JP2012516301A5 - - Google Patents
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- JP2012516301A5 JP2012516301A5 JP2011546824A JP2011546824A JP2012516301A5 JP 2012516301 A5 JP2012516301 A5 JP 2012516301A5 JP 2011546824 A JP2011546824 A JP 2011546824A JP 2011546824 A JP2011546824 A JP 2011546824A JP 2012516301 A5 JP2012516301 A5 JP 2012516301A5
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- JP
- Japan
- Prior art keywords
- composition
- atoms
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- compound
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- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 125000004432 carbon atom Chemical group C* 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 22
- 238000004821 distillation Methods 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 15
- 150000001923 cyclic compounds Chemical class 0.000 claims description 11
- 125000000468 ketone group Chemical group 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 8
- 125000003172 aldehyde group Chemical group 0.000 claims description 5
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims 6
- -1 cyclic olefin Chemical class 0.000 claims 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- ZOLLIQAKMYWTBR-RYMQXAEESA-N cyclododecatriene Chemical compound C/1C\C=C\CC\C=C/CC\C=C\1 ZOLLIQAKMYWTBR-RYMQXAEESA-N 0.000 claims 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 claims 2
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims 2
- 238000000746 purification Methods 0.000 claims 2
- KEMUGHMYINTXKW-NQOXHWNZSA-N (1z,5z)-cyclododeca-1,5-diene Chemical compound C1CCC\C=C/CC\C=C/CC1 KEMUGHMYINTXKW-NQOXHWNZSA-N 0.000 claims 1
- QCSDLMPAQMQZOE-QSWGICILSA-N (1z,9z)-cyclohexadeca-1,9-diene Chemical compound C1CCC\C=C/CCCCCC\C=C/CC1 QCSDLMPAQMQZOE-QSWGICILSA-N 0.000 claims 1
- OJOWICOBYCXEKR-KRXBUXKQSA-N (5e)-5-ethylidenebicyclo[2.2.1]hept-2-ene Chemical compound C1C2C(=C/C)/CC1C=C2 OJOWICOBYCXEKR-KRXBUXKQSA-N 0.000 claims 1
- VYXHVRARDIDEHS-UHFFFAOYSA-N 1,5-cyclooctadiene Chemical compound C1CC=CCCC=C1 VYXHVRARDIDEHS-UHFFFAOYSA-N 0.000 claims 1
- 239000004912 1,5-cyclooctadiene Substances 0.000 claims 1
- SDRZFSPCVYEJTP-UHFFFAOYSA-N 1-ethenylcyclohexene Chemical compound C=CC1=CCCCC1 SDRZFSPCVYEJTP-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000001336 alkenes Chemical class 0.000 claims 1
- 238000002425 crystallisation Methods 0.000 claims 1
- 230000008025 crystallization Effects 0.000 claims 1
- JRVYFDBNSAHSKS-UHFFFAOYSA-N cyclododeca-1,6-diene Chemical compound C1CCC=CCCCC=CCC1 JRVYFDBNSAHSKS-UHFFFAOYSA-N 0.000 claims 1
- NVTIGTMUDIOSDY-UHFFFAOYSA-N cyclopentadeca-1,6,11-triene Chemical compound C1CC=CCCCC=CCCCC=CC1 NVTIGTMUDIOSDY-UHFFFAOYSA-N 0.000 claims 1
- WCMISCDQOHKOAN-UHFFFAOYSA-N cyclotetradeca-1,8-diene Chemical compound C1CCC=CCCCCCC=CCC1 WCMISCDQOHKOAN-UHFFFAOYSA-N 0.000 claims 1
- 238000000605 extraction Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229960001730 nitrous oxide Drugs 0.000 claims 1
- 235000013842 nitrous oxide Nutrition 0.000 claims 1
- SJYNFBVQFBRSIB-UHFFFAOYSA-N norbornadiene Chemical compound C1=CC2C=CC1C2 SJYNFBVQFBRSIB-UHFFFAOYSA-N 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 229910052723 transition metal Inorganic materials 0.000 claims 1
- 150000003624 transition metals Chemical class 0.000 claims 1
- 238000005829 trimerization reaction Methods 0.000 claims 1
- 239000007858 starting material Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000001577 simple distillation Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09151525.4 | 2009-01-28 | ||
| EP09151525 | 2009-01-28 | ||
| PCT/EP2010/050888 WO2010086314A1 (de) | 2009-01-28 | 2010-01-27 | Verfahren zur herstellung von reinem cyclododecanon |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012516301A JP2012516301A (ja) | 2012-07-19 |
