JP2015510541A5 - - Google Patents
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- Publication number
- JP2015510541A5 JP2015510541A5 JP2014546109A JP2014546109A JP2015510541A5 JP 2015510541 A5 JP2015510541 A5 JP 2015510541A5 JP 2014546109 A JP2014546109 A JP 2014546109A JP 2014546109 A JP2014546109 A JP 2014546109A JP 2015510541 A5 JP2015510541 A5 JP 2015510541A5
- Authority
- JP
- Japan
- Prior art keywords
- rare earth
- waste
- ammonium sulfate
- oxide
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
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- 238000000034 method Methods 0.000 claims 22
- 229910052761 rare earth metal Inorganic materials 0.000 claims 20
- 150000002910 rare earth metals Chemical class 0.000 claims 20
- 239000002699 waste material Substances 0.000 claims 17
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims 16
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims 8
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims 8
- 235000011130 ammonium sulphate Nutrition 0.000 claims 8
- 239000000243 solution Substances 0.000 claims 8
- 239000000203 mixture Substances 0.000 claims 5
- 239000000843 powder Substances 0.000 claims 4
- 239000002244 precipitate Substances 0.000 claims 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- 238000000576 coating method Methods 0.000 claims 3
- 238000010438 heat treatment Methods 0.000 claims 3
- 238000002156 mixing Methods 0.000 claims 3
- 238000001556 precipitation Methods 0.000 claims 3
- 229910052684 Cerium Inorganic materials 0.000 claims 2
- 229910052692 Dysprosium Inorganic materials 0.000 claims 2
- 229910052691 Erbium Inorganic materials 0.000 claims 2
- 229910052693 Europium Inorganic materials 0.000 claims 2
- 229910052688 Gadolinium Inorganic materials 0.000 claims 2
- 229910052779 Neodymium Inorganic materials 0.000 claims 2
- 229910052777 Praseodymium Inorganic materials 0.000 claims 2
- 229910052772 Samarium Inorganic materials 0.000 claims 2
- 229910052771 Terbium Inorganic materials 0.000 claims 2
- 239000007864 aqueous solution Substances 0.000 claims 2
- 239000006227 byproduct Substances 0.000 claims 2
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 claims 2
- 239000011248 coating agent Substances 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- KBQHZAAAGSGFKK-UHFFFAOYSA-N dysprosium atom Chemical compound [Dy] KBQHZAAAGSGFKK-UHFFFAOYSA-N 0.000 claims 2
- UYAHIZSMUZPPFV-UHFFFAOYSA-N erbium Chemical compound [Er] UYAHIZSMUZPPFV-UHFFFAOYSA-N 0.000 claims 2
- OGPBJKLSAFTDLK-UHFFFAOYSA-N europium atom Chemical compound [Eu] OGPBJKLSAFTDLK-UHFFFAOYSA-N 0.000 claims 2
- 239000000706 filtrate Substances 0.000 claims 2
- UIWYJDYFSGRHKR-UHFFFAOYSA-N gadolinium atom Chemical compound [Gd] UIWYJDYFSGRHKR-UHFFFAOYSA-N 0.000 claims 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 2
- 229910052746 lanthanum Inorganic materials 0.000 claims 2
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims 2
- 239000011707 mineral Substances 0.000 claims 2
- QEFYFXOXNSNQGX-UHFFFAOYSA-N neodymium atom Chemical compound [Nd] QEFYFXOXNSNQGX-UHFFFAOYSA-N 0.000 claims 2
