CN102365256A - 制备纯环十二酮的方法 - Google Patents

制备纯环十二酮的方法 Download PDF

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Publication number
CN102365256A
CN102365256A CN2010800147909A CN201080014790A CN102365256A CN 102365256 A CN102365256 A CN 102365256A CN 2010800147909 A CN2010800147909 A CN 2010800147909A CN 201080014790 A CN201080014790 A CN 201080014790A CN 102365256 A CN102365256 A CN 102365256A
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CN
China
Prior art keywords
carbon atoms
rings
composition
compound
cyclic
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Pending
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CN2010800147909A
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English (en)
Chinese (zh)
Inventor
J·H·特莱斯
B·罗斯勒-菲戈尔`
A·豪克
A·迈尔
C·米勒
M·舍伯尔
T·基希纳
S·塞斯什库斯
R·平科斯
G-D·特本
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BASF SE
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BASF SE
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Publication of CN102365256A publication Critical patent/CN102365256A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20—Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN2010800147909A 2009-01-28 2010-01-27 制备纯环十二酮的方法 Pending CN102365256A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09151525 2009-01-28
EP09151525.4 2009-01-28
PCT/EP2010/050888 WO2010086314A1 (de) 2009-01-28 2010-01-27 Verfahren zur herstellung von reinem cyclododecanon

Publications (1)

Publication Number Publication Date
CN102365256A true CN102365256A (zh) 2012-02-29

Family

ID=42262059

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2010800147909A Pending CN102365256A (zh) 2009-01-28 2010-01-27 制备纯环十二酮的方法

Country Status (7)

Country Link
US (1) US8188320B2 (enExample)
EP (1) EP2391597B1 (enExample)
JP (1) JP5661647B2 (enExample)
KR (1) KR20110110359A (enExample)
CN (1) CN102365256A (enExample)
ES (1) ES2698849T3 (enExample)
WO (1) WO2010086314A1 (enExample)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104379547A (zh) * 2012-06-13 2015-02-25 巴斯夫欧洲公司 制备大环酮的方法
CN105315146A (zh) * 2014-08-01 2016-02-10 赢创德固赛有限公司 制备环十二酮的方法
CN106715375A (zh) * 2014-09-30 2017-05-24 巴斯夫欧洲公司 新环状醛作为芳香物质的用途
CN107001996A (zh) * 2014-10-14 2017-08-01 巴斯夫欧洲公司 十六碳‑8,15‑二烯醛作为合成香料的用途
CN108137461A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 提纯环十六碳-8-烯-1-酮的方法
CN108137460A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 (e/z)-环十五碳烯酮异构体的新型混合物的用途、其制备和作为增香剂物质的用途
CN114874085A (zh) * 2022-07-12 2022-08-09 中国天辰工程有限公司 一种环十二酮提纯工艺
CN116003254A (zh) * 2015-01-30 2023-04-25 西姆莱斯股份公司 用于制备取代的烷基环烷酮的方法

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US8188320B2 (en) 2009-01-28 2012-05-29 Basf Se Process for preparing pure cyclododecanone
DE102009047196A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von 1,6-Hexandiol
CN103864657A (zh) * 2010-03-15 2014-06-18 宇部兴产株式会社 制备酰胺化合物的方法
US9394212B2 (en) 2010-06-15 2016-07-19 Basf Se Process for the cooligomerization of olefins
DE102014212602A1 (de) 2013-07-02 2015-01-08 Basf Se Verfahren zur Herstellung eines Ketons aus einem Olefin
EP3002058A1 (de) * 2014-10-02 2016-04-06 Evonik Degussa GmbH Katalysatorsystem zur Herstellung von Ketonen aus Epoxiden
MX2021011092A (es) * 2019-03-15 2021-10-26 Basf Se Uso de 4,8,11-dodecatrienal para impartir una impresion de aroma limpio a una composicion.