| JP2012516301A5 true JP2012516301A5 (enExample) | 2014-10-30 |
| JP5661647B2 JP5661647B2 (ja) | 2015-01-28 |
Family
ID=42262059
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011546824A Expired - Fee Related JP5661647B2 (ja) | 2009-01-28 | 2010-01-27 | 純粋なシクロドデカノンの製法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8188320B2 (enExample) |
| EP (1) | EP2391597B1 (enExample) |
| JP (1) | JP5661647B2 (enExample) |
| KR (1) | KR20110110359A (enExample) |
| CN (1) | CN102365256A (enExample) |
| ES (1) | ES2698849T3 (enExample) |
| WO (1) | WO2010086314A1 (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102365256A (zh) | 2009-01-28 | 2012-02-29 | 巴斯夫欧洲公司 | 制备纯环十二酮的方法 |
| DE102009047196A1 (de) * | 2009-11-26 | 2011-06-01 | Basf Se | Verfahren zur Herstellung von 1,6-Hexandiol |
| EP2738161B1 (en) * | 2010-03-15 | 2018-04-11 | Ube Industries, Ltd. | Method for producing amide compound |
| US9394212B2 (en) | 2010-06-15 | 2016-07-19 | Basf Se | Process for the cooligomerization of olefins |
| CN104379547B (zh) * | 2012-06-13 | 2017-05-17 | 巴斯夫欧洲公司 | 制备大环酮的方法 |
| DE102014212602A1 (de) | 2013-07-02 | 2015-01-08 | Basf Se | Verfahren zur Herstellung eines Ketons aus einem Olefin |
| EP2980069A1 (de) * | 2014-08-01 | 2016-02-03 | Evonik Degussa GmbH | Verfahren zur Herstellung von Cyclododecanon |
| EP3002003A1 (de) | 2014-09-30 | 2016-04-06 | Basf Se | Verwendung neuartiger cyclischer Carbaldehyde als Aromastoff |
| EP3002058A1 (de) * | 2014-10-02 | 2016-04-06 | Evonik Degussa GmbH | Katalysatorsystem zur Herstellung von Ketonen aus Epoxiden |
| CN107001996A (zh) * | 2014-10-14 | 2017-08-01 | 巴斯夫欧洲公司 | 十六碳‑8,15‑二烯醛作为合成香料的用途 |
| EP3050869B1 (de) * | 2015-01-30 | 2019-10-02 | Symrise AG | Verfahren zur Herstellung von substituierten Alkylcycloalkanonen |
| EP3153493A1 (de) * | 2015-10-08 | 2017-04-12 | Basf Se | Verfahren zur reinigung von cyclohexadec-8-en-1-on |
| WO2017060440A1 (de) * | 2015-10-08 | 2017-04-13 | Basf Se | Verwendung neuartiger gemische von (e/z)-cyclopentadecenon-isomeren, deren herstellung und deren verwendung als aromastoff |
| US20220154099A1 (en) * | 2019-03-15 | 2022-05-19 | Basf Se | Use of 4,8,11-dodecatrienal to impart a clean aroma impression to a composition |
| CN114874085B (zh) * | 2022-07-12 | 2022-10-11 | 中国天辰工程有限公司 | 一种环十二酮提纯工艺 |
Family Cites Families (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US316917A (en) | 1885-04-28 | Cord-spool and tension device for grain-binders | ||
| US2875256A (en) | 1953-01-21 | 1959-02-24 | Shell Dev | Dienic hydrocarbons and derivatives thereof |
| DE1283836B (de) | 1959-12-22 | 1968-11-28 | Studiengesellschaft Kohle Mbh | Verfahren zur Herstellung von hauptsaechlich Cyclododekatrien-(1,5,9) enthaltenden Produkten durch Cyclooligomerisation von 1, 3-Diolefinen |
| US3182093A (en) | 1961-10-02 | 1965-05-04 | Exxon Research Engineering Co | Preparation of 1, 5-cyclododecadiene |
| BE646244A (enExample) | 1963-04-10 | 1900-01-01 | ||
| US3804914A (en) | 1972-05-25 | 1974-04-16 | Phillips Petroleum Co | Ruthenium(ii)complexes as catalysts for selective hydrogenation of cyclic polyenes to cyclic monoenes |
| DD115480A2 (enExample) | 1974-08-19 | 1975-10-05 | ||
| DE2519817A1 (de) | 1975-05-03 | 1976-11-11 | Hoechst Ag | Verfahren zur herstellung von butandiol-(1.4) |
| EP0158229B1 (en) | 1984-03-28 | 1988-06-22 | Asahi Kasei Kogyo Kabushiki Kaisha | Process for producing polyether polyol, the produced polyether polyol and polyurethane |
| DE3863195D1 (de) | 1987-02-16 | 1991-07-18 | Sumitomo Chemical Co | Feste base, verfahren zu deren herstellung und ihre anwendung fuer die herstellung von olefinen mit innerer doppelbindung. |
| GB8707595D0 (en) | 1987-03-31 | 1987-05-07 | British Petroleum Co Plc | Chemical process |
