JP2013516180A5 - - Google Patents
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- Publication number
- JP2013516180A5 JP2013516180A5 JP2012547320A JP2012547320A JP2013516180A5 JP 2013516180 A5 JP2013516180 A5 JP 2013516180A5 JP 2012547320 A JP2012547320 A JP 2012547320A JP 2012547320 A JP2012547320 A JP 2012547320A JP 2013516180 A5 JP2013516180 A5 JP 2013516180A5
- Authority
- JP
- Japan
- Prior art keywords
- ion exchange
- carboxylic acid
- exchange resin
- fermentation broth
- succinate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000010633 broth Nutrition 0.000 claims 34
- 238000000855 fermentation Methods 0.000 claims 32
- 230000004151 fermentation Effects 0.000 claims 32
- 238000000034 method Methods 0.000 claims 31
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims 30
- 239000003456 ion exchange resin Substances 0.000 claims 30
- 229920003303 ion-exchange polymer Polymers 0.000 claims 30
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 29
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims 23
- 150000003839 salts Chemical class 0.000 claims 16
- NHJPVZLSLOHJDM-UHFFFAOYSA-N azane;butanedioic acid Chemical compound [NH4+].[NH4+].[O-]C(=O)CCC([O-])=O NHJPVZLSLOHJDM-UHFFFAOYSA-N 0.000 claims 15
- 150000007942 carboxylates Chemical class 0.000 claims 11
- 239000001384 succinic acid Substances 0.000 claims 11
- -1 succinate anion Chemical class 0.000 claims 9
- 230000002378 acidificating effect Effects 0.000 claims 6
- 150000001450 anions Chemical class 0.000 claims 6
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 claims 6
- 238000011282 treatment Methods 0.000 claims 6
- 238000005406 washing Methods 0.000 claims 5
- 239000007864 aqueous solution Substances 0.000 claims 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 239000003513 alkali Substances 0.000 claims 3
- 230000015572 biosynthetic process Effects 0.000 claims 3
- 238000005119 centrifugation Methods 0.000 claims 3
- 238000002425 crystallisation Methods 0.000 claims 3
- 230000008025 crystallization Effects 0.000 claims 3
- 238000004042 decolorization Methods 0.000 claims 3
- 238000000354 decomposition reaction Methods 0.000 claims 3
- 238000010828 elution Methods 0.000 claims 3
- 238000001914 filtration Methods 0.000 claims 3
- 238000005342 ion exchange Methods 0.000 claims 3
- 238000001471 micro-filtration Methods 0.000 claims 3
- 238000007670 refining Methods 0.000 claims 3
- 230000001172 regenerating effect Effects 0.000 claims 3
- 239000000243 solution Substances 0.000 claims 3
- 238000013060 ultrafiltration and diafiltration Methods 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 239000003929 acidic solution Substances 0.000 claims 2
- 125000000129 anionic group Chemical group 0.000 claims 2
- 150000001734 carboxylic acid salts Chemical class 0.000 claims 2
- 150000001768 cations Chemical class 0.000 claims 2
- 238000001704 evaporation Methods 0.000 claims 2
- 239000012071 phase Substances 0.000 claims 2
- 230000008929 regeneration Effects 0.000 claims 2
- 238000011069 regeneration method Methods 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- 239000012670 alkaline solution Substances 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 239000000908 ammonium hydroxide Substances 0.000 claims 1
- 239000008346 aqueous phase Substances 0.000 claims 1
- 150000001735 carboxylic acids Chemical class 0.000 claims 1
- 238000004140 cleaning Methods 0.000 claims 1
- CVOQYKPWIVSMDC-UHFFFAOYSA-L dipotassium;butanedioate Chemical compound [K+].[K+].[O-]C(=O)CCC([O-])=O CVOQYKPWIVSMDC-UHFFFAOYSA-L 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 239000002120 nanofilm Substances 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 239000011347 resin Substances 0.000 claims 1
- 229920005989 resin Polymers 0.000 claims 1
- 229940074404 sodium succinate Drugs 0.000 claims 1
