JP2013241601A - 液晶媒体 - Google Patents
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- JP2013241601A JP2013241601A JP2013124215A JP2013124215A JP2013241601A JP 2013241601 A JP2013241601 A JP 2013241601A JP 2013124215 A JP2013124215 A JP 2013124215A JP 2013124215 A JP2013124215 A JP 2013124215A JP 2013241601 A JP2013241601 A JP 2013241601A
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- 239000004973 liquid crystal related substance Substances 0.000 title claims abstract description 62
- 150000001875 compounds Chemical class 0.000 claims abstract description 118
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 54
- 125000003342 alkenyl group Chemical group 0.000 claims abstract description 28
- 229910052731 fluorine Inorganic materials 0.000 claims abstract description 28
- 125000003545 alkoxy group Chemical group 0.000 claims abstract description 15
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 12
- 125000004432 carbon atom Chemical group C* 0.000 claims description 49
- -1 oxaalkyl Chemical group 0.000 claims description 23
- 125000003709 fluoroalkyl group Chemical group 0.000 claims description 4
- 125000003302 alkenyloxy group Chemical group 0.000 claims description 3
- 125000005843 halogen group Chemical group 0.000 claims description 3
- 125000001140 1,4-phenylene group Chemical group [H]C1=C([H])C([*:2])=C([H])C([H])=C1[*:1] 0.000 claims description 2
- 239000012963 UV stabilizer Substances 0.000 claims description 2
- 239000000654 additive Substances 0.000 claims description 2
- 239000003963 antioxidant agent Substances 0.000 claims description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 2
- 125000004430 oxygen atom Chemical group O* 0.000 claims description 2
- 125000005407 trans-1,4-cyclohexylene group Chemical group [H]C1([H])C([H])([H])[C@]([H])([*:2])C([H])([H])C([H])([H])[C@@]1([H])[*:1] 0.000 claims description 2
- 230000004044 response Effects 0.000 abstract description 12
- 239000000203 mixture Substances 0.000 description 42
- 210000004027 cell Anatomy 0.000 description 22
- 230000003287 optical effect Effects 0.000 description 13
- 239000011159 matrix material Substances 0.000 description 12
- 239000000460 chlorine Substances 0.000 description 11
- 239000000463 material Substances 0.000 description 11
- 0 *CCCCC(C(C1)=C)=CC=C1c(cc1)ccc1N=C Chemical compound *CCCCC(C(C1)=C)=CC=C1c(cc1)ccc1N=C 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- 239000011737 fluorine Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 239000000758 substrate Substances 0.000 description 6
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 4
- 238000013461 design Methods 0.000 description 4
- 239000002019 doping agent Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 125000001153 fluoro group Chemical group F* 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 229910052736 halogen Inorganic materials 0.000 description 3
- 229910052740 iodine Inorganic materials 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- 230000007704 transition Effects 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- RPMUDXVQHUECRE-UHFFFAOYSA-N CC1COC(C)OC1 Chemical compound CC1COC(C)OC1 RPMUDXVQHUECRE-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 239000004990 Smectic liquid crystal Substances 0.000 description 2
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000005684 electric field Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
- 150000002367 halogens Chemical class 0.000 description 2
- 125000003187 heptyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 229910021420 polycrystalline silicon Inorganic materials 0.000 description 2
- 229920001690 polydopamine Polymers 0.000 description 2
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 125000001424 substituent group Chemical group 0.000 description 2
- 238000009281 ultraviolet germicidal irradiation Methods 0.000 description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- HNEGJTWNOOWEMH-UHFFFAOYSA-N 1-fluoropropane Chemical group [CH2]CCF HNEGJTWNOOWEMH-UHFFFAOYSA-N 0.000 description 1
