JP2016088982A - 光増感剤組成物及び光重合性組成物 - Google Patents
光増感剤組成物及び光重合性組成物 Download PDFInfo
- Publication number
- JP2016088982A JP2016088982A JP2014222581A JP2014222581A JP2016088982A JP 2016088982 A JP2016088982 A JP 2016088982A JP 2014222581 A JP2014222581 A JP 2014222581A JP 2014222581 A JP2014222581 A JP 2014222581A JP 2016088982 A JP2016088982 A JP 2016088982A
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- JP
- Japan
- Prior art keywords
- bis
- anthracene
- group
- naphthalene
- oxy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000203 mixture Substances 0.000 title claims abstract description 91
- 239000003504 photosensitizing agent Substances 0.000 title claims abstract description 63
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Natural products C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 claims abstract description 495
- -1 anthracene compound Chemical class 0.000 claims abstract description 269
- UFWIBTONFRDIAS-UHFFFAOYSA-N naphthalene-acid Natural products C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 claims abstract description 67
- UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims abstract description 56
- 125000003545 alkoxy group Chemical group 0.000 claims abstract description 23
- 125000003118 aryl group Chemical group 0.000 claims abstract description 8
- 125000000217 alkyl group Chemical group 0.000 claims description 56
- 150000001875 compounds Chemical class 0.000 claims description 42
- 125000004432 carbon atom Chemical group C* 0.000 claims description 36
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 30
- 125000003277 amino group Chemical group 0.000 claims description 18
- 125000005843 halogen group Chemical group 0.000 claims description 17
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 claims description 16
- 125000004183 alkoxy alkyl group Chemical group 0.000 claims description 14
- 125000003710 aryl alkyl group Chemical group 0.000 claims description 14
- 125000002768 hydroxyalkyl group Chemical group 0.000 claims description 14
- 125000000542 sulfonic acid group Chemical group 0.000 claims description 13
- 239000004593 Epoxy Substances 0.000 claims description 12
- 125000003342 alkenyl group Chemical group 0.000 claims description 12
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 12
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims description 12
- 230000001678 irradiating effect Effects 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims description 5
- 125000001424 substituent group Chemical group 0.000 claims description 5
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims description 4
- 230000000379 polymerizing effect Effects 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 150000003457 sulfones Chemical class 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 208000017983 photosensitivity disease Diseases 0.000 abstract description 2
