JP2010537947A - 四フッ化ケイ素及び塩化水素を含有するガス流の処理方法 - Google Patents
四フッ化ケイ素及び塩化水素を含有するガス流の処理方法 Download PDFInfo
- Publication number
- JP2010537947A JP2010537947A JP2010524115A JP2010524115A JP2010537947A JP 2010537947 A JP2010537947 A JP 2010537947A JP 2010524115 A JP2010524115 A JP 2010524115A JP 2010524115 A JP2010524115 A JP 2010524115A JP 2010537947 A JP2010537947 A JP 2010537947A
- Authority
- JP
- Japan
- Prior art keywords
- gas stream
- ppm
- psig
- hydrogen chloride
- less
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007789 gas Substances 0.000 title claims abstract description 169
- ABTOQLMXBSRXSM-UHFFFAOYSA-N silicon tetrafluoride Chemical compound F[Si](F)(F)F ABTOQLMXBSRXSM-UHFFFAOYSA-N 0.000 title claims abstract description 162
- 238000000034 method Methods 0.000 title claims abstract description 109
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 title claims abstract description 80
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 title claims abstract description 78
- 229910000041 hydrogen chloride Inorganic materials 0.000 title claims abstract description 78
- 229910052751 metal Inorganic materials 0.000 claims abstract description 83
- 239000002184 metal Substances 0.000 claims abstract description 83
- 230000002829 reductive effect Effects 0.000 claims abstract description 16
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 18
- 229910052725 zinc Inorganic materials 0.000 claims description 17
- 239000011701 zinc Substances 0.000 claims description 17
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 10
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 8
- 229910052749 magnesium Inorganic materials 0.000 claims description 8
- 239000011777 magnesium Substances 0.000 claims description 8
- 230000006835 compression Effects 0.000 claims description 6
- 238000007906 compression Methods 0.000 claims description 6
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims description 6
- 239000011787 zinc oxide Substances 0.000 claims description 5
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 claims description 4
- 239000011592 zinc chloride Substances 0.000 claims description 3
- 235000005074 zinc chloride Nutrition 0.000 claims description 3
- UGZADUVQMDAIAO-UHFFFAOYSA-L zinc hydroxide Chemical compound [OH-].[OH-].[Zn+2] UGZADUVQMDAIAO-UHFFFAOYSA-L 0.000 claims description 3
- 229910021511 zinc hydroxide Inorganic materials 0.000 claims description 3
- 229940007718 zinc hydroxide Drugs 0.000 claims description 3
- 229910001629 magnesium chloride Inorganic materials 0.000 claims description 2
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 2
- 239000000347 magnesium hydroxide Substances 0.000 claims description 2
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 2
- 239000000395 magnesium oxide Substances 0.000 claims description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 2
- 229910000000 metal hydroxide Inorganic materials 0.000 claims description 2
- 150000004692 metal hydroxides Chemical class 0.000 claims description 2
- 229910044991 metal oxide Inorganic materials 0.000 claims description 2
- 150000004706 metal oxides Chemical class 0.000 claims description 2
- 239000011236 particulate material Substances 0.000 claims 1
- 239000012535 impurity Substances 0.000 description 50
- 238000012545 processing Methods 0.000 description 9
- 150000002739 metals Chemical class 0.000 description 6
- 238000005260 corrosion Methods 0.000 description 5
- 230000007797 corrosion Effects 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 239000000356 contaminant Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 2
- 230000002745 absorbent Effects 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000001506 calcium phosphate Substances 0.000 description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 description 2