| US5210349A (en) | 1991-07-01 | 1993-05-11 | Phillips Petroleum Company | Selective hydrogenation of cyclic polyenes |
| US5128296A (en) | 1991-07-01 | 1992-07-07 | Phillips Petroleum Company | Selective hydrogenation of cyclic polyenes |
| US5180870A (en) | 1991-10-23 | 1993-01-19 | E. I. Du Pont De Nemours And Company | Hydrogenation of polyenes |
| US5177278A (en) | 1991-10-23 | 1993-01-05 | E. I. Du Pont De Nemours And Company | Preparation of cyclododecene |
| US5321176A (en) | 1992-12-22 | 1994-06-14 | E. I. Du Pont De Nemours And Company | Hydrogenation of polyenes |
| DE19510993C1 (de) | 1995-03-24 | 1996-08-29 | Fhw Brenntechnik Gmbh | Vorrichtung zur thermischen Abgasbehandlung, insbesondere von oxidierbaren Schwelgasen |
| EP0915100A4 (en) | 1996-12-05 | 2002-10-09 | Kyowa Hakko Kogyo Kk | NEW PROTEIN |
| DE10142033A1 (de) | 2001-08-28 | 2003-03-20 | Haarmann & Reimer Gmbh | Metathesekatalysatoren |
| DE10344595A1 (de) * | 2003-09-25 | 2005-05-12 | Basf Ag | Verfahren zur Herstellung eines Ketons |
| DE102004046167A1 (de) | 2004-09-23 | 2006-04-06 | Basf Ag | Verfahren zur Reinigung und Aufkonzentrierung von Distickstoffmonoxid |
| DE102005048250A1 (de) * | 2005-10-07 | 2007-04-12 | Basf Ag | Verfahren zur Farbzahlverbesserung |
| DE102005055588A1 (de) | 2005-11-22 | 2007-05-24 | Basf Ag | Verfahren zur Isolierung von N2O |
| CN101400645B (zh) | 2006-03-10 | 2013-11-13 | 巴斯夫欧洲公司 | 制备二苯酮亚胺的方法 |
| ATE471307T1 (de) * | 2006-06-29 | 2010-07-15 | Basf Se | Verfahren zur herstellung von cyclischen ketonen |
| KR101390580B1 (ko) | 2006-06-29 | 2014-04-30 | 바스프 에스이 | 시클릭 케톤의 제조 방법 |
| EP2041061B1 (de) | 2006-06-29 | 2013-05-08 | Basf Se | Reinigung von Cyclododecanon durch thermisches Behandeln |
| CN101558009B (zh) | 2006-12-11 | 2012-03-28 | 巴斯夫欧洲公司 | 分离n2o的方法 |
| MY155650A (en) | 2007-08-21 | 2015-11-13 | Basf Se | Process and device for the oxidation of organic compounds |
| WO2009024549A2 (de) | 2007-08-21 | 2009-02-26 | Basf Se | Verfahren und vorrichtung zur oxidation organischer verbindungen |
| EP2225220B1 (de) | 2007-12-21 | 2013-05-22 | Basf Se | Verfahren zur Herstellung von epsilon-Caprolacton |
| DE112009000169B4 (de) | 2008-01-25 | 2021-07-29 | Basf Se | Methode zur selektiven großtechnischen Herstellung von 1,5,9 Cyclododecatrien |
| WO2009092682A2 (de) | 2008-01-25 | 2009-07-30 | Basf Se | Verfahren und vorrichtung zur destillativen aufarbeitung von 1,5,9-cyclododecatrien und gewinnung von cdt mit hoher reinheit |
| CA2720403C (en) | 2008-04-02 | 2016-02-23 | Basf Se | Process for isolating n2o |
| JP5518044B2 (ja) | 2008-04-02 | 2014-06-11 | ビーエーエスエフ ソシエタス・ヨーロピア | 一酸化二窒素の精製方法 |
| KR101651699B1 (ko) | 2008-08-29 | 2016-08-26 | 바스프 에스이 | 시클릭 케톤의 제조 방법 |
| WO2010076182A1 (de) | 2008-12-30 | 2010-07-08 | Basf Se | Verfahren zur herstellung von ketonen durch umsetzung von 1,1-disubstituierten olefinen mit n2o |
| US9174192B2 (en) | 2009-01-21 | 2015-11-03 | Basf Se | Tube bundle reactor for uncatalyzed or homogeneously catalyzed reactions |
| JP5698152B2 (ja) | 2009-01-28 | 2015-04-08 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | ドデカトリエナールの単離法、及びその香料としての使用 |
| CN102365256A (zh) | 2009-01-28 | 2012-02-29 | 巴斯夫欧洲公司 | 制备纯环十二酮的方法 |
-
2010
- 2010-01-27 CN CN2010800147909A patent/CN102365256A/zh active Pending
- 2010-01-27 JP JP2011546824A patent/JP5661647B2/ja not_active Expired - Fee Related
- 2010-01-27 WO PCT/EP2010/050888 patent/WO2010086314A1/de not_active Ceased
- 2010-01-27 EP EP10701244.5A patent/EP2391597B1/de active Active
- 2010-01-27 US US12/694,815 patent/US8188320B2/en not_active Expired - Fee Related
- 2010-01-27 ES ES10701244T patent/ES2698849T3/es active Active
- 2010-01-27 KR KR1020117019844A patent/KR20110110359A/ko not_active Abandoned
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