- AUXIEQKHXAYAHG-UHFFFAOYSA-N 1-phenylcyclohexane-1-carbonitrile Chemical compound C=1C=CC=CC=1C1(C#N)CCCCC1 AUXIEQKHXAYAHG-UHFFFAOYSA-N 0.000 description 1
- 125000004777 2-fluoroethyl group Chemical group [H]C([H])(F)C([H])([H])* 0.000 description 1
- 125000004975 3-butenyl group Chemical group C(CC=C)* 0.000 description 1
- 125000006043 5-hexenyl group Chemical group 0.000 description 1
- RSOILICUEWXSLA-UHFFFAOYSA-N CC(C)(C1)N(C)C(C)(C)CC1OC(CCCCCCCCC(OC1CC(C)(C)N(C)C(C)(C)C1)=O)=O Chemical compound CC(C)(C1)N(C)C(C)(C)CC1OC(CCCCCCCCC(OC1CC(C)(C)N(C)C(C)(C)C1)=O)=O RSOILICUEWXSLA-UHFFFAOYSA-N 0.000 description 1
- SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 1
- 229940123457 Free radical scavenger Drugs 0.000 description 1
- 239000004988 Nematic liquid crystal Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 241000620457 Telestes souffia Species 0.000 description 1
- 206010047571 Visual impairment Diseases 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910021417 amorphous silicon Inorganic materials 0.000 description 1
- UHYPYGJEEGLRJD-UHFFFAOYSA-N cadmium(2+);selenium(2-) Chemical compound [Se-2].[Cd+2] UHYPYGJEEGLRJD-UHFFFAOYSA-N 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 description 1
- 230000003098 cholesteric effect Effects 0.000 description 1
- 238000004883 computer application Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 125000004956 cyclohexylene group Chemical group 0.000 description 1
- 125000002704 decyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000005670 electromagnetic radiation Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000001301 ethoxy group Chemical group [H]C([H])([H])C([H])([H])O* 0.000 description 1
- 125000005745 ethoxymethyl group Chemical group [H]C([H])([H])C([H])([H])OC([H])([H])* 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 125000005817 fluorobutyl group Chemical group [H]C([H])(F)C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000004216 fluoromethyl group Chemical group [H]C([H])(F)* 0.000 description 1
- 238000012826 global research Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000005446 heptyloxy group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])O* 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 210000004263 induced pluripotent stem cell Anatomy 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 125000004184 methoxymethyl group Chemical group [H]C([H])([H])OC([H])([H])* 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910021421 monocrystalline silicon Inorganic materials 0.000 description 1
- 125000001421 myristyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 231100000989 no adverse effect Toxicity 0.000 description 1
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000005693 optoelectronics Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 125000002958 pentadecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000003230 pyrimidines Chemical class 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 description 1
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000002948 undecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
- C09K19/06—Non-steroidal liquid crystal compounds
- C09K19/34—Non-steroidal liquid crystal compounds containing at least one heterocyclic ring
- C09K19/3402—Non-steroidal liquid crystal compounds containing at least one heterocyclic ring having oxygen as hetero atom
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
- C09K19/42—Mixtures of liquid crystal compounds covered by two or more of the preceding groups C09K19/06 - C09K19/40
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
- C09K19/06—Non-steroidal liquid crystal compounds
- C09K19/34—Non-steroidal liquid crystal compounds containing at least one heterocyclic ring
- C09K19/3402—Non-steroidal liquid crystal compounds containing at least one heterocyclic ring having oxygen as hetero atom
- C09K2019/3422—Non-steroidal liquid crystal compounds containing at least one heterocyclic ring having oxygen as hetero atom the heterocyclic ring being a six-membered ring