- 231100000434 photosensitization Toxicity 0.000 abstract description 2
- 125000004400 (C1-C12) alkyl group Chemical group 0.000 abstract 1
- 125000005336 allyloxy group Chemical group 0.000 abstract 1
- LJSLYKNKVQMIJY-UHFFFAOYSA-N 1,4-diethoxynaphthalene Chemical compound C1=CC=C2C(OCC)=CC=C(OCC)C2=C1 LJSLYKNKVQMIJY-UHFFFAOYSA-N 0.000 description 18
- 239000003999 initiator Substances 0.000 description 15
- QPCMKVGYDGXROK-UHFFFAOYSA-N (10-octanoyloxyanthracen-9-yl) octanoate Chemical compound C(CCCCCCC)(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(CCCCCCC)=O QPCMKVGYDGXROK-UHFFFAOYSA-N 0.000 description 14
- MZMKBSPKOUSOFJ-UHFFFAOYSA-N C(CCCC)(=O)OC1=CC=CC2=CC3=CC=CC=C3C=C12 Chemical compound C(CCCC)(=O)OC1=CC=CC2=CC3=CC=CC=C3C=C12 MZMKBSPKOUSOFJ-UHFFFAOYSA-N 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 13
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 12
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 11
- AZQHHLVLEQCFIM-UHFFFAOYSA-N anthracen-1-yl butanoate Chemical compound C(CCC)(=O)OC1=CC=CC2=CC3=CC=CC=C3C=C12 AZQHHLVLEQCFIM-UHFFFAOYSA-N 0.000 description 11
- 239000000463 material Substances 0.000 description 11
- 125000006606 n-butoxy group Chemical group 0.000 description 10
- DFMJWQFCLBTBHC-UHFFFAOYSA-N (10-butoxycarbonyloxyanthracen-9-yl) butyl carbonate Chemical compound C(CCC)OC(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(=O)OCCCC DFMJWQFCLBTBHC-UHFFFAOYSA-N 0.000 description 9
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 9
- 125000004423 acyloxy group Chemical group 0.000 description 9
- 239000011248 coating agent Substances 0.000 description 8
- 230000003287 optical effect Effects 0.000 description 8
- LAJCSHRWLHTXHK-UHFFFAOYSA-N (10-propoxycarbonyloxyanthracen-9-yl) propyl carbonate Chemical compound C(CC)OC(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(=O)OCCC LAJCSHRWLHTXHK-UHFFFAOYSA-N 0.000 description 7
- VIMUQVLJMSKXGY-UHFFFAOYSA-N anthracen-1-yl hexyl carbonate Chemical compound C(OC1=CC=CC2=CC3=CC=CC=C3C=C12)(OCCCCCC)=O VIMUQVLJMSKXGY-UHFFFAOYSA-N 0.000 description 7
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 7
- 150000001454 anthracenes Chemical class 0.000 description 6
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 6
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 6
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 6
- PCILLCXFKWDRMK-UHFFFAOYSA-N naphthalene-1,4-diol Chemical compound C1=CC=C2C(O)=CC=C(O)C2=C1 PCILLCXFKWDRMK-UHFFFAOYSA-N 0.000 description 6
- 238000006116 polymerization reaction Methods 0.000 description 6
- 238000002834 transmittance Methods 0.000 description 6
