JP2011526946A5 - - Google Patents
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- Publication number
- JP2011526946A5 JP2011526946A5 JP2011516397A JP2011516397A JP2011526946A5 JP 2011526946 A5 JP2011526946 A5 JP 2011526946A5 JP 2011516397 A JP2011516397 A JP 2011516397A JP 2011516397 A JP2011516397 A JP 2011516397A JP 2011526946 A5 JP2011526946 A5 JP 2011526946A5
- Authority
- JP
- Japan
- Prior art keywords
- zone
- amine
- reaction zone
- epoxy resin
- functional epoxy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000006243 chemical reaction Methods 0.000 claims 18
- 238000002156 mixing Methods 0.000 claims 17
- 150000001412 amines Chemical class 0.000 claims 15
- 229920000647 polyepoxide Polymers 0.000 claims 15
- 239000003822 epoxy resin Substances 0.000 claims 13
- 239000011230 binding agent Substances 0.000 claims 11
- 238000000034 method Methods 0.000 claims 11
- 239000006185 dispersion Substances 0.000 claims 9
- 239000000203 mixture Substances 0.000 claims 8
- 238000004070 electrodeposition Methods 0.000 claims 7
- 239000012530 fluid Substances 0.000 claims 6
- 239000000463 material Substances 0.000 claims 6
- 239000002253 acid Substances 0.000 claims 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 5
- 239000004971 Cross linker Substances 0.000 claims 4
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 claims 4
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims 4
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 claims 4
- QCOGKXLOEWLIDC-UHFFFAOYSA-N N-methylbutylamine Chemical compound CCCCNC QCOGKXLOEWLIDC-UHFFFAOYSA-N 0.000 claims 4
- JQVDAXLFBXTEQA-UHFFFAOYSA-N dibutylamine Chemical compound CCCCNCCCC JQVDAXLFBXTEQA-UHFFFAOYSA-N 0.000 claims 4
- 238000001704 evaporation Methods 0.000 claims 4
- 230000008020 evaporation Effects 0.000 claims 4
- QOHMWDJIBGVPIF-UHFFFAOYSA-N n',n'-diethylpropane-1,3-diamine Chemical compound CCN(CC)CCCN QOHMWDJIBGVPIF-UHFFFAOYSA-N 0.000 claims 4
- 239000004014 plasticizer Substances 0.000 claims 4
- 239000000376 reactant Substances 0.000 claims 4
- 239000002904 solvent Substances 0.000 claims 4
- 238000011144 upstream manufacturing Methods 0.000 claims 4
- 239000000839 emulsion Substances 0.000 claims 3
- 238000007151 ring opening polymerisation reaction Methods 0.000 claims 3
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 claims 2
- UIKUBYKUYUSRSM-UHFFFAOYSA-N 3-morpholinopropylamine Chemical compound NCCCN1CCOCC1 UIKUBYKUYUSRSM-UHFFFAOYSA-N 0.000 claims 2
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 claims 2
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims 2
- 239000000654 additive Substances 0.000 claims 2
- 230000000996 additive effect Effects 0.000 claims 2
- IMUDHTPIFIBORV-UHFFFAOYSA-N aminoethylpiperazine Chemical compound NCCN1CCNCC1 IMUDHTPIFIBORV-UHFFFAOYSA-N 0.000 claims 2
- 238000010924 continuous production Methods 0.000 claims 2
- 239000006184 cosolvent Substances 0.000 claims 2
- IUNMPGNGSSIWFP-UHFFFAOYSA-N dimethylaminopropylamine Chemical compound CN(C)CCCN IUNMPGNGSSIWFP-UHFFFAOYSA-N 0.000 claims 2
- WEHWNAOGRSTTBQ-UHFFFAOYSA-N dipropylamine Chemical compound CCCNCCC WEHWNAOGRSTTBQ-UHFFFAOYSA-N 0.000 claims 2
- JILXUIANNUALRZ-UHFFFAOYSA-N n',n'-diethylbutane-1,4-diamine Chemical compound CCN(CC)CCCCN JILXUIANNUALRZ-UHFFFAOYSA-N 0.000 claims 2
- GCOWZPRIMFGIDQ-UHFFFAOYSA-N n',n'-dimethylbutane-1,4-diamine Chemical compound CN(C)CCCCN GCOWZPRIMFGIDQ-UHFFFAOYSA-N 0.000 claims 2
- DILRJUIACXKSQE-UHFFFAOYSA-N n',n'-dimethylethane-1,2-diamine Chemical compound CN(C)CCN DILRJUIACXKSQE-UHFFFAOYSA-N 0.000 claims 2
- BXYVQNNEFZOBOZ-UHFFFAOYSA-N n-[3-(dimethylamino)propyl]-n',n'-dimethylpropane-1,3-diamine Chemical compound CN(C)CCCNCCCN(C)C BXYVQNNEFZOBOZ-UHFFFAOYSA-N 0.000 claims 2