- 235000011010 calcium phosphates Nutrition 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 150000004820 halides Chemical class 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 238000003672 processing method Methods 0.000 description 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 229910000792 Monel Inorganic materials 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 238000010960 commercial process Methods 0.000 description 1
- 230000001143 conditioned effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- -1 for example Substances 0.000 description 1
- 229910000856 hastalloy Inorganic materials 0.000 description 1
- 229910001293 incoloy Inorganic materials 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000011112 process operation Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000007514 turning Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/38—Removing components of undefined structure
- B01D53/40—Acidic components
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/68—Halogens or halogen compounds
- B01D53/685—Halogens or halogen compounds by treating the gases with solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/20—Reductants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/40—Alkaline earth metal or magnesium compounds
- B01D2251/402—Alkaline earth metal or magnesium compounds of magnesium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/60—Inorganic bases or salts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2256/00—Main component in the product gas stream after treatment
- B01D2256/26—Halogens or halogen compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/20—Halogens or halogen compounds
- B01D2257/204—Inorganic halogen compounds
- B01D2257/2045—Hydrochloric acid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2258/00—Sources of waste gases
- B01D2258/02—Other waste gases
- B01D2258/0216—Other waste gases from CVD treatment or semi-conductor manufacturing
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Biomedical Technology (AREA)
- Analytical Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Gas Separation By Absorption (AREA)
- Treating Waste Gases (AREA)
- Silicon Compounds (AREA)
- Drying Of Gases (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US96983607P | 2007-09-04 | 2007-09-04 | |
| PCT/US2008/075048 WO2009032819A1 (en) | 2007-09-04 | 2008-09-02 | Method for treatment of a gas stream containing silicon tetrafluoride and hydrogen chloride |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2010537947A true JP2010537947A (ja) | 2010-12-09 |
| JP2010537947A5 JP2010537947A5 (enExample) | 2011-09-22 |
Family
ID=40076566
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010524115A Pending JP2010537947A (ja) | 2007-09-04 | 2008-09-02 | 四フッ化ケイ素及び塩化水素を含有するガス流の処理方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US7691351B2 (enExample) |
| EP (1) | EP2188039A1 (enExample) |
| JP (1) | JP2010537947A (enExample) |
| KR (1) | KR101447310B1 (enExample) |
| CN (1) | CN101827642A (enExample) |
| MY (1) | MY150562A (enExample) |
| TW (1) | TW200927271A (enExample) |
| WO (1) | WO2009032819A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2188039A1 (en) * | 2007-09-04 | 2010-05-26 | MEMC Electronic Materials, Inc. | Method for treatment of a gas stream containing silicon tetrafluoride and hydrogen chloride |
| JP5656298B2 (ja) * | 2010-06-15 | 2015-01-21 | 協和化学工業株式会社 | 複合水酸化マグネシウム、その製造方法および吸着剤 |
| US9440218B2 (en) | 2013-06-13 | 2016-09-13 | Clariant Corporation | Methods and active materials for reducing halide concentration in gas streams |
| CN108455616A (zh) * | 2017-12-20 | 2018-08-28 | 湖北瓮福蓝天化工有限公司 | 一种氟硅酸除氯方法及装置 |
| CN114345106B (zh) * | 2021-12-30 | 2023-12-12 | 湖北瓮福蓝天化工有限公司 | 一种无水氟化氢生产过程中去除氯元素的方法及系统 |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59162122A (ja) * | 1983-03-08 | 1984-09-13 | Mitsui Toatsu Chem Inc | 四弗化ケイ素の精製法 |
| JPS6443333A (en) * | 1987-07-29 | 1989-02-15 | Andritz Ag Maschf | Purification of waste gas containing hydrochloric acid and sulfur dioxide |
| JPH06239610A (ja) * | 1992-12-22 | 1994-08-30 | Mitsui Toatsu Chem Inc | フルオロシラン |