- PUDIUYLPXJFUGB-UHFFFAOYSA-N praseodymium atom Chemical compound [Pr] PUDIUYLPXJFUGB-UHFFFAOYSA-N 0.000 claims 2
- 239000002994 raw material Substances 0.000 claims 2
- 150000003839 salts Chemical class 0.000 claims 2
- KZUNJOHGWZRPMI-UHFFFAOYSA-N samarium atom Chemical compound [Sm] KZUNJOHGWZRPMI-UHFFFAOYSA-N 0.000 claims 2
- 229910052706 scandium Inorganic materials 0.000 claims 2
- SIXSYDAISGFNSX-UHFFFAOYSA-N scandium atom Chemical compound [Sc] SIXSYDAISGFNSX-UHFFFAOYSA-N 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- GZCRRIHWUXGPOV-UHFFFAOYSA-N terbium atom Chemical compound [Tb] GZCRRIHWUXGPOV-UHFFFAOYSA-N 0.000 claims 2
- 238000005406 washing Methods 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- 229910052727 yttrium Inorganic materials 0.000 claims 2
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims 1
- 229910000640 Fe alloy Inorganic materials 0.000 claims 1
- 229910005813 NiMH Inorganic materials 0.000 claims 1
- 229910052769 Ytterbium Inorganic materials 0.000 claims 1
- 239000000908 ammonium hydroxide Substances 0.000 claims 1
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 claims 1
- 238000001354 calcination Methods 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 239000010987 cubic zirconia Substances 0.000 claims 1
- 239000005548 dental material Substances 0.000 claims 1
- HBAGRTDVSXKKDO-UHFFFAOYSA-N dioxido(dioxo)manganese lanthanum(3+) Chemical compound [La+3].[La+3].[O-][Mn]([O-])(=O)=O.[O-][Mn]([O-])(=O)=O.[O-][Mn]([O-])(=O)=O HBAGRTDVSXKKDO-UHFFFAOYSA-N 0.000 claims 1
- 238000005566 electron beam evaporation Methods 0.000 claims 1
- 239000000446 fuel Substances 0.000 claims 1
- 239000010437 gem Substances 0.000 claims 1
- 229910001751 gemstone Inorganic materials 0.000 claims 1
- 238000000227 grinding Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000003754 machining Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- UZLYXNNZYFBAQO-UHFFFAOYSA-N oxygen(2-);ytterbium(3+) Chemical class [O-2].[O-2].[O-2].[Yb+3].[Yb+3] UZLYXNNZYFBAQO-UHFFFAOYSA-N 0.000 claims 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 238000005507 spraying Methods 0.000 claims 1
- NAWDYIZEMPQZHO-UHFFFAOYSA-N ytterbium Chemical compound [Yb] NAWDYIZEMPQZHO-UHFFFAOYSA-N 0.000 claims 1
- 229910003454 ytterbium oxide Inorganic materials 0.000 claims 1
- 229910001928 zirconium oxide Inorganic materials 0.000 claims 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161630255P | 2011-12-07 | 2011-12-07 | |
| US61/630,255 | 2011-12-07 | ||
| US13/706,546 | 2012-12-06 | ||
| US13/706,546 US8940256B2 (en) | 2011-12-07 | 2012-12-06 | Method for recycling of rare earth and zirconium oxide materials |
| PCT/US2012/068397 WO2013086288A2 (en) | 2011-12-07 | 2012-12-07 | Method for recycling of rare earth and zirconium oxide materials |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2015510541A JP2015510541A (ja) | 2015-04-09 |
| JP2015510541A5 true JP2015510541A5 (enExample) | 2016-01-14 |
Family
ID=48575061