- 239000007787 solid Substances 0.000 claims 2
- -1 (A) Continuously Polymers 0.000 claims 1
- 239000004606 Fillers/Extenders Substances 0.000 claims 1
- 125000003277 amino group Chemical group 0.000 claims 1
- 239000006227 byproduct Substances 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 239000003431 cross linking reagent Substances 0.000 claims 1
- 239000008367 deionised water Substances 0.000 claims 1
- 229910021641 deionized water Inorganic materials 0.000 claims 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 238000004064 recycling Methods 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/164,883 US8242234B2 (en) | 2008-06-30 | 2008-06-30 | Process for continuous production of epoxy resins |
| US12/164,883 | 2008-06-30 | ||
| PCT/US2009/046201 WO2010002539A1 (en) | 2008-06-30 | 2009-06-04 | Process for continuous production of epoxy resins |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011526946A JP2011526946A (ja) | 2011-10-20 |
| JP2011526946A5 true JP2011526946A5 (https=) | 2012-07-19 |
| JP5415536B2 JP5415536B2 (ja) | 2014-02-12 |
Family
ID=41016513
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011516397A Expired - Fee Related JP5415536B2 (ja) | 2008-06-30 | 2009-06-04 | エポキシ樹脂の連続的製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8242234B2 (https=) |
| EP (1) | EP2294109B1 (https=) |
| JP (1) | JP5415536B2 (https=) |
| CN (1) | CN102143985B (https=) |
| AT (1) | ATE540068T1 (https=) |
| WO (1) | WO2010002539A1 (https=) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MX2015010210A (es) | 2013-03-15 | 2015-11-25 | Basf Se | Productos reticulados preparados mediante la reticulacion ionica de un oligomero de grado solido y un polimero, que utilizan un agente reticulante ionico y metodos para preparar los mismos. |
| MX2015012047A (es) | 2013-03-15 | 2015-12-16 | Basf Se | Composiciones que comprenden un copolimero de un oligomero de graso solido y un monomero hidrofobico y/o un monomero en fase gaseosa y metodos para producir el mismo. |
| US9504983B2 (en) * | 2013-10-09 | 2016-11-29 | Karlton D. Krause | System and method for converting biomass into fuel, oil and other useful products |
| CN106029750B (zh) | 2013-12-20 | 2019-04-16 | 巴斯夫欧洲公司 | 使用离子交联剂制备的组合物及其制备方法 |
| CN106492722B (zh) * | 2016-10-21 | 2018-07-20 | 山西省交通科学研究院 | 一种水性环氧树脂制备装置 |
| CN108654547A (zh) * | 2018-06-26 | 2018-10-16 | 江苏博砚电子科技有限公司 | 一种感光树脂合成装置 |
| US11186734B2 (en) * | 2019-05-31 | 2021-11-30 | Axalta Coating Systems Ip Co., Llc | Epoxy resin emulsions for electrocoating |
| KR102891804B1 (ko) * | 2024-02-14 | 2025-11-26 | 한국화학연구원 | 에폭시-아민 클릭반응을 통해 제조되는 에폭시 수지 |
Family Cites Families (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3735558A (en) | 1971-06-29 | 1973-05-29 | Perma Pure Process Inc | Process for separating fluids and apparatus |
| US4001156A (en) * | 1972-08-03 | 1977-01-04 | Ppg Industries, Inc. | Method of producing epoxy group-containing, quaternary ammonium salt-containing resins |
| US3919169A (en) * | 1974-02-20 | 1975-11-11 | Dow Chemical Co | Continuous process for the production of solid epoxy resins |
| CA1111598A (en) * | 1976-01-14 | 1981-10-27 | Joseph R. Marchetti | Amine acide salt-containing polymers for cationic electrodeposition |
| US4105634A (en) * | 1976-08-11 | 1978-08-08 | Celanese Corporation | Production of thermosetting resinous polyepoxides |
| US4338232A (en) | 1977-12-27 | 1982-07-06 | The Dow Chemical Company | Radiation-curable resins |
| US4186086A (en) * | 1978-06-26 | 1980-01-29 | The Dow Chemical Company | Weak base ion exchange resins of a polyalkylenepolyamine and polyepoxide |
| US4568735A (en) * | 1984-11-05 | 1986-02-04 | Shell Oil Company | Process for preparing polyepoxides (II) |