- FWWRTYBQQDXLDD-UHFFFAOYSA-N 1,4-dimethoxynaphthalene Chemical compound C1=CC=C2C(OC)=CC=C(OC)C2=C1 FWWRTYBQQDXLDD-UHFFFAOYSA-N 0.000 description 5
- APQSQLNWAIULLK-UHFFFAOYSA-N 1,4-dimethoxynaphthalene Natural products C1=CC=C2C(C)=CC=C(C)C2=C1 APQSQLNWAIULLK-UHFFFAOYSA-N 0.000 description 5
- BOTGCZBEERTTDQ-UHFFFAOYSA-N 4-Methoxy-1-naphthol Chemical compound C1=CC=C2C(OC)=CC=C(O)C2=C1 BOTGCZBEERTTDQ-UHFFFAOYSA-N 0.000 description 5
- 125000002723 alicyclic group Chemical group 0.000 description 5
- 125000003302 alkenyloxy group Chemical group 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000001723 curing Methods 0.000 description 5
- 239000000976 ink Substances 0.000 description 5
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 5
- 239000000758 substrate Substances 0.000 description 5
- MEDLHZNRAQAHCV-UHFFFAOYSA-N (10-heptanoyloxyanthracen-9-yl) heptanoate Chemical compound C(CCCCCC)(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(CCCCCC)=O MEDLHZNRAQAHCV-UHFFFAOYSA-N 0.000 description 4
- YPESPOJYFDMJPO-UHFFFAOYSA-N (10-nonanoyloxyanthracen-9-yl) nonanoate Chemical compound C(CCCCCCCC)(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(CCCCCCCC)=O YPESPOJYFDMJPO-UHFFFAOYSA-N 0.000 description 4
- ICDVRRFJYKMRAK-UHFFFAOYSA-N (10-propanoyloxyanthracen-9-yl) propanoate Chemical compound C(CC)(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC12)OC(CC)=O ICDVRRFJYKMRAK-UHFFFAOYSA-N 0.000 description 4
- AYGVEPSCRTYPAD-UHFFFAOYSA-N 2-(2,2-diphenylethoxy)naphthalene Chemical compound C1(=CC=CC=C1)C(COC1=CC2=CC=CC=C2C=C1)C1=CC=CC=C1 AYGVEPSCRTYPAD-UHFFFAOYSA-N 0.000 description 4
- KSMGAOMUPSQGTB-UHFFFAOYSA-N 9,10-dibutoxyanthracene Chemical compound C1=CC=C2C(OCCCC)=C(C=CC=C3)C3=C(OCCCC)C2=C1 KSMGAOMUPSQGTB-UHFFFAOYSA-N 0.000 description 4
- KHEDNBRORNZTNH-UHFFFAOYSA-N [10-(2-ethylhexanoyloxy)anthracen-9-yl] 2-ethylhexanoate Chemical compound C(C)C(C(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(C(CCCC)CC)=O)CCCC KHEDNBRORNZTNH-UHFFFAOYSA-N 0.000 description 4
- GROQZUISBOBUSK-UHFFFAOYSA-N [10-(2-ethylhexoxycarbonyloxy)anthracen-9-yl] 2-ethylhexyl carbonate Chemical compound C(C)C(COC(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(=O)OCC(CCCC)CC)CCCC GROQZUISBOBUSK-UHFFFAOYSA-N 0.000 description 4
- RURGWVZQAKAYDM-UHFFFAOYSA-N anthracene-9,10-diol diacetate Chemical compound C1=CC=C2C(OC(=O)C)=C(C=CC=C3)C3=C(OC(C)=O)C2=C1 RURGWVZQAKAYDM-UHFFFAOYSA-N 0.000 description 4
- 238000004040 coloring Methods 0.000 description 4
- 239000000945 filler Substances 0.000 description 4
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical class I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 4
