JP2013513010A5 - - Google Patents
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- Publication number
- JP2013513010A5 JP2013513010A5 JP2012543099A JP2012543099A JP2013513010A5 JP 2013513010 A5 JP2013513010 A5 JP 2013513010A5 JP 2012543099 A JP2012543099 A JP 2012543099A JP 2012543099 A JP2012543099 A JP 2012543099A JP 2013513010 A5 JP2013513010 A5 JP 2013513010A5
- Authority
- JP
- Japan
- Prior art keywords
- group
- trifluoroethenyl
- oxy
- methyl
- tetrafluoroethoxy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- -1 Perfluoro Chemical group 0.000 claims description 38
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 28
- 239000000178 monomer Substances 0.000 claims description 28
- PQIOSYKVBBWRRI-UHFFFAOYSA-N methylphosphonyl difluoride Chemical group CP(F)(F)=O PQIOSYKVBBWRRI-UHFFFAOYSA-N 0.000 claims description 24
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 24
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims description 18
- 229920005573 silicon-containing polymer Polymers 0.000 claims description 14
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 10
- JMGNVALALWCTLC-UHFFFAOYSA-N 1-fluoro-2-(2-fluoroethenoxy)ethene Chemical compound FC=COC=CF JMGNVALALWCTLC-UHFFFAOYSA-N 0.000 claims description 8
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims description 8
- 125000004432 carbon atom Chemical group C* 0.000 claims description 8
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 claims description 8
- 229920002313 fluoropolymer Polymers 0.000 claims description 8
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 claims description 8
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims description 8
- 125000006551 perfluoro alkylene group Chemical group 0.000 claims description 8
- FVSKHRXBFJPNKK-UHFFFAOYSA-N propionitrile Chemical compound CCC#N FVSKHRXBFJPNKK-UHFFFAOYSA-N 0.000 claims description 8
- UKRDPEFKFJNXQM-UHFFFAOYSA-N vinylsilane Chemical compound [SiH3]C=C UKRDPEFKFJNXQM-UHFFFAOYSA-N 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 5
- 125000006273 (C1-C3) alkyl group Chemical group 0.000 claims description 4
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical group [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- LKJPYSCBVHEWIU-UHFFFAOYSA-N N-[4-cyano-3-(trifluoromethyl)phenyl]-3-[(4-fluorophenyl)sulfonyl]-2-hydroxy-2-methylpropanamide Chemical compound C=1C=C(C#N)C(C(F)(F)F)=CC=1NC(=O)C(O)(C)CS(=O)(=O)C1=CC=C(F)C=C1 LKJPYSCBVHEWIU-UHFFFAOYSA-N 0.000 claims description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 claims description 4
- OIBMEBLCOQCFIT-UHFFFAOYSA-N ethanesulfonyl fluoride Chemical compound CCS(F)(=O)=O OIBMEBLCOQCFIT-UHFFFAOYSA-N 0.000 claims description 4
- AILKHAQXUAOOFU-UHFFFAOYSA-N hexanenitrile Chemical compound CCCCCC#N AILKHAQXUAOOFU-UHFFFAOYSA-N 0.000 claims description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- OVAULROCPRKKJF-UHFFFAOYSA-N methyl 2,2,3,3-tetrafluoro-3-[1,1,1,2,3,3-hexafluoro-3-(1,2,2-trifluoroethenoxy)propan-2-yl]oxypropanoate Chemical compound COC(=O)C(F)(F)C(F)(F)OC(F)(C(F)(F)F)C(F)(F)OC(F)=C(F)F OVAULROCPRKKJF-UHFFFAOYSA-N 0.000 claims description 4
- DUWWHGPELOTTOE-UHFFFAOYSA-N n-(5-chloro-2,4-dimethoxyphenyl)-3-oxobutanamide Chemical compound COC1=CC(OC)=C(NC(=O)CC(C)=O)C=C1Cl DUWWHGPELOTTOE-UHFFFAOYSA-N 0.000 claims description 4
- 125000005010 perfluoroalkyl group Chemical group 0.000 claims description 4
- 229910052698 phosphorus Inorganic materials 0.000 claims description 4
- 239000011574 phosphorus Substances 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 4
- 235000019260 propionic acid Nutrition 0.000 claims description 4