| JPH07119271B2 (ja) | 1987-09-07 | 1995-12-20 | ダイセル化学工業株式会社 | エポキシ樹脂の連続製造方法 |
| JPH03122112A (ja) | 1989-10-05 | 1991-05-24 | Dainippon Ink & Chem Inc | 固形ビスフェノールａ型エポキシ樹脂の連続重合製造法 |
| US5089100A (en) | 1990-08-06 | 1992-02-18 | E. I. Du Pont De Nemours And Company | Method of incorporating polyamine into a cationic resin |
| GB9028037D0 (en) | 1990-12-24 | 1991-02-13 | Dow Rheinmuenster | Stable amine advanced epoxy resin compositions |
| US5372790A (en) * | 1991-01-18 | 1994-12-13 | The Dow Chemical Company | Vertical continuous reactor |
| JPH04335019A (ja) | 1991-05-10 | 1992-11-24 | Dainippon Ink & Chem Inc | ビニルエステル樹脂の連続製造法 |
| JP2511216B2 (ja) | 1991-10-02 | 1996-06-26 | カネボウ・エヌエスシー株式会社 | 無溶剤型エポキシエマルジヨンの製法 |
| US6245835B1 (en) | 1996-02-29 | 2001-06-12 | The Dow Chemical Company | Polymeric amines and reactive epoxy polymer compositions |
| CO4850623A1 (es) * | 1996-04-19 | 1999-10-26 | Shell Int Research | Procedimiento para la preparacion de resinas avanzadas . |
| GB9611118D0 (en) * | 1996-05-29 | 1996-07-31 | Ici Plc | Dispersions |
| US6017432A (en) * | 1997-07-03 | 2000-01-25 | Ppg Industries Ohio, Inc. | Electrodepositable coating compositions and their use in a method of cationic electrodeposition |
| JP2003500506A (ja) * | 1999-05-20 | 2003-01-07 | ザ ダウ ケミカル カンパニー | 水性もしくは非水性媒体にポリマー樹脂を押し出しかつ機械的に分散させる連続方法 |
| AR024361A1 (es) * | 1999-06-15 | 2002-10-02 | Dow Chemical Co | Proceso y aparato para preparar una composicion utilizando un reactor continuo y mezclador en serie |
| EP1198481B1 (en) | 1999-07-14 | 2006-01-04 | Johnson Polymer, Inc. | Process for the continuous production of epoxy - (meth)acrylic - styrene polymers and their use in coating |
| JP2001064353A (ja) | 1999-08-30 | 2001-03-13 | Japan Epoxy Resin Kk | 高分子量エポキシ樹脂の製造方法 |
| US6492483B1 (en) * | 1999-12-21 | 2002-12-10 | Resolution Performance Products Llc | Integrated continuous process for upstaging epoxy resins |
| DE60114378T2 (de) * | 2000-02-11 | 2006-07-27 | Akzo Nobel Coatings International B.V. | Verfahren zur herstellung einer wässrigen pulverlack-dispersion |
| AU2001266827A1 (en) * | 2000-06-15 | 2001-12-24 | Dow Global Technologies Inc. | Process and apparatus for preparing polymers, utilizing a side stream ultrasonic device for monitoring and controlling the properties of the polymer |
| US6605681B1 (en) | 2000-07-12 | 2003-08-12 | Johnson Polymer, Inc. | Process for the continuous production of epoxylated addition polymers, and powder and liquid coating applications containing epoxylated addition polymers |
| KR100549366B1 (ko) * | 2003-12-30 | 2006-02-03 | 주식회사 디피아이 | 양이온성 전착 도료 조성물 및 이의 제조 방법 |
| JP4335019B2 (ja) | 2004-01-13 | 2009-09-30 | 小川香料株式会社 | フレーバー組成物の製造方法 |
| TW200710116A (en) | 2005-06-13 | 2007-03-16 | Nippon Paint Co Ltd | Method for making amine-modified epoxy resin and cationic electrodeposition coating composition |
| US7790011B2 (en) | 2006-05-03 | 2010-09-07 | Basf Coatings Gmbh | Solid resin-crosslinker mixture for use in aqueous coatings |
| US7842177B2 (en) | 2006-05-03 | 2010-11-30 | Basf Coatings Gmbh | Solid pigmented resin-crosslinker mixture for use in aqueous coatings |
| JP2008018320A (ja) * | 2006-07-12 | 2008-01-31 | Nippon Paint Co Ltd | エマルションの製造方法およびその製造方法から得られる水性塗料組成物 |
-
2008
- 2008-06-30 US US12/164,883 patent/US8242234B2/en not_active Expired - Fee Related
-
2009
- 2009-06-04 EP EP09773991A patent/EP2294109B1/en not_active Not-in-force
- 2009-06-04 CN CN200980107626XA patent/CN102143985B/zh not_active Expired - Fee Related
- 2009-06-04 JP JP2011516397A patent/JP5415536B2/ja not_active Expired - Fee Related
- 2009-06-04 WO PCT/US2009/046201 patent/WO2010002539A1/en not_active Ceased
- 2009-06-04 AT AT09773991T patent/ATE540068T1/de active
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