JP2012107207A - 印刷用溶剤又は溶剤組成物 - Google Patents
印刷用溶剤又は溶剤組成物 Download PDFInfo
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- JP2012107207A JP2012107207A JP2011219851A JP2011219851A JP2012107207A JP 2012107207 A JP2012107207 A JP 2012107207A JP 2011219851 A JP2011219851 A JP 2011219851A JP 2011219851 A JP2011219851 A JP 2011219851A JP 2012107207 A JP2012107207 A JP 2012107207A
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- 239000002904 solvent Substances 0.000 title claims abstract description 65
- 238000007639 printing Methods 0.000 title claims abstract description 56
- 239000000203 mixture Substances 0.000 title claims abstract description 54
- 238000000034 method Methods 0.000 claims abstract description 89
- -1 dipropylene glycol dialkyl ether Chemical class 0.000 claims abstract description 31
- 239000011347 resin Substances 0.000 claims abstract description 28
- 229920005989 resin Polymers 0.000 claims abstract description 28
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 20
- 239000011230 binding agent Substances 0.000 claims abstract description 15
- 150000001875 compounds Chemical class 0.000 claims abstract description 8
- 238000005401 electroluminescence Methods 0.000 claims abstract description 8
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 7
- 238000007646 gravure printing Methods 0.000 claims abstract description 6
- 238000000813 microcontact printing Methods 0.000 claims abstract description 6
- 238000007645 offset printing Methods 0.000 claims abstract description 6
- 238000007650 screen-printing Methods 0.000 claims abstract description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 22
- 230000007261 regionalization Effects 0.000 claims description 18
- 239000000758 substrate Substances 0.000 claims description 15
- 239000004925 Acrylic resin Substances 0.000 claims description 5
- 229920000178 Acrylic resin Polymers 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
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- 238000011156 evaluation Methods 0.000 description 2
- CATSNJVOTSVZJV-UHFFFAOYSA-N heptan-2-one Chemical compound CCCCCC(C)=O CATSNJVOTSVZJV-UHFFFAOYSA-N 0.000 description 2
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- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
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- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/033—Printing inks characterised by features other than the chemical nature of the binder characterised by the solvent
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/02—Ethers
- C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
- C07C43/04—Saturated ethers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/52—Electrically conductive inks
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
- H01L21/48—Manufacture or treatment of parts, e.g. containers, prior to assembly of the devices, using processes not provided for in a single one of the subgroups H01L21/06 - H01L21/326
- H01L21/4814—Conductive parts
- H01L21/4846—Leads on or in insulating or insulated substrates, e.g. metallisation
- H01L21/4867—Applying pastes or inks, e.g. screen printing
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- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B33/00—Electroluminescent light sources
- H05B33/12—Light sources with substantially two-dimensional radiating surfaces
- H05B33/22—Light sources with substantially two-dimensional radiating surfaces characterised by the chemical or physical composition or the arrangement of auxiliary dielectric or reflective layers
