA 4, Inc. | Compositions comprising water, cationic alpha-1,6-glucan ether and organic solvent |
| WO2024112740A1 (en) | 2022-11-23 | 2024-05-30 | Nutrition & Biosciences USA 4, Inc. | Hygienic treatment of surfaces with compositions comprising hydrophobically modified alpha-glucan derivative |
| CN116589606B (zh) * | 2022-12-01 | 2024-05-28 | 中国药科大学 | 一种丁酰化酵母葡聚糖及其制备方法、应用 |
| WO2024129953A1 (en) | 2022-12-16 | 2024-06-20 | Nutrition & Biosciences USA 4, Inc. | Esterification of alpha-glucan comprising alpha-1,6 glycosidic linkages |
| WO2024163584A1 (en) | 2023-02-01 | 2024-08-08 | Danisco Us Inc. | Subtilisin variants and methods of use |
| EP4410941A1 (en) | 2023-02-01 | 2024-08-07 | The Procter & Gamble Company | Detergent compositions containing enzymes |
| WO2025072419A1 (en) | 2023-09-29 | 2025-04-03 | Nutrition & Biosciences Usa 1, Llc | Crosslinked alpha-glucan derivatives |
| WO2025072417A1 (en) | 2023-09-29 | 2025-04-03 | Nutrition & Biosciences USA 4, Inc. | Polysaccharide derivatives |
| WO2025072416A1 (en) | 2023-09-29 | 2025-04-03 | Nutrition & Biosciences USA 4, Inc. | Polysaccharide derivatives |
| WO2025117349A1 (en) | 2023-11-28 | 2025-06-05 | Nutrition & Biosciences USA 4, Inc. | Esterification of alpha-glucan comprising alpha-1,6 glycosidic linkages |
| WO2025199079A1 (en) | 2024-03-20 | 2025-09-25 | Nutrition & Biosciences USA 4, Inc. | Esterification of alpha-glucan comprising alpha-1,6 glycosidic linkages |
| WO2026024921A1 (en) | 2024-07-25 | 2026-01-29 | The Procter & Gamble Company | Detergent composition comprising a subtilisin variant and methods of use |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4501886A (en) * | 1982-08-09 | 1985-02-26 | E. I. Du Pont De Nemours And Company | Cellulosic fibers from anisotropic solutions |
| KR20010101647A (ko) | 1999-01-25 | 2001-11-14 | 메리 이. 보울러 | 폴리사카라이드 섬유 |
| CN1133654C (zh) | 1999-08-05 | 2004-01-07 | 武汉大学 | 灵芝α-(1→3)-D-葡聚糖羧甲基化衍生物及其用途和制备方法 |
| CN1133653C (zh) * | 1999-08-05 | 2004-01-07 | 武汉大学 | 灵芝α-(1→3)-D-葡聚糖硫酸酯衍生物及其用途和制备方法 |
| JP4584146B2 (ja) | 2003-07-09 | 2010-11-17 | 江崎グリコ株式会社 | α−１，４−グルカンおよび／またはその修飾物を含む成型物およびその製造方法 |
| US8642757B2 (en) | 2011-09-09 | 2014-02-04 | E I Du Pont De Nemours And Company | High titer production of highly linear poly (α 1,3 glucan) |
| US9080195B2 (en) | 2011-09-09 | 2015-07-14 | E I Du Pont De Nemours And Company | High titer production of poly (α 1,3 glucan) |
| US9403917B2 (en) * | 2012-12-27 | 2016-08-02 | E I Du Pont De Nemours And Company | Preparation of poly alpha-1,3-glucan esters and films therefrom |
| EP2938639B1 (en) * | 2012-12-27 | 2019-05-01 | E. I. du Pont de Nemours and Company | Preparation of poly alpha-1,3-glucan esters |
-
2013
- 2013-12-20 EP EP13821334.3A patent/EP2938639B1/en active Active
- 2013-12-20 AU AU2013370663A patent/AU2013370663B2/en not_active Ceased
- 2013-12-20 CA CA2895132A patent/CA2895132A1/en not_active Abandoned
- 2013-12-20 MY MYPI2015701718A patent/MY170135A/en unknown
- 2013-12-20 WO PCT/US2013/076905 patent/WO2014105696A1/en not_active Ceased
- 2013-12-20 CN CN201380073853.1A patent/CN105008401A/zh active Pending
- 2013-12-20 MX MX2015008463A patent/MX370287B/es active IP Right Grant
- 2013-12-20 KR KR1020157017106A patent/KR20150100702A/ko not_active Abandoned
- 2013-12-20 US US14/136,226 patent/US9278988B2/en active Active
- 2013-12-20 BR BR112015015528A patent/BR112015015528A8/pt not_active Application Discontinuation
- 2013-12-20 JP JP2015550693A patent/JP6261610B2/ja active Active
- 2013-12-20 WO PCT/US2013/076919 patent/WO2014105698A1/en not_active Ceased
- 2013-12-20 SG SG11201504218XA patent/SG11201504218XA/en unknown
- 2013-12-20 NZ NZ70855813A patent/NZ708558A/en not_active IP Right Cessation
- 2013-12-20 ES ES13821334T patent/ES2736042T3/es active Active
- 2013-12-20 US US14/136,168 patent/US20140187766A1/en not_active Abandoned
-
2014
- 2014-06-26 SG SG11201505127QA patent/SG11201505127QA/en unknown
-
2015
- 2015-06-26 CL CL2015001853A patent/CL2015001853A1/es unknown
- 2015-07-08 PH PH12015501541A patent/PH12015501541B1/en unknown
-
2016
- 2016-03-02 US US15/058,406 patent/US10000580B2/en active Active
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