| JPH0826715A (ja) * | 1994-07-13 | 1996-01-30 | Central Glass Co Ltd | フッ化シランの製造法およびその精製法 |
| JPH11116230A (ja) * | 1997-10-08 | 1999-04-27 | Central Glass Co Ltd | フッ化シランの精製法 |
| JPH11128675A (ja) * | 1997-11-05 | 1999-05-18 | Mitsui Chem Inc | 塩素または塩素化合物の除害方法および装置 |
| JP2003095636A (ja) * | 2001-07-12 | 2003-04-03 | Showa Denko Kk | テトラフルオロシランの製造方法およびその用途 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4557921A (en) * | 1984-06-27 | 1985-12-10 | Ethyl Corporation | Purification of halide |
| CA2096536C (fr) | 1990-11-21 | 2001-07-03 | Philippe Dumont | Hydroxyde de calcium et/ou de magnesium, sa preparation et son utilisation |
| US5378444A (en) * | 1991-12-11 | 1995-01-03 | Japan Pionics Co., Ltd. | Process for cleaning harmful gas |
| US5988165A (en) * | 1997-10-01 | 1999-11-23 | Invacare Corporation | Apparatus and method for forming oxygen-enriched gas and compression thereof for high-pressure mobile storage utilization |
| US8062521B2 (en) * | 1998-05-29 | 2011-11-22 | Crystaphase Products, Inc. | Filtering medium and method for contacting solids-containing feeds for chemical reactors |
| US6649082B2 (en) * | 2000-05-26 | 2003-11-18 | Showa Denko K.K. | Harm-removing agent and method for rendering halogen-containing gas harmless and uses thereof |
| US7666379B2 (en) * | 2001-07-16 | 2010-02-23 | Voltaix, Inc. | Process and apparatus for removing Bronsted acid impurities in binary halides |
| CN100344345C (zh) * | 2001-10-12 | 2007-10-24 | 旭硝子株式会社 | 卤素类气体的除去方法 |
| US6805728B2 (en) | 2002-12-09 | 2004-10-19 | Advanced Technology Materials, Inc. | Method and apparatus for the abatement of toxic gas components from a semiconductor manufacturing process effluent stream |
| US20050126338A1 (en) * | 2003-02-24 | 2005-06-16 | Nanoproducts Corporation | Zinc comprising nanoparticles and related nanotechnology |
| US20070116620A1 (en) * | 2005-11-21 | 2007-05-24 | Kanazirev Vladislav I | Halide scavengers for high temperature applications |
| EP2188039A1 (en) * | 2007-09-04 | 2010-05-26 | MEMC Electronic Materials, Inc. | Method for treatment of a gas stream containing silicon tetrafluoride and hydrogen chloride |
-
2008
- 2008-09-02 EP EP08829262A patent/EP2188039A1/en not_active Withdrawn
- 2008-09-02 KR KR1020107007329A patent/KR101447310B1/ko not_active Expired - Fee Related
- 2008-09-02 JP JP2010524115A patent/JP2010537947A/ja active Pending
- 2008-09-02 MY MYPI20100901 patent/MY150562A/en unknown
- 2008-09-02 WO PCT/US2008/075048 patent/WO2009032819A1/en not_active Ceased
- 2008-09-02 CN CN200880109341A patent/CN101827642A/zh active Pending
- 2008-09-02 US US12/202,807 patent/US7691351B2/en not_active Expired - Fee Related
- 2008-09-04 TW TW097133985A patent/TW200927271A/zh unknown
-
2010
- 2010-03-25 US US12/731,847 patent/US20100178225A1/en not_active Abandoned
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59162122A (ja) * | 1983-03-08 | 1984-09-13 | Mitsui Toatsu Chem Inc | 四弗化ケイ素の精製法 |
| JPS6443333A (en) * | 1987-07-29 | 1989-02-15 | Andritz Ag Maschf | Purification of waste gas containing hydrochloric acid and sulfur dioxide |
| JPH06239610A (ja) * | 1992-12-22 | 1994-08-30 | Mitsui Toatsu Chem Inc | フルオロシラン |
| JPH0826715A (ja) * | 1994-07-13 | 1996-01-30 | Central Glass Co Ltd | フッ化シランの製造法およびその精製法 |
| JPH11116230A (ja) * | 1997-10-08 | 1999-04-27 | Central Glass Co Ltd | フッ化シランの精製法 |
| JPH11128675A (ja) * | 1997-11-05 | 1999-05-18 | Mitsui Chem Inc | 塩素または塩素化合物の除害方法および装置 |
| JP2003095636A (ja) * | 2001-07-12 | 2003-04-03 | Showa Denko Kk | テトラフルオロシランの製造方法およびその用途 |
Also Published As
| Publication number | Publication date |
|---|---|
| MY150562A (en) | 2014-01-30 |
| US20090092530A1 (en) | 2009-04-09 |
| WO2009032819A1 (en) | 2009-03-12 |
| TW200927271A (en) | 2009-07-01 |
| KR20100061832A (ko) | 2010-06-09 |
| KR101447310B1 (ko) | 2014-10-06 |
| CN101827642A (zh) | 2010-09-08 |
| EP2188039A1 (en) | 2010-05-26 |
| US20100178225A1 (en) | 2010-07-15 |
| US7691351B2 (en) | 2010-04-06 |
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