- 239000003973 paint Substances 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- HDXJWZHGDQGINF-UHFFFAOYSA-N (10-hexanoyloxyanthracen-9-yl) hexanoate Chemical compound C(CCCCC)(=O)OC=1C2=CC=CC=C2C(=C2C=CC=CC=12)OC(CCCCC)=O HDXJWZHGDQGINF-UHFFFAOYSA-N 0.000 description 3
- GDFQRDTZOFMSSM-UHFFFAOYSA-N (10-methoxycarbonyloxyanthracen-9-yl) methyl carbonate Chemical compound C1=CC=C2C(OC(=O)OC)=C(C=CC=C3)C3=C(OC(=O)OC)C2=C1 GDFQRDTZOFMSSM-UHFFFAOYSA-N 0.000 description 3
- YHZACTONCWMCNR-UHFFFAOYSA-N 1,2,6-trimethoxynaphthalene Chemical compound COC1=C(OC)C=CC2=CC(OC)=CC=C21 YHZACTONCWMCNR-UHFFFAOYSA-N 0.000 description 3
- LAGRACHHBNQZAL-UHFFFAOYSA-N 2-methyl-1,4-dipropoxynaphthalene Chemical compound CC1=C(C2=CC=CC=C2C(=C1)OCCC)OCCC LAGRACHHBNQZAL-UHFFFAOYSA-N 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- BIYFTUVRMSVKEH-UHFFFAOYSA-N anthracen-1-yl octanoate Chemical compound C(CCCCCCC)(=O)OC1=CC=CC2=CC3=CC=CC=C3C=C12 BIYFTUVRMSVKEH-UHFFFAOYSA-N 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 3
- 239000003085 diluting agent Substances 0.000 description 3
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 3
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 3
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- ZJTLZYDQJHKRMQ-UHFFFAOYSA-N menadiol Chemical compound C1=CC=CC2=C(O)C(C)=CC(O)=C21 ZJTLZYDQJHKRMQ-UHFFFAOYSA-N 0.000 description 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 3
- 229910052753 mercury Inorganic materials 0.000 description 3
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 3
- 125000003506 n-propoxy group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])O* 0.000 description 3
- 150000002790 naphthalenes Chemical class 0.000 description 3
- 125000001820 oxy group Chemical group [*:1]O[*:2] 0.000 description 3
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- Polymerisation Methods In General (AREA)
- Epoxy Resins (AREA)
Abstract
Description
本発明の光増感剤組成物における、アントラセン化合物は、下記一般式(1)で表される化合物である。
次に、本発明の光重合性組成物について説明する。本発明の光重合性組成物は、上記の光増感剤組成物と光重合開始剤と重合性化合物と、を含有する組成物である。光重合開始剤としては、スルホニウム塩、ヨ−ドニウム塩のようなオニウム塩等が挙げられる。スルホニウム塩としては、S,S,S’,S’−テトラフェニル−S,S’−(4、4’−チオジフェニル)ジスルホニウムビスヘキサフルオロフォスフェート、ジフェニル−4−フェニルチオフェニルスルホニウムヘキサフルオロフォスフェート、トリフェニルスルホニウムヘキサフルオロフォスフェート等が挙げられ、例えばサンアプロ製CPI−100Pを用いることができる。
本発明の光重合性組成物は、可視光や紫外線等の活性エネルギー線を照射することにより重合させることができる。照射光の波長は250nmから500nmの範囲の光であれば特に制限はないが、好ましくは300nm〜450nmの範囲の光、さらに好ましくは355nm〜420nmに含まれる光を照射することにより速やかに硬化させることができる。この場合の光源としては、上述の波長範囲に含まれる光を照射することのできる光源であればいずれも使用でき、例えば太陽光の他、高圧水銀ランプ、キセノンランプ、紫外線LED、青紫LED、メタルハライドランプ、フュージョン(株)製のHランプ、Dランプ、Vランプが好適に使用できる。また基材上に塗布したフィルム状物のみならず、塊状物を硬化させることも可能である。