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014546109A Withdrawn JP2015510541A (ja) | 2011-12-07 | 2012-12-07 | 希土類材料および酸化ジルコニウム材料のリサイクル方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8940256B2 (enExample) |
| EP (1) | EP2788517A4 (enExample) |
| JP (1) | JP2015510541A (enExample) |
| KR (1) | KR20140102725A (enExample) |
| CN (1) | CN104185606A (enExample) |
| WO (1) | WO2013086288A2 (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103451433B (zh) * | 2013-08-27 | 2015-10-14 | 李露青 | 一种从含贵金属废催化剂中提取贵金属的方法 |
| CN103451432B (zh) * | 2013-08-27 | 2015-08-05 | 江西南城鑫业环保处置有限公司 | 一种从含贵金属废催化剂中提取铅和贵金属的方法 |
| US9334549B2 (en) | 2013-12-20 | 2016-05-10 | General Electric Company | Systems and methods for recovery of rare-earth constituents from environmental barrier coatings |
| KR101588390B1 (ko) | 2014-04-11 | 2016-02-15 | 한전원자력연료 주식회사 | 지르코늄 합금 스크랩 재활용을 위한 세정기술 |
| CN104628382B (zh) * | 2014-10-16 | 2017-03-08 | 深圳市商德先进陶瓷有限公司 | 回收氧化锆陶瓷注射喂料的处理方法 |
| CN104651619B (zh) * | 2015-03-17 | 2016-09-28 | 湖南东方钪业股份有限公司 | 含有钪及稀土稳定的氧化锆陶瓷废料中分离回收钪的方法 |
| EP3135779A1 (de) * | 2015-08-24 | 2017-03-01 | Siemens Aktiengesellschaft | Verfahren und vorrichtung zur verarbeitung eines mindestens einen wertstoff, insbesondere aus der gruppe der seltenen erden, und begleitstoffe aufweisenden rohstoffs |
| KR101717255B1 (ko) * | 2015-10-05 | 2017-03-16 | 군산대학교 산학협력단 | 재생 지르코니아 블록 및 그 제조방법 |
| CN107377867B (zh) * | 2017-08-22 | 2019-10-18 | 汉川市石金科技有限公司 | 一种铸钢涂料及其制备方法 |
| KR102035295B1 (ko) * | 2018-07-24 | 2019-10-22 | 주식회사 엔코 | 폐니켈-수소전지로부터 희토류 산화물을 제조하는 방법 |
| CN109457297A (zh) * | 2018-11-15 | 2019-03-12 | 四川建志科技有限责任公司 | 氧化锆晶体加工废粉料循环利用方法 |
| JP7337609B2 (ja) * | 2019-09-04 | 2023-09-04 | 株式会社東芝 | セラミックスからの金属回収方法 |
| US12077835B2 (en) * | 2019-10-07 | 2024-09-03 | West Virginia University | Methods and compositions for extraction of rare earth elements from coal ash |
| CN112708768B (zh) * | 2021-01-13 | 2023-06-13 | 广东先导稀材股份有限公司 | 一种固态氧化物燃料电池高铬废料的预处理方法 |
| CN116535172B (zh) * | 2023-07-06 | 2023-09-22 | 北京建工环境修复股份有限公司 | 一种高比活度稀土渣的处置方法及固化体 |
Family Cites Families (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1995334A (en) | 1931-06-09 | 1935-03-26 | Burgess Lab Inc C F | Method of decomposing and further treating material containing titanium oxide |
| US2160148A (en) | 1935-04-12 | 1939-05-30 | Hunyady Istvan | Treatment of aluminum ores |
| US2520958A (en) | 1947-01-14 | 1950-09-05 | Poole Henry Gordon | Nickel recovery |
| US2525474A (en) | 1949-05-18 | 1950-10-10 | Nat Lead Co | Method for preparing ammonium zirconium sulfate salt |
| US2801153A (en) | 1953-08-21 | 1957-07-30 | Tholand Inc | Recovery of lithium from spodumene ores |
| US3057685A (en) | 1960-05-23 | 1962-10-09 | Edna Y Kamlet | Cyclic process for the beneficiation of titania ores and slags |
| DE1294947B (de) | 1962-05-08 | 1969-05-14 | Degussa | Verfahren zum Aufschliessen von Zirkonsand |
| FR2063581A5 (enExample) | 1969-10-22 | 1971-07-09 | Ugine Kuhlmann | |
| GB1340276A (en) | 1970-04-21 | 1973-12-12 | Kernforschungsanlage Juelich | Process for decomposing metallic oxide materials |