- ZDQYSKICYIVCPN-UHFFFAOYSA-L sodium succinate (anhydrous) Chemical compound [Na+].[Na+].[O-]C(=O)CCC([O-])=O ZDQYSKICYIVCPN-UHFFFAOYSA-L 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US33518909P | 2009-12-31 | 2009-12-31 | |
| US61/335,189 | 2009-12-31 | ||
| PCT/US2010/062635 WO2011082378A2 (en) | 2009-12-31 | 2010-12-31 | Purification of succinic acid from the fermentation broth containing ammonium succinate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2013516180A JP2013516180A (ja) | 2013-05-13 |
| JP2013516180A5 true JP2013516180A5 (https=) | 2014-02-13 |
Family
ID=44227170
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012547320A Pending JP2013516180A (ja) | 2009-12-31 | 2010-12-31 | コハク酸アンモニウムを含有する発酵ブロスからのコハク酸の精製 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US9233906B2 (https=) |
| EP (2) | EP2519491A4 (https=) |
| JP (1) | JP2013516180A (https=) |
| KR (1) | KR20120099154A (https=) |
| CN (1) | CN102781900A (https=) |
| WO (1) | WO2011082378A2 (https=) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010025167A1 (de) * | 2010-06-25 | 2011-12-29 | Uhde Gmbh | Verfahren zur Abtrennung, Gewinnung und Reinigung von Bernsteinsäure |
| DE102011120632A1 (de) * | 2011-12-09 | 2013-06-13 | Thyssenkrupp Uhde Gmbh | Verfahren zur Aufreinigung von Carbonsäuren aus Fermentationsbrühen |
| EP2847342B1 (en) * | 2012-05-07 | 2020-08-12 | Archer Daniels Midland Co. | Purification of succinic acid |
| HUE024575T2 (hu) | 2012-05-24 | 2016-02-29 | Purac Biochem Bv | Karbonsav kinyerése magnézium-karboxilát elegybõl |
| KR101540520B1 (ko) * | 2012-11-29 | 2015-07-30 | 롯데케미칼 주식회사 | 역삼투막을 이용한 숙신산 정제 방법 |
| EP2745905A1 (en) | 2012-12-21 | 2014-06-25 | ThyssenKrupp Uhde GmbH | Process for the purification of carboxylic acids by subcritical or supercritical fluid chromatography |
| DE102013000027A1 (de) * | 2013-01-03 | 2014-07-03 | Thyssenkrupp Industrial Solutions Ag | Verfahren zur Aufreinigung von Carbonsäuren aus Fermentationsbrühen |
| US20160207797A1 (en) * | 2013-08-27 | 2016-07-21 | Purolite Corporation | Ion exchange resin regeneration method |
| CN105705647B (zh) | 2013-09-03 | 2020-03-27 | Ptt全球化学公众有限公司 | 从1，3-丙二醇制造丙烯酸、丙烯腈和1，4-丁二醇的方法 |
| KR102304834B1 (ko) | 2014-02-07 | 2021-09-27 | 바스프 에스이 | 숙신산 생산을 위한 개선된 미생물 |
| KR102304838B1 (ko) | 2014-02-07 | 2021-09-28 | 바스프 에스이 | 개선된 바이오매스 분리 거동을 갖는 변형된 미생물 |
| FR3028864B1 (fr) | 2014-11-26 | 2018-05-18 | Roquette Freres | Procede de recuperation de cristaux d'acide succinique avec mise en œuvre de tensioactifs au cours de la cristallisation, cristaux obtenus et leurs utilisations |
| WO2016164798A1 (en) * | 2015-04-08 | 2016-10-13 | Invista North America S.A.R.L. | Materials and methods for the selective recovery of multivalent products |
| US20160297747A1 (en) * | 2015-04-08 | 2016-10-13 | Invista North America S.A.R.L. | Materials and methods for the selective recovery of monovalent products from aqueous solutions using continuous ion exchange |
| KR20200009010A (ko) | 2017-05-19 | 2020-01-29 | 바스프 에스이 | 유기 화합물 제조 방법 |
| CN109206313B (zh) * | 2017-07-05 | 2021-06-11 | 中国石化扬子石油化工有限公司 | 丁二酸盐厌氧发酵液制备丁二酸的方法 |
| WO2019068642A1 (en) * | 2017-10-02 | 2019-04-11 | Metabolic Explorer | PROCESS FOR PRODUCING ORGANIC ACID SALTS FROM A FERMENTATION BROTH |
| PL236607B1 (pl) * | 2017-11-09 | 2021-02-08 | Politechnika Poznanska | Sposób wydzielania kwasu bursztynowego z brzeczki fermentacyjnej |
| EP3502241A1 (en) | 2017-12-21 | 2019-06-26 | Basf Se | Modified microorganism for improved production of succinate |
| CN113015578B (zh) | 2018-09-18 | 2023-11-21 | 英威达纺织（英国）有限公司 | 用于从水性混合物中回收胺及其衍生物的系统和方法 |
| CN109612978B (zh) * | 2018-10-30 | 2022-02-25 | 欣旺达电子股份有限公司 | 锂离子电池电极膜片补锂量检测方法 |
| CN110194714A (zh) * | 2019-07-02 | 2019-09-03 | 安徽丰原发酵技术工程研究有限公司 | 一种分离苹果酸与丁二酸的方法 |
| CN110204437A (zh) * | 2019-07-02 | 2019-09-06 | 安徽丰原发酵技术工程研究有限公司 | 一种生产l-苹果酸联产丁二酸的方法 |