本発明の光重合性組成物は、活性エネルギー線の照射によって反応、重合、硬化させることができるコーティング剤、塗料、インク、成型材等に用いることができる。具体的には金属や樹脂、ガラス、紙、木材等の基材上に塗布する塗料、自動車、船舶、航空機等向けの塗料、ハードコート剤、汚れ防止膜、反射防止膜、衝撃緩衝膜、帯電防止コート剤、オーバーコート剤、などのコーティング剤や保護膜材料、光硬化型の接着剤、粘着剤、光崩壊・分解型の塗料、塗膜、成型物などに用いられる。特に光重合後の着色を低減できることから液晶ディスプレイや有機ELディスプレイなどのディスプレイ向けコーティング剤や接着剤、粘着剤に好適に用いられる。さらにホログラム材料などの光記録媒体もしくは光記録媒体向け材料、光造形用樹脂、3Dプリンタ用インク(樹脂)、電子回路や半導体製造用フォトレジスト、ドライフィルムレジスト、液晶ディスプレイ、有機ELディスプレイなどのディスプレイ向けカラーフィルター用レジスト、ブラックマトリックス用レジスト、光取り出し膜、封止剤、スクリーン印刷・オフセット印刷・グラビア印刷等の印刷用インク、インクジェットプリンタ向けの光硬化型インク、レーザパタニング用組成物、レンズ、レンズアレイ、光導波路、導光板、光拡散板、回折素子、光学用接着剤等の光学部材、ナノインプリンティング用材料、などの種々の用途への適用が可能である。
セロキサイド2021P:ダイセル社製脂環式エポキシ化合物
CPI−100P:サンアプロ社製スルホニウム塩
化合物A:9,10−ビス(n−オクタノイルオキシ)アントラセン
DBA:9,10−ジブトキシアントラセン
DEN:1,4−ジエトキシナフタレン
重合性化合物として、脂環式エポキシ化合物(ダイセル社製セロキサイド2021P)100部に対し、光重合開始剤として、スルホニウム塩(サンアプロ社製CPI−100P)3.0部、光増感剤として、9,10−ビス(n−オクタノイルオキシ)アントラセンを1.5部、1,4−ジエトキシナフタレン1.5部を混合し、光重合性組成物を調製した。該組成物をポリエステルフィルム(東レ社製ルミラー)の上にバーコーターを用いて膜厚が12μmになるように塗布した。次いで、表面からフォセオン社製紫外線LEDを用いて光照射した。照射光の中心波長は395nmで照射強度は50mW/cm2である。光照射してからフィルム上の塗布物のべたつき(タック)がなくなるまでの光照射時間「タック・フリー・タイム」は30秒であった。
光増感剤として、9,10−ビス(n−オクタノイルオキシ)アントラセンを1.5部、1,4−ジエトキシナフタレン3.0部とした他は実施例1と同様にして光重合性組成物を調製し、実施例1と同様の条件で光照射した。べたつき(タック)がなくなるまでの光照射時間「タック・フリー・タイム」は25秒であった。
光増感剤として、9,10−ビス(n−オクタノイルオキシ)アントラセンを1.5部、1,4−ジエトキシナフタレン6.0部とした他は実施例1と同様にして光重合性組成物を調製し、実施例1と同様の条件で光照射した。べたつき(タック)がなくなるまでの光照射時間「タック・フリー・タイム」は25秒であった。
光増感剤として、1,4−ジエトキシナフタレンを使用しないこと以外は実施例1と同様にして光重合性組成物を調製し、実施例1と同様の条件で光照射した。べたつき(タック)がなくなるまでの光照射時間「タック・フリー・タイム」は60秒であった。
光増感剤として、1,4−ジエトキシナフタレンを使用せず9,10−ビス(n−オクタノイルオキシ)アントラセンを3.0部とした以外は実施例1と同様にして光重合性組成物を調製し、実施例1と同様の条件で光照射した。べたつき(タック)がなくなるまでの光照射時間「タック・フリー・タイム」は30秒であった。
光増感剤として、1,4−ジエトキシナフタレンを使用せず9,10−ジブトキシアントラセンを1.5部とした以外は実施例1と同様にして光重合性組成物を調製し、実施例1と同様の条件で光照射した。べたつき(タック)がなくなるまでの光照射時間「タック・フリー・タイム」は30秒であった。
光増感剤として、9,10−ビス(n−オクタノイルオキシ)アントラセンを使用しないこと以外は実施例1と同様にして光重合性組成物を調製し、実施例1と同様の条件で光照射した。しかし、300秒たってもべたつき(タック)がなくならず、光重合していなかった。
重合性化合物として脂環式エポキシ化合物(ダイセル社製セロキサイド2021P)100部に対し、光重合開始剤として、スルホニウム塩(サンアプロ社製CPI−100P)3.0部、光増感剤として、9,10−ビス(n−オクタノイルオキシ)アントラセンを1.5部、1,4−ジエトキシナフタレン1.5部を混合し、光重合性組成物を調製した。該組成物をアセテートフィルム(サンプラテック社、厚膜100μm)の上にバーコーターを用いて膜厚が12μmになるように塗布した。次いで、表面からフォセオン社製紫外線LEDを用いて30秒間光照射した。照射光の中心波長は395nmで照射強度は50mW/cm2である。このようにして得られたフィルムの黄色度(YI)を紫外線(UV)分光光度計(島津製作所、形式UV−2600)で測定したところ、YIは1.09であった。
光増感剤として、1,4−ジエトキシナフタレンを使用せず9,10−ビス(n−オクタノイルオキシ)アントラセンを3.0部とした以外は実施例4と同様の操作を行ったところ、得られたフィルムの黄色度は1.76であった。
光増感剤として、1,4−ジエトキシナフタレンを使用せず9,10−ジブトキシアントラセンを1.5部とした以外は実施例4と同様の操作を行ったところ、得られたフィルムの黄色度は3.47であった。
Claims (10)
- 下記一般式(1)で表されるアントラセン化合物と、下記一般式(2)で表されるナフタレン化合物又は下記一般式(3)で表されるベンゼン化合物と、を含有する光増感剤組成物。
- 光増感剤組成物において、アントラセン化合物の1重量部に対し、ナフタレン化合物又はベンゼン化合物を0.1〜100重量部含有することを特徴とする請求項1乃至3のいずれか一項に記載の光増感剤組成物。
- 請求項1乃至4のいずれか一項に記載の光増感剤組成物と、光重合開始剤と、重合性化合物を含有する光重合性組成物。
- 前記重合性化合物がエポキシ化合物又はビニルエーテルである請求項5に記載の光重合性組成物。
- 請求項5又は6のいずれかに記載の光重合性組成物に、活性エネルギー線を照射することを特徴とする光重合性組成物の重合方法。
- 前記活性エネルギー線が波長範囲355〜420nmの光を含む活性エネルギー線であることを特徴とする請求項7に記載の光重合性組成物の重合方法。
- 請求項5又は6のいずれかに記載の光重合性組成物に、活性エネルギー線を照射することにより、光重合してなる光硬化物。
- 前記活性エネルギー線が波長範囲355〜420nmの光を含む活性エネルギー線であるであることを特徴とする請求項9に記載の光硬化物。
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