| FI65088C (fi) | 1979-05-25 | 1984-03-12 | Pekka Juhani Saikkonen | Foerfarande foer aotervinning av icke-jaernmetaller ur deras mineralier mineralslig oxidiska rostningsprodukter och slagg |
| DE2927128C2 (de) | 1979-07-05 | 1981-06-11 | Th. Goldschmidt Ag, 4300 Essen | Verfahren zur Herstellung von basischem Zirkoncarbonat hoher Reinheit |
| NZ215774A (en) | 1985-05-02 | 1988-08-30 | Ici Australia Ltd | Purification of zirconium compounds |
| US5129945A (en) | 1990-10-24 | 1992-07-14 | The United States Of America As Represented By The Secretary Of The Interior | Scrap treatment method for rare earth transition metal alloys |
| FR2668764B1 (fr) | 1990-11-07 | 1993-12-24 | Westinghouse Electric Corp | Production d'un oxyde de zirconium ou d'hafnium de haute qualite. |
| KR950013315B1 (ko) * | 1993-05-07 | 1995-11-02 | 주식회사엘지금속 | 폐수중 불소처리 잔사의 재처리방법 |
| IT1275426B (it) | 1995-05-16 | 1997-08-07 | Bracco Spa | Recupero del gadolinio e dei suoi agenti complessanti da soluzioni acquose contenenti i loro complessi |
| JPH09217132A (ja) | 1996-02-13 | 1997-08-19 | Santoku Kinzoku Kogyo Kk | 希土類−鉄系合金からの有用元素の回収方法 |
| EP1035074B1 (en) | 1999-03-05 | 2007-02-14 | Daiichi Kigenso Kagaku Co., Ltd. | Zirconium- and cerium-based mixed oxide, method of production thereof, catalyst material comprising the mixed oxide and use of the catalyst in exhaust gas purification |
| DE19913550B4 (de) | 1999-03-25 | 2006-05-04 | Siemens Ag | Verfahren zur Herstellung von Seltenerdoxysulfid-Pulver |
| BR0208294A (pt) | 2001-03-08 | 2004-04-13 | Cotter Corp Nsl | Método de recuperar valores de zircÈnio |
| US6703334B2 (en) | 2001-12-17 | 2004-03-09 | Praxair S.T. Technology, Inc. | Method for manufacturing stabilized zirconia |
| JP4287749B2 (ja) * | 2002-03-19 | 2009-07-01 | 株式会社三徳 | 希土類−遷移金属合金スクラップからの有用元素の回収方法 |
| US7147832B2 (en) | 2003-12-30 | 2006-12-12 | Vladimir Belov | Process for the isolation and purification of zirconium peroxosulfate and uses thereof |
| DE102006025945A1 (de) | 2006-06-02 | 2007-12-06 | Patent-Treuhand-Gesellschaft für elektrische Glühlampen mbH | Verfahren zur Rückgewinnung Seltener Erden aus Leuchtstofflampen |
| JP5086021B2 (ja) | 2007-10-03 | 2012-11-28 | Ａｇｃセイミケミカル株式会社 | 稀土類元素の回収方法 |
| CN101244843B (zh) * | 2008-03-18 | 2010-08-18 | 李树昌 | 从氧化钇稳定氧化锆固熔体废物中回收氧化锆及氧化钇的方法 |
| US8936770B2 (en) | 2010-01-22 | 2015-01-20 | Molycorp Minerals, Llc | Hydrometallurgical process and method for recovering metals |
| US8137645B2 (en) | 2010-02-23 | 2012-03-20 | General Electric Company | Rare earth recovery from fluorescent material and associated method |
-
2012
- 2012-12-06 US US13/706,546 patent/US8940256B2/en active Active
- 2012-12-07 CN CN201280069226.6A patent/CN104185606A/zh active Pending
- 2012-12-07 JP JP2014546109A patent/JP2015510541A/ja not_active Withdrawn
- 2012-12-07 KR KR20147018367A patent/KR20140102725A/ko not_active Withdrawn
- 2012-12-07 WO PCT/US2012/068397 patent/WO2013086288A2/en not_active Ceased
- 2012-12-07 EP EP12855747.7A patent/EP2788517A4/en not_active Withdrawn
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