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2323/00—Functional layers of liquid crystal optical display excluding electroactive liquid crystal layer characterised by chemical composition
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- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Liquid Crystal Substances (AREA)
Abstract
【解決手段】式(I)の1種類以上の化合物を含有する液晶媒体、および、電気光学的液晶ディスプレイにおけるそれの使用にも関する。
式中、R0は、1〜15個のC原子を有するアルキルまたはアルコキシ基を表し、X0は、F、Cl、CN、SF5、SCN、NCS、6個までのC原子を有するハロゲン化されたアルキル基、ハロゲン化されたアルケニル基、ハロゲン化されたアルコキシ基またはハロゲン化されたアルケニルオキシ基を表し、およびL1〜6は、それぞれ互いに独立に、HまたはFを表す。)
【選択図】なし
Description
1.基板としてのシリコンウエハー上のMOS(金属酸化物半導体:metal oxide semiconductor)または他のダイオード、
2.基板としてのガラスプレート上の薄膜トランジスター(TFT:thin−film transistor)。
−広げられたネマチック相範囲(特に、低い温度まで)
−極めて低温におけるスイッチ能力(屋外用途、自動車、航空機)
−UV照射に対する増大された耐性(より長い寿命)
−低い閾電圧。
R0は、1〜15個のC原子を有するアルキルまたはアルコキシ基を表し、ただし加えて、これらの基における1個以上のCH2基は、それぞれ互いに独立に、O原子が互いに直接つながらないようにして、−C≡C−、−CF2O−、−CH=CH−、
X0は、F、Cl、CN、SF5、SCN、NCS、6個までのC原子を有するハロゲン化されたアルキル基、ハロゲン化されたアルケニル基、ハロゲン化されたアルコキシ基またはハロゲン化されたアルケニルオキシ基を表し、および
L1〜6は、それぞれ互いに独立に、HまたはFを表す。
Aは、1,4−フェニレンまたはトランス−1,4−シクロヘキシレンを表し、
aは、0または1であり、および
R3は、2〜9個のC原子を有するアルケニルを表し、
および、R4は式I中のR0について示される意味を有し、好ましくは1〜12個のC原子を有するアルキルまたは2〜9個のC原子を有するアルケニルを表す。
R0およびX0は、式Iにおいて示される意味を有し、および
Y1〜6は、それぞれ互いに独立に、HまたはFを表し、
Z0は、−C2H4−、−(CH2)4−、−CH=CH−、−CF=CF−、−C2F4−、−CH2CF2−、−CF2CH2−、−CH2O−、−OCH2−、−COO−、−CF2O−または−OCF2−を表し、式VおよびVIにおいては単結合も表し、および
rは、0または1を表す。
alkylおよびalkyl*は、それぞれ互いに独立に、1〜6個のC原子を有する直鎖状のアルキル基を表し、および
alkenylおよびalkenyl*は、それぞれ互いに独立に、2〜6個のC原子を有する直鎖状のアルケニル基を表す。
Conference、サンフランシスコ、1984年6月、第304頁(1984年);G.Weberら、Liquid Crystals、第5巻、第1381頁(1989年)]によって、下式
−Δnは、589nmおよび20℃における光学的異方性を表わし、
−γ1は、20℃における回転粘度(mPa・s)を表わし、
−V10は、10%透過(基板表面に垂直な視角)における電圧(V)を表し(閾電圧)、
−Δεは、20℃および1kHzにおける誘電異方性(Δε=ε‖ε−ε⊥、ここでε‖は分子の長軸に平行な誘電率、ε⊥はそれに垂直な誘電率を表す)を表す。
Claims (15)
- 式Iの1種類以上の化合物を含むことを特徴とする液晶媒体。
R0は、1〜15個のC原子を有するアルキルまたはアルコキシ基を表し、ただし加えて、これらの基における1個以上のCH2基は、それぞれ互いに独立に、O原子が互いに直接つながらないようにして、−C≡C−、−CF2O−、−CH=CH−、
X0は、F、Cl、CN、SF5、SCN、NCS、6個までのC原子を有するハロゲン化されたアルキル基、ハロゲン化されたアルケニル基、ハロゲン化されたアルコキシ基またはハロゲン化されたアルケニルオキシ基を表し、および
L1〜6は、それぞれ互いに独立に、HまたはFを表す。) - 1〜25重量%の式Iの化合物を含むことを特徴とする請求項1〜10のいずれか一項に記載の液晶媒体。
- 1種類以上のUV安定化剤および/または抗酸化剤を追加的に含むことを特徴とする請求項1〜11のいずれか一項に記載の液晶媒体。
- 電気光学的目的のための請求項1〜12のいずれか一項に記載の液晶媒体の使用。
- 請求項1〜12のいずれか一項に記載の液晶媒体を含有する電気光学的液晶ディスプレイ。
- 式Iの1種類以上の化合物を、少なくとも1種類の更なる液晶化合物および任意成分としての添加剤と混合することを特徴とする請求項1〜12のいずれか一項に記載の液晶媒体を調製する方法。
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DE102008010193.1 | 2008-02-20 | ||
DE102008010193 | 2008-02-20 |
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JP2010547098A Division JP5542695B2 (ja) | 2008-02-20 | 2009-02-18 | 液晶媒体 |
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JP2013241601A true JP2013241601A (ja) | 2013-12-05 |
JP5917445B2 JP5917445B2 (ja) | 2016-05-11 |
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JP2010547098A Active JP5542695B2 (ja) | 2008-02-20 | 2009-02-18 | 液晶媒体 |
JP2013124215A Active JP5917445B2 (ja) | 2008-02-20 | 2013-06-12 | 液晶媒体 |
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Country Status (8)
Country | Link |
---|---|
US (2) | US8574456B2 (ja) |
EP (1) | EP2242819B1 (ja) |
JP (2) | JP5542695B2 (ja) |
KR (1) | KR101573097B1 (ja) |
CN (3) | CN104357062B (ja) |
DE (1) | DE102009009414A1 (ja) |
TW (1) | TWI464243B (ja) |
WO (1) | WO2009103495A1 (ja) |
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Also Published As
Publication number | Publication date |
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CN104357062A (zh) | 2015-02-18 |
US20130327984A1 (en) | 2013-12-12 |
WO2009103495A1 (de) | 2009-08-27 |
US8834744B2 (en) | 2014-09-16 |
CN104357062B (zh) | 2016-11-02 |
CN104194801A (zh) | 2014-12-10 |
EP2242819B1 (de) | 2012-07-11 |
US20110001089A1 (en) | 2011-01-06 |
JP5542695B2 (ja) | 2014-07-09 |
JP5917445B2 (ja) | 2016-05-11 |
DE102009009414A1 (de) | 2009-08-27 |
TWI464243B (zh) | 2014-12-11 |
KR20100125335A (ko) | 2010-11-30 |
US8574456B2 (en) | 2013-11-05 |
CN101945976A (zh) | 2011-01-12 |
JP2011514410A (ja) | 2011-05-06 |
KR101573097B1 (ko) | 2015-11-30 |
CN104194801B (zh) | 2017-04-12 |
TW200946650A (en) | 2009-11-16 |
EP2242819A1 (de) | 2010-10-27 |
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