- 150000003376 silicon Chemical class 0.000 claims description 4
- 239000003638 chemical reducing agent Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 description 11
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 229940098779 methanesulfonic acid Drugs 0.000 description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 2
- CSJWOWRPMBXQLD-UHFFFAOYSA-N perfluoromethylvinylether group Chemical group FC(=C(C(F)(F)F)F)OC(=C(F)C(F)(F)F)F CSJWOWRPMBXQLD-UHFFFAOYSA-N 0.000 description 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 2
- ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000000010 aprotic solvent Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000012280 lithium aluminium hydride Substances 0.000 description 1
- MJGFBOZCAJSGQW-UHFFFAOYSA-N mercury sodium Chemical compound [Na].[Hg] MJGFBOZCAJSGQW-UHFFFAOYSA-N 0.000 description 1
- 229910001023 sodium amalgam Inorganic materials 0.000 description 1
- 239000012279 sodium borohydride Substances 0.000 description 1
- 229910000033 sodium borohydride Inorganic materials 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- DBGVGMSCBYYSLD-UHFFFAOYSA-N tributylstannane Chemical compound CCCC[SnH](CCCC)CCCC DBGVGMSCBYYSLD-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/632,982 | 2009-12-08 | ||
| US12/632,982 US8138274B2 (en) | 2009-12-08 | 2009-12-08 | Process for preparation of fluorosilicon polymer |
| PCT/US2010/053319 WO2011071599A2 (en) | 2009-12-08 | 2010-10-20 | Process for preparation of fluorosilicon polymer |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013513010A JP2013513010A (ja) | 2013-04-18 |
| JP2013513010A5 true JP2013513010A5 (enExample) | 2013-11-14 |
| JP5635124B2 JP5635124B2 (ja) | 2014-12-03 |
Family
ID=44082648
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012543099A Expired - Fee Related JP5635124B2 (ja) | 2009-12-08 | 2010-10-20 | フルオロシリコンポリマーの調製方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8138274B2 (enExample) |
| EP (1) | EP2510045A4 (enExample) |
| JP (1) | JP5635124B2 (enExample) |
| KR (1) | KR20120129883A (enExample) |
| CN (1) | CN102782015B (enExample) |
| WO (1) | WO2011071599A2 (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9012025B2 (en) * | 2012-04-05 | 2015-04-21 | Xerox Corporation | Fuser member |
| JP6478988B2 (ja) | 2013-06-25 | 2019-03-06 | スリーエム イノベイティブ プロパティズ カンパニー | 湿気硬化性組成物、使用法、及び複合物品 |
| US10213993B2 (en) * | 2013-12-19 | 2019-02-26 | 3M Innovative Properties Company | Multilayer composite article |
| US9994676B2 (en) | 2014-06-23 | 2018-06-12 | 3M Innovative Properties Company | Silicon-containing polymer and method of making a silicon-containing polymer |
| CN104558364B (zh) * | 2014-12-31 | 2017-05-03 | 山东华夏神舟新材料有限公司 | 含氟弹性体及其制备方法 |
| WO2021094884A1 (en) * | 2019-11-13 | 2021-05-20 | 3M Innovative Properties Company | A method of functionalizing fluorinated polymers, a functionalized fluorinated polymer and coating compositions thereof |
| CN115093501A (zh) * | 2022-07-01 | 2022-09-23 | 北京化工大学 | 一种碘封端低分子量全氟弹性体、其制备方法及应用 |
| CN117946346A (zh) * | 2023-12-15 | 2024-04-30 | 中昊晨光化工研究院有限公司 | 一种改性乙烯-四氟乙烯共聚物及其制备方法 |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2637738A (en) * | 1949-09-17 | 1953-05-05 | Union Carbide & Carbon Corp | Reaction of silanes with aliphatic unsaturated compounds |
| JPS53125491A (en) * | 1977-04-08 | 1978-11-01 | Daikin Ind Ltd | Fluorine-containing polymer easily curable and its curable composition |
| JPS5657811A (en) * | 1979-10-17 | 1981-05-20 | Daikin Ind Ltd | Preparation of liquid fluorine-containing polymer |
| US4579965A (en) * | 1985-01-24 | 1986-04-01 | Union Carbide Corporation | Process for preparing vinyl-tri-(tertiary substituted) alkoxysilanes |
