JP2013256661A - 複合シート、その製造方法及びこれを含むディスプレイ基板 - Google Patents
複合シート、その製造方法及びこれを含むディスプレイ基板 Download PDFInfo
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- C08J2383/14—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
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- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
- Y10T442/10—Scrim [e.g., open net or mesh, gauze, loose or open weave or knit, etc.]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y10T442/00—Fabric [woven, knitted, or nonwoven textile or cloth, etc.]
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- Y10T442/2926—Coated or impregnated inorganic fiber fabric
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Abstract
【解決手段】本発明の複合シートは、マトリックス;及び前記マトリックス内に含浸された補強材を含み、前記複合シートは、数式1による350℃における質量変化率(△W)が98%以上で、100μNで測定した緩和弾性率が1000MPa以下であることを特徴とする。複合シートは、350℃以上の高温環境で環変形及び熱分解が抑制されるため、基板製作時の高温工程で発生し得る材料の不良を改善できる。
【選択図】図1
Description
テトラメチルシクロテトラシロキサンを直鎖のビニル末端ポリオルガノシロキサンであるDMS−V03(Gelest Inc.,MW500,DP5)と2:1の当量比で混合した後、ボルテックスミキサーを用いてよく混ぜ合わせた。前記混合物をD−glass系ガラス繊維(Nittobo社製造,製品名3313)に含浸した後、離型処理がされたガラス基板間に入れ、粘度が増加するまで常温で24時間放置した。その後、上段面をガラス基板で覆い、ラミネーターを用いて余分な樹脂を除去し、100℃のオーブンで4時間熱硬化して透明なシリコーン複合シートを生成した。
ビニル末端ポリオルガノシロキサンとして、DMS−V03の代わりにDMS−V05(Gelest Inc.,MW800,DP9)を使用したことを除いて、実施例1と同様に行った。
ビニル末端ポリオルガノシロキサンとして、DMS−V03の代わりにDMS−V21(Gelest Inc.,MW6000,DP65)を使用したことを除いて、実施例1と同様に行った。
Dow Corning社で製造したポリオルガノシロキサンであるSylgard184 AパートとBパートを1:10の質量比で混合した後、ボルテックスミキサーを用いてよく混ぜ合わせた。前記混合物をE−glass系ガラス繊維(Nittobo社製造,製品名3313)に含浸した後、離型処理がされたガラス基板間に入れ、ラミネーターを用いて余分な樹脂を除去した後、100℃のオーブンで4時間熱硬化して透明なシリコーン複合シートを生成した。
ビニル末端ポリオルガノシロキサンとして、テトラビニルテトラメチルシクロテトラシロキサンを使用したことを除いて、実施例1と同様に行った。
(1)熱安定性:Mettler toledo社のTGA/DSC1 Thermogravimetric Analysisを用いて50mgのサンプルをロードした後、25℃〜350℃の温度区間を5℃/分の条件で窒素雰囲気下において昇温し、質量減量を測定した。初期質量と、250℃の場合、300℃の場合、及び350℃の場合のそれぞれに対して質量を測定し、下記数式によって質量変化率(△W)を求めた。
Claims (14)
- 前記マトリックスは、環状シロキサンを含むシリコーン系樹脂を含むことを特徴とする、請求項1に記載の複合シート。
- 前記マトリックスは、環状シロキサンと直鎖の末端ビニル基含有ポリシロキサンの反応物を含むことを特徴とする、請求項1に記載の複合シート。
- 前記環状シロキサンと前記直鎖の末端ビニル基含有ポリシロキサンのモル当量比は、0.5:1〜2.5:1であることを特徴とする、請求項3に記載の複合シート。
- 550nm波長における透過度が90%以上である、請求項1に記載の複合シート。
- ASTM D522による耐屈曲性が5mm未満であり、熱膨張係数(CTE)が10ppm/K未満である、請求項1に記載の複合シート。
- 前記補強材は、ガラス繊維布(glass fiber cloth)、ガラス織物(glass fibric)、ガラス不織布及びガラスメッシュ(glass mesh)からなる群から選ばれる1種以上を含むことを特徴とする、請求項1に記載の複合シート。
- 環状シロキサンと直鎖の末端ビニル基含有ポリシロキサンを含むマトリックス用組成物を製造し;
前記マトリックス用組成物に補強材を含浸し硬化させることを含む、複合シートの製造方法。 - 前記環状シロキサンと前記直鎖の末端ビニル基含有ポリシロキサンのモル当量比は、0.5:1〜2.5:1であることを特徴とする、請求項10に記載の方法。
- 請求項1に記載の複合シートを含むディスプレイ基板。
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Application Number | Priority Date | Filing Date | Title |
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KR1020120062916A KR101518497B1 (ko) | 2012-06-12 | 2012-06-12 | 복합시트, 그 제조방법 및 이를 포함하는 디스플레이 기판 |
KR10-2012-0062916 | 2012-06-12 |
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JP2013256661A true JP2013256661A (ja) | 2013-12-26 |
JP6321331B2 JP6321331B2 (ja) | 2018-05-09 |
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JP2013122603A Active JP6321331B2 (ja) | 2012-06-12 | 2013-06-11 | 複合シート、その製造方法及びこれを含むディスプレイ基板 |
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US (1) | US20130330989A1 (ja) |
EP (1) | EP2674448A1 (ja) |
JP (1) | JP6321331B2 (ja) |
KR (1) | KR101518497B1 (ja) |
CN (1) | CN103481608B (ja) |
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KR101575440B1 (ko) * | 2013-12-30 | 2015-12-07 | 코오롱인더스트리 주식회사 | 수지층 형성용 조성물 및 이를 이용한 플렉서블 디스플레이 기판 |
KR20150078583A (ko) * | 2013-12-31 | 2015-07-08 | 코오롱인더스트리 주식회사 | 수지 조성물 및 이를 이용한 플렉서블 디스플레이 기판 |