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DE10344595A1 (de) 2003-09-25 2005-05-12 Basf Ag Verfahren zur Herstellung eines Ketons
DE102004046167A1 (de) 2004-09-23 2006-04-06 Basf Ag Verfahren zur Reinigung und Aufkonzentrierung von Distickstoffmonoxid
DE102005048250A1 (de) * 2005-10-07 2007-04-12 Basf Ag Verfahren zur Farbzahlverbesserung
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JP5108880B2 (ja) * 2006-06-29 2012-12-26 ビーエーエスエフ ソシエタス・ヨーロピア 環状ケトンの製造方法
EP2041061B1 (de) 2006-06-29 2013-05-08 Basf Se Reinigung von Cyclododecanon durch thermisches Behandeln
CN101558009B (zh) 2006-12-11 2012-03-28 巴斯夫欧洲公司 分离n2o的方法
JP5733979B2 (ja) * 2007-08-21 2015-06-10 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 有機化合物を酸化するための方法および装置
WO2009024549A2 (de) * 2007-08-21 2009-02-26 Basf Se Verfahren und vorrichtung zur oxidation organischer verbindungen
EP2225220B1 (de) * 2007-12-21 2013-05-22 Basf Se Verfahren zur Herstellung von epsilon-Caprolacton
WO2009092682A2 (de) 2008-01-25 2009-07-30 Basf Se Verfahren und vorrichtung zur destillativen aufarbeitung von 1,5,9-cyclododecatrien und gewinnung von cdt mit hoher reinheit
WO2009092683A2 (de) 2008-01-25 2009-07-30 Basf Se METHODE ZUR SELEKTIVEN GROßTECHNISCHEN HERSTELLUNG VON 1,5,9 CYCLODODECATRIEN
US8404901B2 (en) 2008-04-02 2013-03-26 Basf Se Process for purifying dinitrogen monoxide
EP2271584B1 (de) 2008-04-02 2013-05-15 Basf Se Verfahren zur reinigung von n2o
JP5579183B2 (ja) * 2008-08-29 2014-08-27 ビーエーエスエフ ソシエタス・ヨーロピア 環式ケトンの製造方法
WO2010076182A1 (de) * 2008-12-30 2010-07-08 Basf Se Verfahren zur herstellung von ketonen durch umsetzung von 1,1-disubstituierten olefinen mit n2o
CN102361687B (zh) 2009-01-21 2015-05-13 巴斯夫欧洲公司 用于非催化或均相催化反应的管束反应器
JP5698152B2 (ja) * 2009-01-28 2015-04-08 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ドデカトリエナールの単離法、及びその香料としての使用
US8188320B2 (en) 2009-01-28 2012-05-29 Basf Se Process for preparing pure cyclododecanone

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104379547A (zh) * 2012-06-13 2015-02-25 巴斯夫欧洲公司 制备大环酮的方法
CN105315146A (zh) * 2014-08-01 2016-02-10 赢创德固赛有限公司 制备环十二酮的方法
CN105315146B (zh) * 2014-08-01 2019-09-20 赢创德固赛有限公司 制备环十二酮的方法
CN106715375A (zh) * 2014-09-30 2017-05-24 巴斯夫欧洲公司 新环状醛作为芳香物质的用途
CN107001996A (zh) * 2014-10-14 2017-08-01 巴斯夫欧洲公司 十六碳‑8,15‑二烯醛作为合成香料的用途
CN116003254A (zh) * 2015-01-30 2023-04-25 西姆莱斯股份公司 用于制备取代的烷基环烷酮的方法
CN108137461A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 提纯环十六碳-8-烯-1-酮的方法
CN108137460A (zh) * 2015-10-08 2018-06-08 巴斯夫欧洲公司 (e/z)-环十五碳烯酮异构体的新型混合物的用途、其制备和作为增香剂物质的用途
CN114874085A (zh) * 2022-07-12 2022-08-09 中国天辰工程有限公司 一种环十二酮提纯工艺
CN114874085B (zh) * 2022-07-12 2022-10-11 中国天辰工程有限公司 一种环十二酮提纯工艺

Also Published As

Publication number Publication date
US8188320B2 (en) 2012-05-29
KR20110110359A (ko) 2011-10-06
EP2391597A1 (de) 2011-12-07
WO2010086314A1 (de) 2010-08-05
EP2391597B1 (de) 2018-08-22
JP2012516301A (ja) 2012-07-19
US20100191018A1 (en) 2010-07-29
JP5661647B2 (ja) 2015-01-28
ES2698849T3 (es) 2019-02-06

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Application publication date: 20120229