| JPH0725850B2 (ja) * | 1987-03-06 | 1995-03-22 | 日本メクトロン株式会社 | 含フツ素共重合体の製造方法 |
| JP2705105B2 (ja) * | 1988-05-21 | 1998-01-26 | ダイキン工業株式会社 | 新規ポリマーおよびその製法と用途 |
| JPH02115234A (ja) * | 1988-10-26 | 1990-04-27 | Tdk Corp | 架橋ポリフッ化ビニリデンの製造方法 |
| US5077362A (en) * | 1989-03-28 | 1991-12-31 | Shin-Etsu Chemical Co., Ltd. | Vinylidene fluoride copolymer and process for producing the same |
| US5041588A (en) * | 1989-07-03 | 1991-08-20 | Dow Corning Corporation | Chemically reactive fluorinated organosilicon compounds and their polymers |
| US5041595A (en) * | 1990-09-26 | 1991-08-20 | Union Carbide Chemicals And Plastics Technology Corporation | Method for manufacturing vinylalkoxysilanes |
| JPH05261786A (ja) * | 1992-03-23 | 1993-10-12 | Sumitomo Bakelite Co Ltd | ポリオレフィン系樹脂の押出成形物の製造方法 |
| US5208305A (en) * | 1992-04-17 | 1993-05-04 | Minnesota Mining And Manufacturing Company | Fluorine-containing polymers and preparation and use thereof |
| US5290900A (en) * | 1992-04-27 | 1994-03-01 | Dow Corning Toray Silicone, Ltd. | Curable fluorosilicone resin composition |
| JPH07265686A (ja) * | 1994-03-29 | 1995-10-17 | Kansai Shin Gijutsu Kenkyusho:Kk | 均一粒径粒子及びその製造方法 |
| US5919878A (en) | 1996-09-13 | 1999-07-06 | E. I. Du Pont De Nemours And Company | Amorphous fluoropolymer containing perfluoro(ethyl vinyl ether) |
| WO1998055557A1 (en) * | 1997-06-06 | 1998-12-10 | Daikin Industries, Ltd. | Fluorochemical adhesive and adhesive film and laminate made by using the same |
| US20020032292A1 (en) * | 1999-02-05 | 2002-03-14 | Sunao Ikeda | Fluoroelastomer and production thereof |
| CN1336938A (zh) * | 1999-11-12 | 2002-02-20 | 阿托费纳化学股份有限公司 | 包含有机硅烷的含氟聚合物及其制备方法 |
| JP4352546B2 (ja) * | 1999-12-22 | 2009-10-28 | ユニマテック株式会社 | フルオロエラストマー、その製造方法、架橋性組成物およびその硬化物 |
| JP2003527468A (ja) * | 1999-12-29 | 2003-09-16 | ハイドロ−ケベック | 低いＴｇを有し、ビニリデンフルオライドを主成分とし、かつテトラフルオロエチレンもシロキサン基も含まないフルオロエラストマー |
| US6359089B2 (en) * | 2000-04-19 | 2002-03-19 | Dupont Dow Elastomers, L.L.C. | Fluorovinyl ether cure site monomers and fluoroelastomer copolymer compositions thereof |
| US6479610B1 (en) * | 2000-07-27 | 2002-11-12 | General Electric Company | Polyfunctional fluorosilicone composition, method for making, and use |
| CN100338108C (zh) | 2002-03-14 | 2007-09-19 | 大金工业株式会社 | 含氟共聚物、含氟共聚物制造方法、含氟共聚物固化用组合物和固化物 |
| JP4491547B2 (ja) | 2002-04-23 | 2010-06-30 | Ｎｏｋ株式会社 | 含フッ素エラストマー組成物 |
| JP4517229B2 (ja) * | 2004-08-03 | 2010-08-04 | ナガセケムテックス株式会社 | シルセスキオキサン含有化合物及びその製造方法 |
| DE602005018228D1 (de) * | 2004-08-04 | 2010-01-21 | Asahi Glass Co Ltd | Elastomeres fluorcopolymer, dieses enthaltende zusammensetzung und vernetzte kautschuke |
| WO2006038424A1 (ja) * | 2004-10-04 | 2006-04-13 | Unimatec Co., Ltd. | 含フッ素共重合体架橋成形品 |
| JPWO2006057203A1 (ja) | 2004-11-25 | 2008-06-05 | ユニマテック株式会社 | 含フッ素共重合体 |
| EP2094748B1 (en) * | 2006-12-21 | 2012-10-17 | E.I. Du Pont De Nemours And Company | Crosslinkable vinyl fluoride copolymer coated film and process for making same |
| US8288492B2 (en) * | 2007-10-23 | 2012-10-16 | E I Du Pont De Nemours And Company | Difunctional oligomers of perfluoro(methyl vinyl ether) |
-
2009
- 2009-12-08 US US12/632,982 patent/US8138274B2/en not_active Expired - Fee Related
-
2010
- 2010-10-20 KR KR1020127017616A patent/KR20120129883A/ko not_active Withdrawn
- 2010-10-20 JP JP2012543099A patent/JP5635124B2/ja not_active Expired - Fee Related
- 2010-10-20 EP EP10836370.6A patent/EP2510045A4/en not_active Withdrawn
- 2010-10-20 CN CN201080055743.9A patent/CN102782015B/zh not_active Expired - Fee Related
- 2010-10-20 WO PCT/US2010/053319 patent/WO2011071599A2/en not_active Ceased
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