US10669197B2 (en) * | 2014-01-14 | 2020-06-02 | Shin-Etsu Chemical Co., Ltd. | Surface-modified glass fiber film |
DE102016115907A1 (de) | 2016-08-26 | 2018-03-01 | Osram Opto Semiconductors Gmbh | Optoelektronisches Bauelement und Verfahren zur Herstellung eines optoelektronischen Bauelements |
CN114063389A (zh) * | 2020-07-31 | 2022-02-18 | 华为技术有限公司 | 图案化材料和图案化薄膜 |
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JPS496160B1 (ja) * | 1970-12-14 | 1974-02-12 | ||
JPS5263495A (en) * | 1975-11-19 | 1977-05-25 | Toshiba Silicone | Treatment of fire retarding glass fiber fabric |
JPS6213453A (ja) * | 1985-07-12 | 1987-01-22 | Shin Etsu Chem Co Ltd | 硬化性オルガノポリシロキサン組成物 |
JPH0551873A (ja) * | 1991-08-19 | 1993-03-02 | Shin Etsu Chem Co Ltd | ガラス繊維織物の処理剤 |
JP2008530340A (ja) * | 2005-02-16 | 2008-08-07 | ダウ・コーニング・コーポレイション | 強化シリコーン樹脂フィルムおよびその製造方法 |
JP2008201971A (ja) * | 2007-02-22 | 2008-09-04 | Shin Etsu Chem Co Ltd | 繊維強化複合材料用液状付加硬化性シリコーン組成物、繊維強化シリコーン複合材料およびその製造方法 |
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JP2011068787A (ja) * | 2009-09-25 | 2011-04-07 | Sekisui Chem Co Ltd | 透明複合材料及び透明シート |
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JP4219843B2 (ja) | 2004-04-08 | 2009-02-04 | 信越化学工業株式会社 | 硬化性シロキサン系組成物 |
US8092910B2 (en) * | 2005-02-16 | 2012-01-10 | Dow Corning Toray Co., Ltd. | Reinforced silicone resin film and method of preparing same |
US8048977B2 (en) | 2006-04-28 | 2011-11-01 | E. I. Du Pont De Nemours And Company | Organosilicon polymers |
JP2011246652A (ja) * | 2010-05-28 | 2011-12-08 | Kaneka Corp | ポリシロキサン系組成物 |
US20120029157A1 (en) * | 2010-07-29 | 2012-02-02 | Woo-Han Kim | Modified siloxane polymer composition, encapsulant obtained from the modified siloxane polymer composition, and electronic device including the encapsulant |
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2012
- 2012-06-12 KR KR1020120062916A patent/KR101518497B1/ko not_active IP Right Cessation
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2013
- 2013-06-11 EP EP20130171396 patent/EP2674448A1/en not_active Withdrawn
- 2013-06-11 JP JP2013122603A patent/JP6321331B2/ja active Active
- 2013-06-12 US US13/915,975 patent/US20130330989A1/en not_active Abandoned
- 2013-06-13 CN CN201310232685.8A patent/CN103481608B/zh not_active Expired - Fee Related
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS496160B1 (ja) * | 1970-12-14 | 1974-02-12 | ||
JPS5263495A (en) * | 1975-11-19 | 1977-05-25 | Toshiba Silicone | Treatment of fire retarding glass fiber fabric |
JPS6213453A (ja) * | 1985-07-12 | 1987-01-22 | Shin Etsu Chem Co Ltd | 硬化性オルガノポリシロキサン組成物 |
JPH0551873A (ja) * | 1991-08-19 | 1993-03-02 | Shin Etsu Chem Co Ltd | ガラス繊維織物の処理剤 |
JP2008530340A (ja) * | 2005-02-16 | 2008-08-07 | ダウ・コーニング・コーポレイション | 強化シリコーン樹脂フィルムおよびその製造方法 |
JP2009503230A (ja) * | 2005-08-04 | 2009-01-29 | ダウ・コーニング・コーポレイション | 強化シリコーン樹脂フィルムおよびその製造方法 |
JP2008201971A (ja) * | 2007-02-22 | 2008-09-04 | Shin Etsu Chem Co Ltd | 繊維強化複合材料用液状付加硬化性シリコーン組成物、繊維強化シリコーン複合材料およびその製造方法 |
JP2011068787A (ja) * | 2009-09-25 | 2011-04-07 | Sekisui Chem Co Ltd | 透明複合材料及び透明シート |
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Publication number | Publication date |
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CN103481608A (zh) | 2014-01-01 |
CN103481608B (zh) | 2017-04-26 |
JP6321331B2 (ja) | 2018-05-09 |
EP2674448A1 (en) | 2013-12-18 |
KR20130139133A (ko) | 2013-12-20 |
US20130330989A1 (en) | 2013-12-12 |
KR101518497B1 (ko) | 2015-05-11 |
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