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- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Electroluminescent Light Sources (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
【解決手段】本発明の有機エレクトロルミネッセンスデバイスのパターン印刷用溶剤又は溶剤組成物は、有機エレクトロルミネッセンスデバイスを構成する素子パターンを印刷法により形成する際に使用する溶剤組成物であって、プロピレングリコールジアルキルエーテルの2つの末端アルキル基の一方がメチル基であり、もう一方が炭素数4又は炭素数5の直鎖状又は分岐鎖状アルキル基である化合物を含むことを特徴とする。前記印刷法としては、インクジェット法、スクリーン印刷法、凸版印刷法、オフセット印刷法、グラビア印刷法、マイクロコンタクト印刷法、ナノインプリント法からなる群より選択される少なくとも1種の方法が好ましい。
【選択図】なし
Description
本発明の他の目的は、前記有機エレクトロルミネッセンスデバイスのパターン印刷用溶剤又は溶剤組成物を含有する有機エレクトロルミネッセンスデバイスのパターン形成用ペースト組成物を提供することにある。
本発明の更に他の目的は、前記有機エレクトロルミネッセンスデバイスのパターン形成用ペースト組成物を使用してパターン形成を行うパターン形成方法を提供することにある。
本発明に係る有機ELデバイスのパターン印刷用溶剤又は溶剤組成物は、有機ELデバイスを構成する素子を印刷法により形成する際に使用する溶剤組成物であって、プロピレングリコールジアルキルエーテルの2つの末端アルキル基の一方がメチル基であり、もう一方が炭素数4又は炭素数5の直鎖状又は分岐鎖状アルキル基である化合物を含むことを特徴とする。
本発明に係る有機ELデバイスのパターン形成用ペースト組成物は、少なくとも上記有機ELデバイスのパターン印刷用溶剤又は溶剤組成物とバインダー樹脂とを含有することを特徴とする。
本発明に係るパターン形成方法は、有機ELデバイスを構成する素子のパターン形成方法であって、基板上に、上記有機ELデバイスのパターン形成用ペースト組成物を印刷法を用いて塗布することによりパターン層を形成する工程(パターン印刷工程)と、前記パターン層を硬化又は焼成する工程(パターン硬化又は焼成工程)とを有することを特徴とする。
1:ガラス等の基板上に陽極を形成する。
2:ガラス等の基板上の、陽極を形成した部分以外の部分に隔壁を形成する。
3:陽極上に、赤、緑、青、又は白色の発光層を印刷法により形成し、硬化させる。
4:発光層及び隔壁の上に陰極を形成する。
プロピレングリコールメチル‐n‐ブチルエーテル(商品名「PMNB」、ダイセル化学工業(株)製、以後、「PMNB」と称する場合がある)20g、蒸留水 20gを、50mlフラスコに入れ、約10分間撹拌した後、10分間静置し、有機相の水分測定を行ったところ、25℃環境下における水分濃度は0.7%であった。
評価基準
エチルセルロースが完全に溶解した:○
エチルセルロースが一部不溶、或いは全く不溶であった:×
プロピレングリコールジメチルエーテル(商品名「ハイソルブMMPOM」、東邦化学工業(株)製、以後、「MMPOM」と称する場合がある)20g、蒸留水 20gを、50mlフラスコに入れ、約10分間撹拌した後、10分間静置し、有機相の水分測定を行ったところ、25℃環境下における水分濃度は7.3%であった。
「第5版 実験科学講座14」(丸善株式会社出版、p239-241)に記載の方法により合成したプロピレングリコールジブチルエーテル(以後、「PDB」と称する場合がある)20g、蒸留水 20gを、50mlフラスコに入れ、約10分間撹拌した後、10分間静置し、有機相の水分測定を行ったところ、25℃環境下における水分濃度は0.1%であった。
Claims (5)
- 有機エレクトロルミネッセンスデバイスを構成する素子パターンを印刷法により形成する際に使用する溶剤組成物であって、プロピレングリコールジアルキルエーテルの2つの末端アルキル基の一方がメチル基であり、もう一方が炭素数4又は炭素数5の直鎖状又は分岐鎖状アルキル基である化合物を含むことを特徴とする有機エレクトロルミネッセンスデバイスのパターン印刷用溶剤又は溶剤組成物。
- 印刷法がインクジェット法、スクリーン印刷法、凸版印刷法、オフセット印刷法、グラビア印刷法、マイクロコンタクト印刷法、ナノインプリント法からなる群より選択される少なくとも1種の方法である請求項1に記載の有機エレクトロルミネッセンスデバイスのパターン印刷用溶剤又は溶剤組成物。
- 請求項1又は2に記載の有機エレクトロルミネッセンスデバイスのパターン印刷用溶剤又は溶剤組成物とバインダー樹脂とを少なくとも含有する有機エレクトロルミネッセンスデバイスのパターン形成用ペースト組成物。
- バインダー樹脂がセルロース系樹脂及び/又はアクリル系樹脂である請求項3に記載の有機エレクトロルミネッセンスデバイスのパターン形成用ペースト組成物。
- 有機エレクトロルミネッセンスデバイスを構成する素子のパターン形成方法であって、基板上に、請求項3又は4に記載の有機エレクトロルミネッセンスデバイスのパターン形成用ペースト組成物を印刷法を用いて塗布することによりパターン層を形成する工程と、前記パターン層を硬化又は焼成する工程とを有することを特徴とするパターン形成方法。
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JP2017088780A (ja) * | 2015-11-13 | 2017-05-25 | セイコーエプソン株式会社 | インク組成物 |
JP2019102564A (ja) * | 2017-11-30 | 2019-06-24 | コニカミノルタ株式会社 | 有機機能性薄膜、有機機能性積層膜、有機エレクトロルミネッセンス素子、光電変換素子及び有機機能性薄膜形成用塗布液 |
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WO2015087811A1 (ja) * | 2013-12-09 | 2015-06-18 | 株式会社ダイセル | 電気デバイス製造用溶剤組成物 |
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JP2017088780A (ja) * | 2015-11-13 | 2017-05-25 | セイコーエプソン株式会社 | インク組成物 |
JP2019102564A (ja) * | 2017-11-30 | 2019-06-24 | コニカミノルタ株式会社 | 有機機能性薄膜、有機機能性積層膜、有機エレクトロルミネッセンス素子、光電変換素子及び有機機能性薄膜形成用塗布液 |
JP6996260B2 (ja) | 2017-11-30 | 2022-01-17 | コニカミノルタ株式会社 | 有機機能性薄膜、有機機能性積層膜、有機エレクトロルミネッセンス素子、光電変換素子及び有機機能性薄膜形成用塗布液 |
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TW201224075A (en) | 2012-06-16 |
CN102453376A (zh) | 2012-05-16 |
JP5940790B2 (ja) | 2016-06-29 |
KR20120043645A (ko) | 2012-05-04 |
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