| US12011146B2 (en) | 2020-04-30 | 2024-06-18 | Ambu A/S | Method of assembly of an endoscope control system |
| US11518762B2 (en) * | 2020-06-04 | 2022-12-06 | Florida State University Research Foundation, Inc. | Large scale purification of castanospermine |
| IT202000017368A1 (it) | 2020-07-16 | 2022-01-16 | Radici Chimica S P A | Purificazione di acidi dicarbossilici alifatici prodotti mediante processi biotecnologici |
| EP4214326A4 (en) * | 2020-09-21 | 2024-11-06 | Lygos, Inc. | CONTINUOUS ION EXCHANGE AND ESTERIFICATION OF FERMENTED MALONIC ACID |
| EP4271423A4 (en) * | 2021-01-04 | 2025-05-14 | Harcros Chemicals Inc. | Antimicrobial compounds based on glucoheptonous acids and their salts |
| US11952609B2 (en) | 2021-03-01 | 2024-04-09 | Battelle Energy Alliance, Llc | Methods of producing succinic acid from a biomass |
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| US5168055A (en) | 1986-06-11 | 1992-12-01 | Rathin Datta | Fermentation and purification process for succinic acid |
| DE3783081T2 (de) | 1986-06-11 | 1993-04-15 | Michigan Biotech Inst | Verfahren zur herstellung von bernsteinsaeure durch anaerobe fermentation. |
| US5143834A (en) * | 1986-06-11 | 1992-09-01 | Glassner David A | Process for the production and purification of succinic acid |
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| US5770435A (en) | 1995-11-02 | 1998-06-23 | University Of Chicago | Mutant E. coli strain with increased succinic acid production |
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| CN1852978A (zh) | 2003-09-17 | 2006-10-25 | 三菱化学株式会社 | 制备无－氨基有机酸的方法 |
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| KR101245428B1 (ko) | 2004-08-27 | 2013-03-19 | 라이스 유니버시티 | 숙신산 생산이 증가된 돌연변이 대장균 균주 |
| ZA200710330B (en) * | 2005-06-17 | 2009-12-30 | Wyeth Corp | Methods of purifying FC region containing proteins |
| JP4193820B2 (ja) | 2005-07-05 | 2008-12-10 | ブラザー工業株式会社 | 管理装置、およびプログラム |
| US8293940B2 (en) | 2005-10-06 | 2012-10-23 | Hyflux IP Resources Pte, Ltd. | Process for recovery and purification of lactic acid |
| JP5088136B2 (ja) | 2005-10-18 | 2012-12-05 | 味の素株式会社 | コハク酸の製造方法 |
| JP5365824B2 (ja) * | 2006-03-23 | 2013-12-11 | 独立行政法人産業技術総合研究所 | コハク酸ジアルキルの製造方法および１，４−ブタンジオールの製造方法 |
| EP1842843A1 (de) | 2006-04-04 | 2007-10-10 | Basf Aktiengesellschaft | Verfahren zur Herstellung eines Carbonsäurealkylesters |
| ES2527402T3 (es) | 2007-03-20 | 2015-01-23 | University Of Florida Research Foundation, Inc. | Materiales y métodos para la producción eficaz de succinato y malato |
| JP3135606U (ja) | 2007-07-12 | 2007-09-20 | 株式会社ノルコーポレーション | 収納フレーム |
| ATE555203T1 (de) | 2007-11-20 | 2012-05-15 | Dsm Ip Assets Bv | Dicarbonsäureproduktion in eukaryonten |
| FR2925068B1 (fr) | 2007-12-13 | 2010-01-08 | Roquette Freres | Procedes de production d'acide succinique |
| KR20090066958A (ko) | 2007-12-20 | 2009-06-24 | 한국과학기술원 | 배양액의 결정화에 의한 숙신산 정제방법 |
| CN101215583B (zh) * | 2008-01-18 | 2010-11-10 | 南京工业大学 | 一种发酵与膜分离单元耦合制备丁二酸的方法 |
| CA2756705C (en) | 2009-04-02 | 2017-04-11 | University Of Florida Research Foundation, Inc. | Engineered bacterial cells for succinate production |
| US20120238722A1 (en) * | 2009-11-24 | 2012-09-20 | Roquette Freres Sa | Process for the crystallization of succinic acid |
-
2010
- 2010-12-31 JP JP2012547320A patent/JP2013516180A/ja active Pending
- 2010-12-31 CN CN201080059513XA patent/CN102781900A/zh active Pending
- 2010-12-31 US US13/519,491 patent/US9233906B2/en not_active Expired - Fee Related
- 2010-12-31 KR KR1020127020082A patent/KR20120099154A/ko not_active Ceased
- 2010-12-31 WO PCT/US2010/062635 patent/WO2011082378A2/en not_active Ceased
- 2010-12-31 EP EP10841777.5A patent/EP2519491A4/en not_active Withdrawn
- 2010-12-31 EP EP15000821.7A patent/EP2918574A1/en not_active Withdrawn
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